Abstract
In this section of the journal, the literature on continuous-flow synthesis (primarily organic synthesis and functional materials) from the period of January–March 2015 is presented. All the publications are listed and ordered by journal name, with review articles grouped at the end. This time, there is no section on highlighted articles; however, from the next issue, a succinct overview of specific publications will be included in this section. From the next issue, some publications having engineering principles relevant to flow synthesis will also be included in this list with specific highlights that will give new insights on flow synthesis.
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References
“A facile in situ self-assembly strategy for large-scale fabrication of CHS@MOF yolk/shell structure and its catalytic application in a flow system”
H. Gao, Y. Luan, K. Chaikittikul, W. Dong, J. Li, X. Zhang, G. Wang ACS Applied Materials & Interfaces 2015, 7, 4667–4674
“Continuous nanofiltration and recycle of an asymmetric ketone hydrogenation catalyst” E. J. O’Neal, J. Brathwaite, C. H. Lee, K. F. Jensen ACS Catalysis 2015, 5, 2615–2622
“External trapping of halomethyllithium enabled by flow microreactors” L. Degennaro, F. Fanelli, A. Giovine, R. Luisi Advanced Synthesis & Catalysis 2015, 357, 21–27
“A three-minute synthesis and purification of ibuprofen: pushing the limits of continuous-flow processing” D. R. Snead, T. F. Jamison Angewandte Chemie, International Edition 2015, 54, 983–987
“Flow-enabled self-assembly of large-scale aligned nanowires” B. Li, C. Zhang, B. Jiang, W. Han, Z. Lin Angewandte Chemie, International Edition 2015, 54, 4250–4254
“Microfluidic synthesis of rigid nanovesicles for hydrophilic reagents delivery” L. Zhang, Q. Feng, J. Wang, J. Sun, X. Shi, X. Jiang Angewandte Chemie, International Edition 2015, 54, 3952–3956
“Control for divergent, continuous, multistep syntheses of active pharmaceutical ingredients” D. Ghislieri, K. Gilmore, P. H. Seeberger Angewandte Chemie, International Edition 2015, 54, 678–682
“A systems approach towards an intelligent and self-controlling platform for integrated continuous reaction sequences” R. J. Ingham, C. Battilocchio, D. E. Fitzpatrick, E. Sliwinski, J. M. Hawkins, S. V. Ley Angewandte Chemie, International Edition 2015, 54, 144–148
“Flow-enabled self-assembly of large-scale aligned nanowires” B. Li, C. Zhang, B. Jiang, W. Han, Z. Lin Angewandte Chemie, International Edition 2015, 54, 4250–4254
“Rapid and efficient copper-catalyzed Finkelstein reaction of (hetero) aromatics under continuous-flow conditions” M. Chen, S. Ichikawa, S. L. Buchwald Angewandte Chemie, International Edition 2015, 127, 265–268
“Highly effective continuous-flow monolithic silica microreactors for acid catalyzed processes” A. Koreniuk, K. Maresz, K. Odrozek, A. B. Jarzębski, J. Mrowiec-Białoń Applied Catalysis A: General 2015, 489, 203–208
“Palladium on carbon-catalyzed Suzuki–Miyaura coupling reaction using an efficient and continuous flow system” T. Hattori, A. Tsubone, Y. Sawama, Y. Monguchi, H. Sajiki Catalysts 2015, 5, 18–25
“Heterogenization of Pd–NHC complexes onto a silica support and their application in Suzuki–Miyaura coupling under batch and continuous flow conditions” A. Martínez, J. L. Krinsky, I. Peñafiel, S. Castillón, K. Loponov, A. Lapkin, C. Claver Catalysis Science & Technology 2015, 5, 310–319
“Triethanolamine synthesis in a continuous flow microchannel reactor” D. V. Andreev, L. L. Makarshin, A. G. Gribovskii, D. Y. Yushchenko, E. E. Sergeev, E. G. Zhizhina, V. N. Parmon Chemical Engineering Journal 2015, 259, 252–256
“The continuous flow synthesis of 2,4,5-trifluorobenzoic acid via sequential Grignard exchange and carboxylation reactions using microreactors” Q. Deng, R. Shen, Z. Zhao, M. Yan, L. Zhang Chemical Engineering Journal 2015, 262, 1168–1174
“A versatile Carberry-type microcatalytic reactor for transient and/or continuous flow operation at atmospheric or medium pressure” E. L. Fornero, J. L. Giombi, D. L. Chiavassa, A. L. Bonivardi, M. A. Baltanás Chemical Engineering Journal 2015, 264, 664–671
“Characterization method for separation devices based on micro technology” T. Wellsandt, B. Stanisch, J. Strube Chemie Ingenieur Technik 2015, 87, 150–158
“The sequential continuous-flow hydrothermal synthesis of molybdenum disulphide” P. W. Dunne, A. S. Munn, C. L. Starkey, E. H. Lester Chemical Communications 2015, 51, 4048–4050
“Watching polymers grow: real time monitoring of polymerizations via an on-line ESI-MS/microreactor coupling” J. J. Haven, J. Vandenbergh, T. Junkers Chemical Communications 2015, 51, 4611–4614
“Continuous flow reduction of artemisinic acid utilizing multi-injection strategies—closing the gap towards a fully continuous synthesis of antimalarial drugs” B. Pieber, T. Glasnov, C. O. Kappe Chemistry–A European Journal 2015, 21, 4368–4376
“Immobilization and continuous recycling of photoredox catalysts in ionic liquids for applications in batch reactions and flow systems: catalytic alkene isomerization by using visible light” D. C. Fabry, M. A. Ronge, M. Rueping Chemistry–A European Journal 2015, 21, 5350–5354
“Continuous photo fermentative production of hydrogen by immobilized Rhodobacter sphaeroides OU 001” R. Zagrodnik, K. Seifert, M. Stodolny, M. Laniecki International Journal of Hydrogen Energy 2015, 40, 5062–5073
“Aminopropyl-silica-supported Cu nanoparticles: an efficient catalyst for continuous-flow Huisgen azide-alkyne cycloaddition (CuAAC)” R. P. Jumde, C. Evangelisti, A. Mandoli, N. Scotti, R. Psaro Journal of Catalysis 2015, 324, 25–31
“Iridium(I)-catalyzed ortho-directed hydrogen isotope exchange in continuous-flow reactors” E. Habraken, P. Haspeslagh, M. Vliegen, T. Noël Journal of Flow Chemistry 2015, 5, 2–5
“Synthesis of N-hydroxypyrazin-2(1H)-ones via selective O-debenzylation of 1-benzyloxypyrazin-2(1H)-ones using flow methodology” A. Mai, W. De Borggraeve Journal of Flow Chemistry 2015, 5, 6–10
“Continuous-flow hydroisomerization of C5–C7 alkanes using mechanochemically synthesized supported Pt and Pd–SBA-15 materials” J. Hidalgo, A. Pineda, R. Arancon, R. Černý, M. Climent, A. Romero, R. Luque Journal of Flow Chemistry 2015, 5, 11–16
“Continuous-flow stereoselective synthesis in microreactors: nucleophilic additions to nitrostyrenes organocatalyzed by a chiral bifunctional catalyst” S. Rossi, M. Benaglia, A. Puglisi, C. Filippo, M. Maggini Journal of Flow Chemistry 2015, 5, 17–21
“Catalytic properties of platinum nanoparticles obtained in a single step simultaneous reduction of Pt(IV) ions and graphene oxide” M. Wojnicki, M. Luty-Błocho, K. Mech, J. Grzonka, K. Fitzner, K. Kurzydłowski Journal of Flow Chemistry 2015, 5, 22–30
“Understanding the performance of a microfluidic electrolysis cell for routine organic electrosynthesis” R. Green, R. Brown, D. Pletcher Journal of Flow Chemistry 2015, 5, 31–36
“Wall-coated polymer brushes as support for chiral organocatalysts in microreactors” R. Munirathinam, A. Leoncini, J. Huskens, H. Wormeester, W. Verboom Journal of Flow Chemistry 2015, 5, 37–42
“Palladium-catalyzed carbon–carbon cross-coupling reactions in thermomorphous double emulsions” V. Misuk, A. Mai, K. Giannopoulos, D. Karl, J. Heinrich, D. Rauber, H. Löwe Journal of Flow Chemistry 2015, 5, 43–47
“Massive, generic, and controlled microencapsulation by flow focusing: some physicochemical aspects and new applications” A. Gañán-Calvo, E. Castro-Hernández, M. Flores-Mosquera, L. Martín-Banderas Journal of Flow Chemistry 2015, 5, 48–54
“Immobilized palladium nanoparticles on potassium zirconium phosphate as an efficient recoverable heterogeneous catalyst for a clean Heck reaction in flow” C. Petrucci, M. Cappelletti, O. Piermatti, M. Nocchetti, M. Pica, F. Pizzo, L. Vaccaro Journal of Molecular Catalysis A: Chemical 2015, 401, 27–34
“Novel synthesis of thick wall coatings of titania supported Bi poisoned Pd catalysts and application in selective hydrogenation of acetylene alcohols in capillary microreactors” N. Cherkasov, A. O. Ibhadon, E. V. Rebrov Lab on a Chip 2015, 15, 1952–1960
“Site-specific protein modification using immobilized sortase in batch and continuous-flow systems” M. D. Witte, T. Wu, C. P. Guimaraes, C. S. Theile, A. E. Blom, J. R. Ingram, H. L. Ploegh Nature Protocols 2015, 10, 508–516
“Flow synthesis of ethyl isocyanoacetate enabling the telescoped synthesis of 1,2,4-triazoles and pyrrolo-[1,2-c] pyrimidines” M. Baumann, A. M. R. Garcia, I. R. Baxendale Organic & Biomolecular Chemistry 2015, 13, 4231–4239
“Development of a flow method for the hydroboration/oxidation of olefins” J. A. Souto, R. A. Stockman, S. V. Ley, Organic & Biomolecular Chemistry 2015, 13, 3871–3877
“Organocatalyzed Beckmann rearrangement of cyclohexanone oxime in a microchemical system” J. Zhang, C. Dong, C. Du, G. Luo Organic Process Research & Development 2015, 19, 352–356
“Large-scale continuous flow transformation of oximes into fused-bicyclic isoxazolidines: an example of process intensification” J. A. Rincón, C. Mateos, P. García-Losada, D. J. Mergott Organic Process Research & Development 2015, 19, 347–351
“Preparation of PEGA grafted poly(chloromethylstyrene-co-ethylene glycol dimethacrylate) monolith for high-efficiency solid phase peptide synthesis under continuous flow techniques” R. Zhang, Q. Li, Y. Huang, L. Zhao, P. Ye, G. Ma, Z. Su Polymer 2015, 61, 115–122
“Synergic effect of nano-catalyst and continuous flow system: Dakin–West reaction catalyzed by Nafion-H@SPIONs in a microreactor” Z. A. Narei, B. Shafiee, A. R. Khosropour RSC Advances 2015, 5, 20132–20137
“Continuous flow photooxygenation of monoterpenes” C. Y. Park, Y. J. Kim, H. J. Lim, J. H. Park, M. J. Kim, S. W. Seo, C. P. Park RSC Advances 2015, 5, 4233–4237
“Continuous flow vortex fluidic synthesis of silica xerogel as a delivery vehicle for curcumin” C. L. Tong, U. H. Stroeher, M. H. Brown, C. L. Raston RSC Advances 2015, 5, 7953–7958
“Facile azide formation via diazotransfer reaction in a copper tube flow reactor” K. Nuyts, M. Ceulemans, T. N. Parac-Vogt, G. Bultynck, W. M. De Borggraeve Tetrahedron Letters 2015, 56, 1687–1690
“Hydrothermal continuous flow synthesis and exfoliation of NiCo layered double hydroxide nanosheets for enhanced oxygen evolution catalysis” H. Liang, F. Meng, M. Cabán-Acevedo, L. Li, A. Forticaux, L. Xiu, Z. Wang, S. Jin Nano Letters 2015, 15, 1421–1427
“Synthesis of uniform α-Si3N4 nanospheres by RF induction thermal plasma and their application in high thermal conductive nanocomposites” G. Hou, B. Cheng, F. Ding, M. Yao, P. Hu, F. Yuan ACS Applied Materials & Interfaces 2015, 7, 2873–2881
Microfluidic reactor synthesis and photocatalytic behavior of Cu@Cu2O nanocomposite C. L. Xu, S. Kannan, J. H. Peng, M. Yan, D. Zhang, L. Zhang Applied Surface Science 2015, 331, 449–454
“Continuous flow preparation of iron oxide nanoparticles supported on porous silicates” A. Yepez, F. L. Y. Lam, A. A. Romero, C. O. Kappe, R. Luque ChemCatChem 2015, 7, 276–282
“Microfluidic supercritical antisolvent continuous processing and direct spray-coating of poly(3-hexylthiophene) nanoparticles for OFET devices” R. Couto, S. Chambon, C. Aymonier, E. Mignard, B. Pavageau, A. Erriguible, S. Marre Chemical Communications 2015, 51, 1008–1011
“Continuous synthesis of size-tunable silver nanoparticles by a green electrolysis method and multi-electrode design for high yield” Z. Huang, H. Jiang, P. Liu, J. Sun, D. Guo, J. Shan, N. Gu Journal of Materials Chemistry A 2015, 3, 1925–1929
“A flexible lab-on-a-chip for the synthesis and magnetic separation of magnetite decorated with gold nanoparticles” F. C. Cabrera, A. F. A. A. Melo, J. C. P. de Souza, A. E. Job, F. N. Crespilho Lab on a Chip 2015, 15, 1835–1841
“Large-scale synthesis of high quality InP quantum dots in a continuous flow-reactor under supercritical conditions” C. Ippen, B. Schneider, C. Pries, S. Kröpke, T. Greco, A. Holländer Nanotechnology 2015, 26, 085604
“Flow synthesis of plasmonic gold nanoshells via a microreactor” S. Watanabe, T. Hiratsuka, Y. Asahi, A. Tanaka, K. Mae, M. T. Miyahara Particle and Particle System Characterization 2015, 32, 234–242
“An advanced centrifugal microsystem toward high-throughput multiplex colloidal nanocrystal synthesis” B. H. Park, D. Kim, J. H. Jung, S. J. Oh, G. Choi, D. C. Lee, T. S. Seo Sensors and Actuators B: Chemical 2015, 209, 927–933
“Simulation for scale-up of a confined jet mixer for continuous hydrothermal flow synthesis of nanomaterials” Y. C. Ma, J. L. Jing, Y. Zhang, Z. X. Wang The Journal of Supercritical Fluids 2015, 98, 211–221
Reviews
“Flow chemistry: intelligent processing of gas–liquid transformations using a tube-in-tube reactor” M. Brzozowski, M. O’Brien, S. V. Ley, A. Polyzos Accounts of Chemical Research 2015, 48, 349–362
“Toward continuous and scalable production of colloidal nanocrystals by switching from batch to droplet reactors” G. Niu, A. Ruditskiy, M. Vara, Y. Xia Chemical Society Reviews 2015, doi: 10.1039/C5CS00049A
“Microreactor array device” P. Wiktor, A. Brunner, P. Kahn, J. Qiu, M. Magee, X. F. Bian, K. Karthikeyan, J. LaBaer Scientific Reports 2015, 5, Article number: 8736, doi: 10.1038/srep08736
“Diazo compounds in continuous-flow technology” S. T. R. Mueller, T. Wirth ChemSusChem 2015, 8, 245–250
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Kulkarni, A.A. Highlights from the Flow Chemistry Literature 2015 (Part 1). J Flow Chem 5, 119–122 (2015). https://doi.org/10.1556/1846.2015.00020
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DOI: https://doi.org/10.1556/1846.2015.00020