Abstract
Three stereoisomers (cone, partial cone, and 1,3-alternate) of p-tert-butylthiacalix[4]arene bearing four anchor propyltriethoxysilane substituents at the lower rim were synthesized for the first time. Surface modification of silica nanoparticles (d = 12 nm) with the synthesized macrocycles gave novel hybride thiacalix [4]arene‒SiO2 particles. The obtained nanostructured adsorbents were found to efficiently extract nitroaromatic compounds from aqueous solutions. The partial cone and 1,3-alternate thiacalix[4]arene–SiO2 hybrid particles showed affinity to nitrophenols.
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Dedicated to V. F. Mironov on His 60th Anniversary
Original Russian Text © R.V. Ziatdinova, N.A. Losev, I.S. Teren’tev, A.V. Gerasimov, L.S. Yakimova, V.G. Evtyugin, I.I. Stoikov, 2017, published in Zhurnal Obshchei Khimii, 2017, Vol. 87, No. 9, pp. 1487–1494.
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Ziatdinova, R.V., Losev, N.A., Teren’tev, I.S. et al. Modification of silica nanoparticles with stereisomers of p-tert-butylthiacalix[4]arene containing four 2-oxo-2-{[3-(triethoxysilyl)prop-1-yl]amino}ethoxy substituents at the lower rim. Russ J Gen Chem 87, 1969–1976 (2017). https://doi.org/10.1134/S1070363217090122
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DOI: https://doi.org/10.1134/S1070363217090122