Abstract
Fracture mechanics analysis of shear band propagation requires knowledge of the material’s shear fracture energy and its related properties such as the characteristic slip displacement. Yet these properties of stiff clays and shales have not been investigated systematically. This work characterizes and analyzes the shear fracture energies and characteristic slip displacements of various stiff clays and shales based on their triaxial compression data from the literature. A methodology originally developed for hard rocks was adopted for this purpose. Results show that the shear fracture energies of stiff clays and shales generally increase with the effective normal stress on the slip plane, varying by orders of magnitude—approximately from \(4\times 10^{1}\) to \(7\times 10^{3}\) J/m\(^{2}\)—in the range of effective normal stresses from \(10^{2}\) to \(10^{5}\) kPa. An empirical equation is presented for a first-order estimate of the shear fracture energy under a given effective normal stress. The characteristic slip displacements at the laboratory scale are calculated to be smaller than 6 mm, and they appear independent of the effective normal stress. Compared with their nominal values calculated without considering the change of normal stress in triaxial tests, the shear fracture energies are approximately 70% of the nominal values, whereas the characteristic slip displacements are nearly identical to the nominal ones.
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1 Introduction
Shear failures in brittle geomaterials are associated with localization of deformation into narrow zones, which are called shear bands in general, and slip surfaces in soil mechanics. Mathematically, the onset of shear band localization has been well described by bifurcation analysis [1, 2]. Nevertheless, the propagation of a shear band, which is beyond the scope of bifurcation analysis, is also important for many problems. A representative example is progressive failure in low-permeability geomaterials such as clays and shales.
Over the decades, a number of researchers have studied the application of fracture mechanics principles to understand and analyze the propagation of shear bands in geomaterials. Skempton [3], Bjerrum [4], and Bishop [5] were the first to suggest and apply fracture mechanics concepts to slip surface growth in progressive failure. Later, Palmer and Rice [6] formulated a fracture mechanics theory for the growth of a shear band, deriving conditions for propagation. Since 2004, Puzrin and coworkers have pioneered the shear band propagation approach, whereby a generalized version of Palmer and Rice’s theory is applied to slope stability analyses [7,8,9,10]. Quinn et al. [11, 12] have also used the theory of Palmer and Rice to study progressive failure in sensitive clays. Meanwhile, Viesca and Rice [13] have extended the theory to slip surface growth triggered by localized increase of pore pressure, providing insight into the initiation of submarine landslides under various conditions. Very recently, Fei and Choo [14, 15] have developed a numerical method that can simulate a shear banding process from initiation to propagation, by incorporating Palmer and Rice’s theory into phase-field modeling of fracture. Thanks to these advances, fracture mechanics can now be applied to a variety of geotechnical problems that involve shear banding.
Fracture mechanics analysis of shear bands requires knowledge of the material’s shear fracture energy: the energy released during generation of a unit area of slip surface, which corresponds to the critical energy release rate for mode II fracture. Rice [16] suggested an integration scheme to calculate the shear fracture energy of a material from its post-failure deformation data. Following this suggestion, Wong [17] devised a specific procedure to estimate the shear fracture energy from a triaxial compression test, applying it to data from Westerly granite under different pressures and temperatures. Later, Wong [18] refined the procedure to consider change in the normal stress on the failure plane, studying how the shear fracture energies of rocks depend on the normal stress. The procedure has also been adopted by other researchers to estimate shear fracture energies of hard rocks under various conditions, e.g. [19]. The shear fracture energies of rocks characterized in these studies have been useful for addressing fault rupture problems in seismology, e.g. [20, 21].
Nevertheless, no study seems to have examined shear fracture energies of stiff clays and shales in a similar way, although the theory of Palmer and Rice [6] was originally concerned with overconsolidated clays. So it remains mostly unknown what are the typical values of shear fracture energies of these materials and how much the shear fracture energies would depend on the normal stress on the slip plane.
To fill this knowledge gap, this work characterizes and analyzes shear fracture energies of stiff clays and shales and their related quantities based on triaxial test data from the literature. At the outset, it is noted that here the shear fracture energy is regarded as the surface energy dissipated until the material attains a purely frictional residual strength—being consistent with Palmer and Rice’s theory—which can usually be characterized by triaxial/shear-box tests. Some materials, however, manifest “true” residual strength after a very large amount of slip, as a consequence of particle alignment along a localized slip surface [22]. Such residual strength, which is slightly lower than the purely frictional strength, may not be measured by a triaxial/shear-box test but by a ring shear test [23]. Nevertheless, the present work analyzes triaxial test data because drained stress–strain responses under different confining pressures are mostly available from triaxial tests. It would also be debatable whether strength evolution due to particle alignment should be included in fracture energy calculation. A thorough comparison between shear fracture energies of stiff clays and shales characterized by triaxial and ring shear test data is left as a topic of future research.
2 Methodology
2.1 Theory
Consider the softening process during which the shear stress (\(\tau \)) decreases from the peak strength (\(\tau _{\mathrm{p}}\)) to the residual strength (\(\tau _{\mathrm{r}}\)). Palmer and Rice [6] derived that the shear fracture energy (\({\mathcal{G}}\)) is given by
Here, \(\delta \) is the slip displacement along the shear fracture surface, and \(\delta _{\mathrm{r}}\) is its value when shear stress reaches the residual shear strength. Also, \(\bar{\delta }\) is the characteristic slip displacement, which can be used to analyze the stability and size effect of shear band propagation [6, 8, 11, 13]. For example, the critical length of a shear band (\(L_{\mathrm{cr}}\)), above which propagation of the shear band can be triggered without a further increase in shear stress, is related to \(\bar{\delta }\) as \(L_{\mathrm{cr}} \propto \sqrt{\bar{\delta }}\) for a shallow-seated slip surface [8, 13] and \(L_{\mathrm{cr}} \propto \bar{\delta }\) for a deep-seated one [13].
To characterize shear fracture energies from post-peak results of triaxial compression tests, this work adopted the procedure developed by Wong [17, 18]. As shown in Fig. 1, the shear stress and slip displacement can be calculated from triaxial test data as
where \(\sigma_{1}^{\prime }\) and \(\sigma_{3}^{\prime }\) are the maximum and minimum effective principal stresses, respectively, \(\Delta {l}\) is the axial displacement of the specimen, and \(\theta \) is the angle of failure plane from the direction of \(\sigma _{1}\).
Equation (1) assumes that shear stress is a function of the slip displacement only, as it was derived from a simple shear problem where the effective normal stress on the slip plane (\(\sigma _{\mathrm{n}}^{\prime }\)) is constant. In a triaxial test where confining pressure is kept constant, however, \(\sigma _{\mathrm{n}}^{\prime }\) decreases during the softening process. This decrease in \(\sigma _{\mathrm{n}^{\prime }}\) makes the amount of stress drop (\(\tau _{\mathrm{p}} - \tau _{\mathrm{r}}\)) significantly larger than that under a constant normal stress, as illustrated in Fig. 2.
On the basis of an unpublished analysis of Rice, Wong [18] presented a method to consider the effect of evolving \(\sigma _{\mathrm{n}}^{\prime }\) during triaxial compression. Let us refer to quantities directly obtained from a triaxial test as nominal, denoting them with subscript \((\cdot )_{{\mathrm{nom}}}\). The nominal shear fracture energy is given by
where
Note that Wong [18] did not distinguish between \((\tau _{\mathrm{p}} - \tau _{\mathrm{r}})_{{\mathrm{nom}}}\) and \((\tau _{\mathrm{p}} - \tau _{\mathrm{r}})\), but later Liu and Rummel [19] did so. To incorporate the dependence of \(\tau _{\mathrm{p}}\) and \(\tau _{\mathrm{r}}\) on \(\sigma _{\mathrm{n}}^{\prime }\), their relationships are approximated as
where A, B, a, and b are constants. Then, the shear fracture energy can be calculated as (see Wong [18] for detailed derivation)
where
with
denoting the loading path in a triaxial compression test, as illustrated in Fig. 2.
Importantly, Eq. (6) shows that the dependence of \({\mathcal{G}}\) on \(\sigma _{\mathrm{n}}^{\prime }\) is determined by \((A-a)\). This has been experimentally confirmed for rocks (e.g. [18, 19, 24]). Note that the value of \((A-a)\), and so the dependence of \({\mathcal{G}}\) on \(\sigma _{\mathrm{n}}^{\prime }\), can differ significantly by material. Also, because \(\sigma _{\mathrm{n}}^{\prime }\) in Eq. (6) changes during the softening process, this work will present upper and lower bounds on \({\mathcal{G}}\), as in Wong [18].
2.2 Data collection and analysis
The foregoing procedure was applied to determine shear fracture energies of various brittle clays and shales from their post-failure deformation data in the literature. To exclude pore pressure effects on the shear fracture energy, this work only considered results from drained triaxial tests. Table 1 summarizes the materials investigated in this work. Most of these materials were compressed only in the direction normal to the bedding plane, while the Opalinus clay [25] and the Tournemire shale [26] samples were loaded in multiple directions. For consistency, this work only used test data from samples loaded in the bedding-plane normal direction. If \(\theta \) was not provided, it was assumed from Mohr–Coulomb theory. Other details followed the methodology of Wong [18]. To minimize bias, a computer program was developed that automatically calculates shear fracture energies from digitized data. The program was verified by re-calculating the shear fracture energies of different rock specimens in the literature.
3 Results and discussion
3.1 Shear fracture energies
Figure 3 presents the computed values of shear fracture energy with respect to the effective normal stress. It can be seen that the shear fracture energies of these materials vary by orders of magnitude, showing a generally increasing trend with effective normal stresses. Specifically, the shear fracture energies range approximately from \(4\times 10^{1}\) to \(7\times 10^{3}\) J/m\(^{2}\) when the effective normal stress is varied from \(10^{2}\) to \(10^{5}\) kPa. Compared with the shear fracture energies of hard rocks such as granite and gabbro [18], those of stiff clays are about two orders of magnitude lower and exhibit a stronger dependence on the effective normal stress. Yet the shear fracture energies of shales are comparable to those of molded gypsum [24].
As shown in Fig. 3, the values of shear fracture energies and normal stresses can be roughly fitted to the following equation
where \(p_{\mathrm{atm}}=101.3\) kPa is the atmospheric pressure, which is introduced for dimensional consistency. This equation may provide a first-order estimate of the shear fracture energy of a stiff clay or shale when experimental result is unavailable. Interestingly, Eq. (9) is form-identical to a common empirical relationship between the initial shear stiffness (or shear wave velocity) and the effective normal stress in the loading direction [36, 37]. The value of the exponent, 0.72, is also comparable with the typical values of the shear stiffness/velocity equation for fine-grained soils (e.g. [38, 39]).
Despite the general relationship between the shear fracture energies and effective normal stresses, individual materials exhibit varied degrees of stress dependence. This variance can be attributed to that the value of \((A - a)\) in Eq. (6), which is related to the difference between the peak and residual friction angles, is quite different by materials. Further, because the peak strength envelope of soils and rocks is becoming flatter as the normal stress increases [40, 41], the value of A is small at a relatively high normal stress. This explains why the shear fracture energies of shales at high normal stresses appear nearly stress independent. Therefore, although Eq. (9) may be used for a first-order estimate of the shear fracture energies of stiff clays and shales in general, this equation would not be a proper means for assessing the stress dependence of the shear fracture energy of an individual material. For an individual material, it would be more appropriate to use Eq. (6) or another equation derived in a similar manner.
As an additional note, one should be aware that the shear fracture energy may be scale dependent. For dynamic rupture of rock faults, Abercrombie and Rice [20] and Nielsen et al. [42] have argued that \({\mathcal{G}}\propto \delta _{\mathrm{tot}}^{1.3}\) and \({\mathcal{G}}\propto \delta _{\mathrm{tot}}\), respectively, where \(\delta _{\mathrm{tot}}\) is the total slip of a fault. Also, Viesca and Garagash [21] have found \({\mathcal{G}}\propto \delta _{\mathrm{tot}}^{2}\) for small earthquake events and \({\mathcal{G}}\propto \delta _{\mathrm{tot}}^{2/3}\) for large events, elucidating that thermal pressurization is a major mechanism for scaling on fault rupture dynamics. A similar scale-dependence of shear fracture energy may also exist for shear bands in stiff clays and shales. Probing this hypothesis is believed to be an important future research topic.
3.2 Characteristic slip displacements
Figure 4 shows the characteristic slip displacements of the clay and shale samples with respect to the effective normal stresses. As can be seen, the characteristic slip displacements are smaller than 6 mm, and they appear unrelated to the effective normal stress. This apparent stress-independence suggests that \(\bar{\delta }\) can be used for fracture mechanics analysis without consideration of normal stress.
The values of characteristic slip displacements computed herein are close to those calculated from other types of laboratory tests on stiff clays. For example, Palmer and Rice [6] report that the characteristic slip displacements of overconsolidated London clay lie in between 2 and 10 mm, based on the shear test data of Skempton [3] and Skempton and Petley [43]. Also, \(\bar{\delta }\approx 3.9\) mm is computed by the authors for the experimental result of Puzrin et al. [9] on an overconsolidated clay in a 2-m-long inclined slope. It is noted that the characteristic slip displacements of clays and shales are greater than those of hard rocks (\(<1\) mm), because they become greater for more ductile materials [12].
It is emphasized again, however, that a scale effect might exist in the characteristic slip displacement. In the context of fault rupture, several studies have suggested \({\bar{\delta }} \propto \delta _{\mathrm{tot}}\) [44,45,46,47]. Because \({\bar{\delta }}=(\tau _{\mathrm{p}} - \tau _{\mathrm{r}})/{\mathcal{G}}\), this scale dependence of \({\bar{\delta }}\) is consistent with \({\mathcal{G}}\propto \delta _\mathrm{tot}^{1.3}\) [20], and exactly the same as \({\mathcal{G}}\propto \delta _{\mathrm{tot}}\) [42] if \(\tau _{\mathrm{p}}\) and \(\tau _{\mathrm{r}}\) are considered scale independent. Although no investigation has been performed regarding the scale effect of the characteristic slip displacement in shear band propagation in soils and weak rocks, there is limited evidence suggesting a similar scale effect might also exist. For example, from back-analysis of a submarine landslide, Puzrin et al. [10] state that the characteristic slip displacement of the landslide sediment is constrained in between 100 and 160 mm, which is far greater than those estimated from laboratory experiments. If such a scale effect exists, the critical length (\(L_{\mathrm{cr}}\)) might be underestimated from laboratory tests, leading to an overly conservative stability analysis. This aspect is believed to deserve further investigations.
3.3 True versus nominal values
Figure 5 compares the shear fracture energies and characteristic slip displacements with their nominal values. From Fig. 5a, one can see that the nominal shear fracture energies are consistently greater than the true shear fracture energies, which is a natural consequence of that the nominal stress drop \((\tau _{\mathrm{p}} - \tau _{\mathrm{r}})_{\mathrm{nom}}\) is greater than the true stress drop \((\tau _{\mathrm{p}} - \tau _{\mathrm{r}})\) under a constant normal stress test (cf. Fig. 2).
Remarkably, irrespective of materials and normal stresses, it is found that the shear fracture energies are consistently around \(70\%\) of their nominal values. This consistency is interesting because \({\mathcal{G}}/{\mathcal{G}}_{\mathrm{nom}}\) of the rocks studied in Wong [18] and Liu and Rummel [19] show non-trivial variances (e.g. \({\mathcal{G}}/{\mathcal{G}}_{\mathrm{nom}}\approx 0.35\)–0.5 for Fichtelbirge granite). By contrast, as shown in Fig. 5b, the characteristic slip displacements are nearly identical to their nominal values. This similarity, which has also been observed for rocks [19], affirms the stress-independence of the characteristic slip displacements. To summarize,
These approximations may be useful because it is much easier to calculate nominal values than true values.
4 Conclusion
Based on the results above, the following conclusions can be drawn regarding the shear fracture energies and characteristic slip displacements of stiff clays and shales estimated from triaxial tests:
-
1.
The shear fracture energies generally increase with the effective normal stress on the slip plane, varying by orders of magnitude—approximately from \(4\times 10^{1}\) to \(7\times 10^{3}\) J/m\(^{2}\)—in the range of effective normal stresses from \(10^{2}\) to \(10^{5}\) kPa.
-
2.
An empirical Eq. (9) may provide a first-order estimate of the shear fracture energy under a given effective normal stress.
-
3.
The characteristic slip displacements are smaller than 6 mm, and they appear independent of the effective normal stress.
-
4.
Compared with their nominal values calculated without considering the change of normal stress in triaxial tests, the shear fracture energies are approximately 70% of the nominal values, whereas the characteristic slip displacements are nearly identical to the nominal ones.
These findings can be useful for fracture mechanics analysis of shear band propagation in stiff clays and shales. Special care should be exercised, however, when the material of interest would attain its residual strength after a very large slip displacement that cannot be imposed in triaxial tests. It is also emphasized that future work is necessary to elucidate scale effects on the shear fracture energies and characteristic slip displacements of these materials.
References
Rudnicki JW, Rice JR (1975) Conditions for the localization of deformation in pressure-sensitive dilatant materials. J Mech Phys Solids 23(6):371–394
Vardoulakis I, Goldscheider M, Gudehus G (1978) Formation of shear bands in sand bodies as a bifurcation problem. Int J Numer Anal Methods Geomech 2(2):99–128
Skempton AW (1964) Long-term stability of clay slopes. Géotechnique 14(2):77–102
Bjerrum L (1967) Progressive failure in slopes of overconsolidated plastic clay and clay shales. J Soil Mech Found Div 93:1–49
Bishop AW (1968). Progressive failure—with special reference to the mechanism causing it. In: Proceedings of the geotechnical conference, Vol. 2. Norwegian Geotechnical Institute, pp. 142–150
Palmer AC, Rice JR (1973) The growth of slip surfaces in the progressive failure of over-consolidated clay. Proc R Soc Lond A Math Phys Sci 332(1591):527–548
Puzrin AM, Germanovich LN, Kim S (2004) Catastrophic failure of submerged slopes in normally consolidated sediments. Géotechnique 54(10):631–643
Puzrin AM, Germanovich LN (2005) The growth of shear bands in the catastrophic failure of soils. Proc R Soc A Math Phys Eng Sci 461(2056):1199–1228
Puzrin AM, Germanovich LN, Friedli B (2016) Shear band propagation analysis of submarine slope stability. Géotechnique 66(3):188–201
Puzrin AM (2016) Simple criteria for ploughing and runout in post-failure evolution of submarine landslides. Can Geotech J 53(8):1305–1314
Quinn P, Diederichs M, Rowe R, Hutchinson D (2011) A new model for large landslides in sensitive clay using a fracture mechanics approach. Can Geotech J 48(8):1151–1162
Quinn P, Diederichs M, Rowe R, Hutchinson D (2012) Development of progressive failure in sensitive clay slopes. Can Geotech J 49(7):782–795
Viesca RC, Rice JR (2012) Nucleation of slip-weakening rupture instability in landslides by localized increase of pore pressure. J Geophys Res Solid Earth 117(B3):1–21
Fei F, Choo J (2020) A phase-field model of frictional shear fracture in geologic materials. Comput Methods Appl Mech Eng 369:113265
Fei F, Choo J (2021) Double-phase-field formulation for mixed-mode fracture in rocks. Comput Methods Appl Mech Eng 376:113655
Rice JR (1980) The mechanics of earthquake rupture. In: Physics of the earth’s interior. Italian Physical Society, pp 555–649
Wong T-F (1982) Shear fracture energy of Westerly granite from post-failure behavior. J Geophys Res Solid Earth 87(B2):990–1000
Wong T (1986) On the normal stress dependence of the shear fracture energy. In: Earthquake source mechanics, vol 37. American Geophysical Union, pp 1–11
Liu Z, Rummel F (1990) Shear fracture energy of rock at high pressure and high temperature. Phys Chem Earth 17:99–109
Abercrombie RE, Rice JR (2005) Can observations of earthquake scaling constrain slip weakening? Geophys J Int 162(2):406–424
Viesca RC, Garagash DI (2015) Ubiquitous weakening of faults due to thermal pressurization. Nat Geosci 8(11):875–879
Mitchell JK, Soga K (2005) Fundamentals of soil behavior. Wiley, Hoboken
Bishop AW, Green GE, Garga VK, Andresen A, Brown JD (1971) A new ring shear apparatus and its application to the measurement of residual strength. Géotechnique 21(4):273–328
Mutlu O, Bobet A (2006) Slip propagation along frictional discontinuities. Int J Rock Mech Min Sci 43(6):860–876
Favero V, Ferrari A, Laloui L (2018) Anisotropic behaviour of Opalinus Clay through consolidated and drained triaxial testing in saturated conditions. Rock Mech ICS Rock Eng 51(5):1305–1319
Niandou H, Shao J, Henry J, Fourmaintraux D (1997) Laboratory investigation of the mechanical behaviour of Tournemire shale. Int J Rock Mech Min Sci 34(1):3–16
Shi X, Herle I, Yin J (2018) Laboratory study of the shear strength and state boundary surface of a natural lumpy soil. J Geotech Geoenviron Eng 144(12):04018093
Wong RCK (1998) Swelling and softening behaviour of La Biche shale. Can Geotech J 32(2):206–221
Bishop AW, Webb DL, Lewin PI (1965) Undisturbed samples of London Clay from the Ashford Common shaft: strength-effective stress relationships. Géotechnique 15(1):1–31
Lo K (1972) An approach to the problem of progressive failure. Can Geotech J 9(4):407–429
Parry RHG (1972) Some properties of heavily overconsolidated Oxford Clay at a site near Bedford. Geotechnique 22(3):485–507
Callisto L, Rampello S (2002) Shear strength and small-strain stiffness of a natural clay under general stress conditions. Géotechnique 52(8):547–560
Burland J, Rampello S, Georgiannou V, Calabresi G (1996) A laboratory study of the strength of four stiff clays. Géotechnique 46(3):491–514
Mandaglio M, Moraci N, Rosone M, Farulla CA (2016) Experimental study of a naturally weathered stiff clay. Can Geotech J 53(12):2047–2057
Callisto L, Rampello S (2004) An interpretation of structural degradation for three natural clays. Can Geotech J 41(3):392–407
Hardin BO, Richart FE Jr (1963) Elastic wave velocities in granular soils. J Soil Mech Found Eng 89:33–65
Santamarina JC, Klein KA, Fam MA (2001) Soils and waves. Wiley, New York
Rampello S, Viggiani G, Amorosi A (1997) Small-strain stiffness of reconstituted clay compressed along constant triaxial effective stress ratio paths. Géotechnique 47(3):475–489
Choo J, Jung Y-H, Chung C-K (2011) Effect of directional stress history on anisotropy of initial stiffness of cohesive soils measured by bender element tests. Soils Found 51(4):737–747
Atkinson J (2007) Peak strength of overconsolidated clays. Géotechnique 57(2):127–135
Barton N (1976) The shear strength of rock and rock joints. Int J Rock Mech Min Sci Geomech Abst 13(9):255–279
Nielsen S, Spagnuolo E, Violay M, Smith S, Di Toro G, Bistacchi A (2016) G: Fracture energy, friction and dissipation in earthquakes. J Seismol 20(4):1187–1205
A. W. Skempton and D. J. Petley (1968). The strength along structural discontinuities in stiff clays. In: Proceedings of the geotechnical conference Oslo, 1967, vol 2. Norwegian Geotechnical Institute, pp 29–46
Dalguer L, Irikura K, Riera J (2003) Generation of new cracks accompanied by the dynamic shear rupture propagation of the 2000 Tottori (Japan) earthquake. Bull Seismol Soc Am 93(5):2236–2252
Pulido N, Kubo T (2004) Near-fault strong motion complexity of the 2000 Tottori earthquake (Japan) from a broadband source asperity model. Tectonophysics 390(1–4):177–192
Tinti E, Spudich P, Cocco M (2005) Earthquake fracture energy inferred from kinematic rupture models on extended faults. J Geophys Res Solid Earth 110(B12):1–25
Burjánek J, Zahradník J (2007) Dynamic stress field of a kinematic earthquake source model with k-squared slip distribution. Geophys J Int 171(3):1082–1097
Acknowledgements
The authors wish to thank the two anonymous reviewers for their insightful and constructive comments. Financial support for this work was provided by the Research Grants Council of Hong Kong through the Early Career Scheme (27205918), General Research Fund (17201419), and the NSFC/RGC Joint Research Scheme (N_CUHK430/16).
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Choo, J., Sohail, A., Fei, F. et al. Shear fracture energies of stiff clays and shales. Acta Geotech. 16, 2291–2299 (2021). https://doi.org/10.1007/s11440-021-01145-5
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DOI: https://doi.org/10.1007/s11440-021-01145-5