Skip to main content

Recent Developments in Instrumentation for X-Ray Microanalysis

  • Conference paper
Modern Developments and Applications in Microbeam Analysis

Part of the book series: Mikrochimica Acta Supplement ((MIKROCHIMICA,volume 15))

  • 509 Accesses

Abstract

This paper reviews the instrumentation advances for x-ray microanalysis 1991–1997, with particular emphasis on energy dispersive x-ray spectrometers. Most developments have been aimed at improved convenience and reliability while offering sensitivity well below 1 keV, particularly for semiconductor applications. Although EDX technology matured during the 1980’s, previous methods of characterisation are now inadequate to reveal the variability in performance as a function of x-ray energy in this low energy region. Furthermore, at low beam voltages where K lines are not excited, computer processing of peak overlaps is the only way to obtain element intensities. In this situation, detector and electronic stability and reproducibility have to be substantially improved in order to achieve results anywhere near the limit of statistical precision.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Subscribe and save

Springer+ Basic
$34.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or eBook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 84.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 109.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Similar content being viewed by others

References

  1. P. J. Statham, Inst. Phys. Conf. Ser. No. 119: Section 10, Proc. EM AG 91, IOP Publishing Ltd, 1991, 425

    Google Scholar 

  2. D. B. Williams, J. I. Goldstein, D. E. Newbury (eds.). X-Ray Spectrometry in Electron Beam Instruments, Plenum, NY, 1995.

    Google Scholar 

  3. P J. Statham, Microbeam Analysis-1988, San Francisco Press, CA, 1988 p., 429.

    Google Scholar 

  4. Tech. Data Sheet, Quantmap, Oxford Instruments, UK, 1995.

    Google Scholar 

  5. J. Friel, R. Mott, Scanning 1996, 18, 140.

    Google Scholar 

  6. P. J. Statham, Mikrochim. Acta 1996, [Suppl.] 13, 573.

    CAS  Google Scholar 

  7. R. Daniel, reporting ISIS-300/DXP50 performance at IUMAS-1, ACEM-14, 1996.

    Google Scholar 

  8. R. Daniel, Personal Communication, Oxford Instruments.

    Google Scholar 

  9. S. M. Zemyan, D. B. Williams, Microbeam Analysis-1991, San Francisco Press, CA, 1991, 134.

    Google Scholar 

  10. R. P. Kraft, D. N. Burrows, G. P. Garmire, J. A. Nousek, J. R. Janesick, P. N. Vu, Nucl. Instrum. Meth. 1995, A 361, 372.

    Article  CAS  Google Scholar 

  11. Microbeam Analysis-1995, VCH, NY, 1995, pp. 3–13.

    Google Scholar 

  12. P. J. Statham, Microbeam Analysis-1995, VCH, NY, USA, 1995, p. 187

    Google Scholar 

  13. E. Boyes, ICEM 13-Paris, Les editions de physique, 1994, p. 51.

    Google Scholar 

  14. C. E. Nockolds, Microbeam Analysis 1994, 3, 185.

    CAS  Google Scholar 

  15. M. W. Lund, in: X-Ray Spectrometry in Electron Beam Instruments, Plenum, NY 1995, 21.

    Google Scholar 

  16. D. E. Newbury, In: X-Ray Spectrometry in Electron Beam Instruments, Plenum NY, 1995, 167.

    Book  Google Scholar 

  17. J. J. McCarthy, In: X-Ray Spectrometry in Electron Beam Instruments, Plenum NY, 1995, p. 7.

    Google Scholar 

  18. R. B. Mott, J. J. Friel, in: X-Ray Spectrometry in Electron Beam Instruments, Plenum, NY, 1995, 127.

    Book  Google Scholar 

  19. P. J. Statham, X-Ray Spectrometry 1977, 6, 94.

    Article  CAS  Google Scholar 

  20. S. A. Audet, J. J. Friel, T. P. Gagliardi, R. B. Mott, J. I. Patel, C. G. Waldman, 1994 IEEE Nuclear Science Symposium, IEEE, NJ, 1994, p. 155.

    Google Scholar 

  21. P. J. Statham, In: X-Ray Spectrometry in Electron Beam Instruments, Plenum, NY, 1995, p. 101.

    Book  Google Scholar 

  22. D. A. Wollman, G. C. Hilton, K. D. Irwin, J. M. Martinis, Proc. Microscopy and Microanalysis 1996, San Francisco Press, 1996, p. 488.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1998 Springer-Verlag Wien

About this paper

Cite this paper

Statham, P.J. (1998). Recent Developments in Instrumentation for X-Ray Microanalysis. In: Love, G., Nicholson, W.A.P., Armigliato, A. (eds) Modern Developments and Applications in Microbeam Analysis. Mikrochimica Acta Supplement, vol 15. Springer, Vienna. https://doi.org/10.1007/978-3-7091-7506-4_1

Download citation

  • DOI: https://doi.org/10.1007/978-3-7091-7506-4_1

  • Publisher Name: Springer, Vienna

  • Print ISBN: 978-3-211-83106-9

  • Online ISBN: 978-3-7091-7506-4

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics