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Effects of varying calcination temperatures on the optoelectronic and electrical properties of Ni0.4Cu0.4Cd0.2FeCrO4 spinel ferrites

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Abstract

This research investigates the properties of Ni0.4Cu0.4Cd0.2FeCrO4 spinel ferrites at calcination temperatures of 850 °C and 950 °C. X-ray diffraction measurements show a higher average crystallite size and lattice constant for the sample calcined at 950 °C. Conversely, both the tetrahedral (A) and octahedral (B) cation-oxygen bond lengths (dA-O and dB-O) decreased with increasing calcination temperature. To assess the optical properties, absorbance measurements and the Tauc method are employed, which reveal direct optical transitions with an estimated band-gap energy (Eg) of 1.99 eV at 850 °C and 1.89 eV at 950 °C. Furthermore, a comprehensive analysis of other optical parameters, including the penetration depth, refractive index, extinction coefficient, dielectric constants, and optical conductivity, is conducted. Important conclusions about the possible optoelectronic uses of the produced samples were deduced from the changes in these parameters. The electrical conductivity study reveals that the samples exhibit semiconductor behavior, according to the NSPT and CBH conduction models. Moreover, the samples show a decrease in activation energy (Ea) from 0.39 eV (at 850 °C) to 0.33 eV (at 950 °C) and exhibit high electrical resistivity, making them promising candidates for electrical devices.

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Authors and Affiliations

  1. Laboratory of Physical Chemistry of Materials, Physics Department, Faculty of Sciences of Monastir, Monastir University, 5019, Monastir, Tunisia

    Dhouha Hcini & Abdessalem Dhahri

  2. Laboratory of Advanced Multifunctional Materials and Technological Applications, Faculty of Science and Technology of Sidi Bouzid, University Campus Agricultural City, Kairouan University, 9100, Sidi Bouzid, Tunisia

    Dhouha Hcini & Sobhi Hcini

  3. Department of Physics, College of Science, Qassim University, 51452, Buraydah Almolaydah, Buraydah, Saudi Arabia

    Raihane Charguia & Fikria Jabli

  4. Mechanical and Energy Engineering Department, Imam Abdulrahman Bin Faisal University, 31441, Dammam, Saudi Arabia

    Taher Maatallah

  5. Laboratory of Physics of Materials and Nanomaterials Applied to the Environment (LaPhyMNE), Faculty of Sciences of Gabès Cited Erriadh, University of Gabès, 6079, Gabès, Tunisia

    Kamel Khirouni

  6. Department of Mechanical Engineering, College of Engineering, Prince Sattam Bin Abdulaziz University, 16273, Alkharj, Saudi Arabia

    M. L. Bouazizi

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Hcini, D., Hcini, S., Charguia, R. et al. Effects of varying calcination temperatures on the optoelectronic and electrical properties of Ni0.4Cu0.4Cd0.2FeCrO4 spinel ferrites. J Mater Sci: Mater Electron 35, 1062 (2024). https://doi.org/10.1007/s10854-024-12765-4

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