Keywords

1 Introduction

In automotive and aerospace industry, power connection is constantly increasing.

Therefore, the on-board electrical power and the number of power connections such as printed circuit boards (PCB) increase significantly and the power connector was to be one of the major electric system used in the power connections. However, this development can’t be at the expense of system reliability for operational and economic reasons. It is indeed necessary that electric systems offer a reliability level which must be equivalent or even superior to the current systems. The automotive environment was particularly harsh for the electronic components and the electrical wiring systems. There are many constraints (temperature, vibration, humidity…) which are not compatible with the use of electrical components.

To ensure a good performance of the electrical connections in harsh environments, connector manufacturers have used plating contacts with noble materials such as gold or silver. Indeed, the noble materials can fight against the corrosion while ensuring a good electrical resistance.

However, due to the cost more and higher, manufacturers of electronic components have chosen to reduce the gold thickness and the plating surface. The decrease of the material thickness led to a fast wear of contact surfaces inside electrical components which leads to the voltage increase due to the fretting corrosion phenomenon [1].

In this work, the behavior of an electrical contact surface was studied when subjected the several cycles’ vibration and the change of the contact surface wear was analyzed.

1.1 Samples Used and Experimental Set-up

The present study analyzed the contact voltage change for copper alloy samples of 0.6 mm in thickness with a tin coating of 1 μm in thickness. The samples were produced with a sheet of 20 mm width, using the processing technique of stamping and bending.

The instrumented device consisted in applying indentation and insertion forces on two U-shaped samples (Fig. 1). One of the two samples was flat and the other contained a sphere with a radius R equal to 3 mm (Fig. 1). The two samples were fixed on the Teflon part (Fig. 2). Before each experiment, the sample surface was wiped by an antioxidant paste and then the sample was cleaned in an ultrasonic alcohol bath.

Fig. 1.
figure 1

Samples used

Fig. 2.
figure 2

Experimental set-up used

The experimental set-up consists of a shaker (LDS V555 with a maximum force of 939 N, maximum acceleration of 100 g (g = 9.81 m/s2)) which can apply sinusoidal vibrations with an amplitude greater than 1 μm and a frequency between 50 Hz and 100 Hz. A sinusoidal vibration was applied on the lower part of the horizontal linear stage (Fig. 2) which was attached to a slippery table [horizontal displacement between (−a) and (+a)]. The upper part of the sample was attached to a vertical slippery part. A contact force of 3 N (Fc) was applied with the help of a mass.

Two displacement sensors using laser light (0.01 μm of resolution) were used to measure the horizontal displacement of the lower sample and to give the vertical displacement of the upper sample. A D.C. current generator was installed in order to transmit an electrical current of 10 A with the help of a power supply of 14 V. The electrical measurements of the contact voltage were obtained with two oscilloscopes (Tektronix DPO5000 and TDS5000); one was used to give the contact voltage measurement and the second to detect the electrical arc appearance.

In addition a thermo-couple was used to measure the temperature near the contact zone and to stop the current source if the temperature goes beyond 150 °C.

2 Study of Contact Voltage During the Three Fretting Phases

Two ‘‘U’’ samples (plane part and spherical part) were submitted to the shaker vibrations and are moving at frequency 50 Hz with amplitude of 2a = 50 µm (peak to peak, Fig. 2) of sinus oscillations. This movement is controlled and measured by a displacement sensor (using laser with 0.1 µm of resolution) focused. These parameters simulate real conditions of use of a contact in the automotive connectors [2,3,4,5].

Figure 3 gives the change of contact voltage and contact temperature measured near the contact interface between the two sample parts versus the number of vibration cycles.

Fig. 3.
figure 3

Contact voltage and contact temperature versus cycle number (frequency = 50 Hz, total displacement amplitude 2a = 50 μm, current I = 10 A)

Three vibration phases were obtained. The first phase (from 0 kcycles to 2.5 kcycles), corresponds to the self-cleaning contact track and was the beginning of the fretting phenomenon. The second phase (from 2.5 kcycles to 8 kcycles) corresponds to the acceleration of the fretting phenomenon and stops at the saturation voltage. Finally, after 8 kcycles, there has been little change in the fretting phenomenon and the vibration test stops when the measured contact temperature reached 150 °C.

The change in temperature follows the one of the contact voltage, namely during the first phase, but at the end of the second vibration phase, a rapid temperature increase was obtained.

The temperature increase was due to fluctuating potentials whose origins were due to heating caused by electric arcs (6000 °C) and Joule’s effect dissipated in the contact interface [6].

However, the heating goes on during the third phase, despite the stabilization of the contact voltage. This phenomenon is due to the inertia and heat dissipation.

A comparison between the changes of contact voltages and phase cycle number was made for a low (I = 200 mA, V = 5 V) and a high (I = 10 A, V = 16 V) levels fretting contact (Figs. 4 and 5).

Fig. 4.
figure 4

Cycle number for three phases for low (I = 200 mA, V = 5 V) and high (I = 10 A, V = 16 V) levels fretting contact

Fig. 5.
figure 5

Cycle number for three phases for low (I = 200 mA) and high (I = 10 A) levels fretting contact

The duration of phases 1 and 2 for the low contact level was higher than the one obtained during the high level contact (Fig. 4). But the durations of the third phase were close in both level conditions.

During the phases 1 and 2, the electrical potential increase follows the current increase, especially during the first phase (Fig. 5). Indeed, during the beginning of fretting in the first phase, the electrical conduction occurs essentially between metallic spots and remains linear. As for the third phase, the current increase does not generate additional potential (the contact voltages for the two levels were equal) and the contact voltage reaches the breakdown voltage.

Figure 6 shows for different cycle numbers, the change of the contact voltage for a high level contact. Two contact voltage values were observed: a minimum value Vs obtained for 0 cycles (contact voltage without vibrations) and a maximum value Vd characterized by voltage peaks.

Fig. 6.
figure 6

Change of contact voltage (high level contact) during the first fretting phase 1 (10 A, 50 Hz, 2a = 50 µm)

The voltage peaks move to both ends of the contact track (see voltage contact change after 0.75 kcycles). This was related to the constriction of the current lines in granular media.

Figure 7 gives the voltage changes along the contact track in both vibration directions (Right way and Left way), during the phase 1, when the plane part of the ‘‘U’’ sample moves alternately from right to left direction (Fig. 2).

Fig. 7.
figure 7

Contact voltage versus displacement of contact area during the first fretting phase 1

The change analysis of the contact voltage shows that the tension peaks appear in the two directions of vibration (positive direction and negative direction) at both ends of the contact track with different values (V ≈ 43 mV for the end of the left contact track and V ≈ 32 mV for the end of the right contact track) (Fig. 7).

On the left half of the contact track, the contact voltages were more important when the plane part of ‘‘U’’ sample goes towards the positive direction (Right way, Fig. 7), while on the right half, the contact voltages were greater when the plane part of ‘‘U’’ sample goes towards the negative direction (left way).

During the second phase of vibration, the contact voltage behavior remains unchanged and the same as in the first phase (Fig. 8).

Fig. 8.
figure 8

Contact voltage versus displacement of contact area during the second fretting phase 2

Along the contact track during the third vibration phase, the contact voltage becomes unpredictable (Fig. 9) and depends on the resistive film behavior which was deposited on the contact surface.

Fig. 9.
figure 9

Contact voltage versus displacement of contact area during the third fretting phase 3

3 Study of Contact Area Worn Out by Friction During the Three Fretting Phases

Figure 10 gives the wear contact zones (with X100 magnification) after a vibration test with a frequency of 100 Hz, a current of 10 A and a shaker displacement of 50 μm. The tests were stopped at different stages of fretting. At the end of the first phase, the size of the contact track reached 377 μm and reached 762 μm and 1032 μm at the end of the second and third phase respectively. The track sizes have nearly tripled between the first and the third phase of vibration (i.e. between 2 kcycles and 100 kcycles).

Fig. 10.
figure 10

Size of contact zones at the end of the three phases of fretting

After these tests, a chemical analysis using the Energy-dispersive X-ray spectroscopy (EDX) was undertaken to quantify the different chemical element percentages on the damaged contact surface at different vibration phases (Fig. 11).

Fig. 11.
figure 11

Energy-dispersive X-ray spectroscopy of track at the end of each fretting phase

During the first vibration phase, a high tin proportion (Sn ≈ 43%) was detected. Other chemical elements with small proportions were found (O ≈ 4% and Cu ≈ 2%) (Fig. 11a). An increase of the substrate percentages (Cu) and oxygen (O) during the second phase was obtained (O ≈ 10%, Cu ≈ 9%) (Fig. 11b). During the last phase, the copper proportion increases (Cu ≈ 27%) (Fig. 11c), while the percentage of the coating decreases considerably (≈9% during the second phase and ≈6% during the third phase).

Curves of the atomic percentages for each chemical element were obtained (Fig. 12).

Fig. 12.
figure 12

Atomic percentage of elements on contact surface during the three phases of fretting

The different chemical elements come from the substrate (Cu and Zn), from the coating (Sn) and Oxygen (O).

The coating was gradually removed during the first and second vibration phases and disappeared in the third phase where the contact voltage was high. In addition, during the third phase, the oxide debris mainly consist on copper and oxygen.

Finally, the oxygen concentration increases during the first phase and remains high during the second and third phase. We assume that the oxygen and tin were bound to give SnO2 during the initial phase. But in the third phase, oxygen was bound to copper forming Cu2O.

4 Conclusion

A high level current accelerates the appearance of the first and second fretting phases and increases the temperature value at the contact interface due to Joule’s effect.

The change analysis of the contact voltage shows that the tension peaks appear in the two directions of vibration (positive and negative directions) at both ends of the contact track with different values.

On the other hand, the contact voltages on the left half and right half of the contact track are different and depend on the direction displacement.

The size of the contact zone worn out by friction has tripled between the beginning of the vibration test (phase1) and the final vibration cycles (phase 3).

EDX analysis of the contact zones has shown that different chemical elements appear at different vibration phases. Indeed, during the first damage of the contact surface which corresponds to the fretting phase 1, there were little of elements other than tin on the contact surface. The increased wear during the second phase led to the appearance of the copper layer and oxide debris (presence of oxygen), while the percentage of tin drops significantly during the third stage.