Abstract
The main failure mechanism of brittle materials occurs through the initiation and propagation of cracks. Researches involved with various loading modes and material defects have been widely investigated to control the stability of subsurface crack. However, no detailed fracture mechanics analysis has been published to understand the direct effect of process parameters on crack growth. In this paper, taking the plastic deformation below the tool and the intrinsic line defect located at the plastic zone boundary into account, a mechanical and numerical study of the fracture mechanics is proposed from the perspective of process parameters in grinding of brittle materials. The stress intensity factors are computed in detail to analyze the various impacts of process parameters and tool geometry on the subsurface crack propagation. Results indicate that the main fracture mode for median crack induced in brittle material grinding is opening rather than shear. Although the residual stress caused by plastic zone plays an important role in fracture behavior, the effect of dislocations cannot be ignored as well. In addition, the starting point of opening fracture is also affected by grinding parameters and tool geometry. A small grinding speed, a sharp large tool, a large table speed and grinding depth will lead to strong anti-shielding effect on mode I crack propagation and strong shielding effect on mode II crack propagation. The results can be used to provide guidance for the development of controlled spalling technology which enables the reuse of cracking substrate.
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1 Introduction
Brittle materials such as silicon, ceramic and glass are the most employed materials utilized in the manufacturing of a vast majority of semiconductor products, optical instruments, biological materials and various other fields [1–4]. However, brittle materials are not amenable to machining process due to their low fracture toughness. When a brittle material is loaded to the limit of its strength, it tends to undergo cleavage-based fracture in a macroscale machining process and finally fails by the nucleation and propagation of a crack resulting in damaged and non-transparent machined surface [5]. These damages may seriously alter the surface properties and cause strength degradation or even a catastrophic failure of brittle materials [6]. As a consequence, the investigation of growth of surface and subsurface cracks plays an important role in the evaluation of the machining of brittle materials.
In fact, quite a few researches in crack propagation under different loading modes have been carried out. Early in 1964, Cook et al. [7] computed the stress distribution close to crack tip with a finite tip radius which could be opened by means of a remotely applied tension field or a concentrated force, etc. It is concluded that inside a brittle solid, if a plane of weakness or potential cleavage was present and was roughly normal to the plane of the original crack, this interface might break and produce a secondary crack in such a manner as to interfere with the progress of the primary crack. Hillberry et al. [8] described an idea on how to control the propagation of a crack in crystalline materials to produce thin wafers in their patent. Ewart and Suresh [9] studied the crack propagation in ceramics under cyclic loads. Xu and Needleman [10] numerically analyzed the dynamic crack growth in brittle solids with an initial central crack subjected to tensile loading. Gao et al. [11] studied the mechanisms of intersonic shear crack propagation along a weak interface under shear dominated loading by both molecular dynamics and continuum elastodynamics. Promising results were presented for the simulation of crack propagation in single crystals under monotonic loading by Aslan et al. [12]. Bouchard et al. [13] presented a mechanical and numerical study of the fracture process through a detailed analysis of stress intensity factors (SIFs). Influences of process variables on crack propagation direction were elucidated in their study. Yu et al. [14–16] investigated the dynamic responses and fracture behavior of various structural members under impulsive loading. Additionally, Comninou et al. [17, 18] have done many works on the propagation of subsurface crack subjected to surface force utilizing the distribution dislocation technique.
It has long been known that the presence of material defects such as impurities, vacancies, dislocations and microcracks can strongly influence the initiation and propagation of cracks [19–21]. In particular, the availability of dislocations in a material has a strong impact on fracture toughness. Lawn [22] mentioned that a propagating crack might activate pre-existing dislocation sources. Rice and Thomson [23] instituted a physical modeling to study the competition between dislocation emission and cleavage decohesion by comparing the load required to propagate a given crack with the load necessary to emit a dislocation on a slip plane inclined to the crack plane and intersecting the crack front. Renormalized molecular dynamics simulation of machining defect-free monocrystal silicon was carried out to investigate crack initiation process by Inamura et al. [24]. In their study, the generation of dislocation was observed and believed to play an important role in crack initiation process. Beltz et al. [25] and Fischer and Beltz [26] studied the role of crack blunting in the favorability of crack propagation versus dislocation emission using continuum concepts. The growth of a plane strain crack subjected to remote mode I cyclic loading under small-scale yielding was carried out by Deshpande et al. [27] and Clevering et al. [28] using discrete dislocation dynamics. Results showed that the resistance to crack growth tended to increase with an increasing density of dislocation sources. Investigations that aimed to describe the origin of fracture surface instabilities in brittle crystals containing intrinsic line defects in the form of dislocations were presented by Sherman et al. [29]. Sen et al. [30] reported an atomistic-level study of crack-tip cleavage to dislocation emission transition in silicon single crystals. Molecular dynamics simulations of crack propagation in the presence of defects in brittle crystalline materials under mode I loading were carried out by Petucci et al. [21]. Results indicated that the critical load was dependent on the defect species, geometry and position. Additionally, Zhou et al. [31–33] and Fang et al. [34–36] have done a great deal of successful works on the interaction between material defects and cracks as well. The solutions may have potentially significant application in addressing challenging material science, in particular their wear and contact fatigue analysis.
It is worth mentioning that observations of a small amount of plastic deformation in brittle materials have been reported in wear or abrasive machining studies [37–39]. As suggested by Lawn et al. [40], the subsurface cracks might also develop from the boundary zone between plastic and elastic deformation. Nakamura et al. [41] detected experimentally that the ductile–brittle transition point determined by subsurface cracks was shallower than that by surface cracks. Yan et al. [42] investigated the microscopic material removal mechanism of reaction-bonded silicon carbide through diamond turning experiments. Raman spectroscopy revealed that the ductile response of the workpiece material originated from the dislocation-based plasticity of 6H–SiC. Venkatachalam et al. [3] studied the transition undeformed chip thickness in micromachining of single-crystal brittle materials. In their research, the beginning of the formation and propagation of cracks were evaluated utilizing Irwin’s model which gave the relation between the stress intensity factor (SIF) and applied normal stress including effects of crack size and crack inclination. Wang et al. [43] studied the brittle–ductile transition mechanism involved in ultra-precision turning of silicon and pointed out that the deformation behavior of silicon under cutting force was an interaction between crack propagation and dislocation movement. Kharin et al. [44] developed an improved theoretical model of dislocational crack nucleation and growth in solids and analyzed the ductile/brittle behavior. In order to build up a fracture theory which describes the plastic deformation based on the behavior of various defects near the crack tip, the elastic interaction between defects and elliptical blunt cracks has prompted many investigations [45–47]. Recently, Fang and Zhang [48, 49] have established a new analytical model considering the phase transformation in determining the normal threshold load that caused the emission of partial dislocations in silicon during nanoindentation and nanoscratching.
As mentioned above, the main failure mechanism of brittle materials occurs through the creation and propagation of cracks. Researches involved with various loading modes and material defects have been widely investigated to control the crack stability. However, no detailed fracture mechanics analysis has been published to understand the direct effect of process parameters on crack propagation in brittle materials grinding. As a significance material that drives the semiconductor and information technology industries, there is no doubt that the failure components made of silicon has become an important issue [50, 51]. In this paper, a mechanical and numerical study of the fracture mechanics is presented from the perspective of process parameters in grinding of crystalline silicon. Stress fields caused by local plastic deformation and edge dislocation are both taken into account. The effects of different process parameters and tool geometry on crack propagation can be obtained rapidly through a detailed analysis of stress intensity factors.
2 Modeling
The physical problem to be investigated in the current work is depicted in Fig. 1. During brittle materials grinding, a plastic deformation zone with a depth d generates below the indenter. Generally speaking, the plastic zone is determined by material properties, normal force P and indenter geometry. While brittle mode serving as the dominant mode of material removal, median cracking which is considered as the main type of subsurface cracking nucleates and propagates downward along the load axis from the plastic deformation boundary. According to Fang and Zhang [48], we assume that an edge dislocation with Burgers vector \(\vec {b}\) is located at the plastic zone boundary in silicon substrate (\(b=a/{\sqrt{6}},\,a\) is the lattice parameter). The initial position and glide plane of edge dislocation are represented by \(\alpha _d \) and \(\beta \), respectively. The normal force P and the tangential force Q are imposed simultaneously on the specimen surface. Note that the edge dislocation can emit into the elastic matrix when the force acting on it reaches a critical value [36] and the median crack will be initiated only if the normal load is above a threshold value [52].
Various theoretical equations [53–55] have been proposed to evaluate the plastic zone size and subsurface crack, respectively. In the following study, we suppose that the median crack is well developed, that is to say, the median crack is larger than the plastic zone. Considering the threshold parameters (critical loading and its corresponding critical crack) obtained by Lawn and Evans [53], in brittle materials machining, the plastic zone and median crack are given as [56]:
where E is the Young’s modulus, H is the hardness, \(K_{c}\) is the fracture toughness, and \(\alpha _i \) is the half apex angle of indenter. The dimensionless factors \(\alpha \) and \(\eta \) are determined by indenter geometry, and the other two dimensionless terms \(\wp _e \left( \phi \right) \) and \(\wp _r \left( \phi \right) \) are dimensionless terms independent of the indenter/specimen system. The special values of indenter/specimen system parameters \(\chi _e \) and \(\chi _r \) for silicon have also been given by Lawn et al. [56] in their study as illustrated in Table 1.
Firstly, we consider the stress field induced in the material in the absence of the crack. Denote the normal and shear stresses along the line of the crack are \(\tilde{\sigma }_{yy} \) and \(\tilde{\sigma }_{xy} \), respectively, in the present case.
The stress components \(\sigma _{xy\_s} \) and \(\sigma _{yy\_s} \) caused by surface loading are written as [57]:
where \(\upsilon \) is the Poisson’s ratio.
The residual stresses \(\sigma _{xy\_r} \) and \(\sigma _{yy\_r} \) originated by the local inelastic deformation can be expressed as [58]:
The strength parameter \(F_r \) of residual stress field is determined by Jing et al. [55]
where f is the compaction factor (\({fE}/H=1.09\) for sharp indenter) and \(\lambda _r \) is a dimensionless parameter determined by indenter geometry (\(\lambda _r =1.25\) for a Berkovich indenter).
By utilizing the distributed dislocation technique [59], the stress fields \(\sigma _{xy\_d} \) and \(\sigma _{yy\_d} \) due to the edge dislocation at position \(\left( {x_0 ,y_0 } \right) \) with Burgers vector \(\vec {b}\) are given as:
where
For the convenience of writing, we set
It should be emphasized that four possible modes of response, i.e., open, closed and slipping forwards, closed and stuck, closed and slipping backwards, may well occur in combination for a given crack, sometimes at a given point in its history. The point \(\left( {x,0} \right) \) at crack line is expected to be closed when the stress component \(\tilde{\sigma }_{yy} \left( {x,0} \right) \) is compressive and only glide dislocations will be distributed along crack line. In contrast, the crack is expected to be open if \(\tilde{\sigma }_{yy} \left( {x,0} \right) \) is tensile. In this case, climb dislocations must be distributed along the crack line and glide dislocations should be distributed as well if \(\tilde{\sigma }_{xy} \left( {x,0} \right) \ne 0\). Therefore, in order to judge whether the median crack is open or closed in current state, influences of surface load on normal stress \(\tilde{\sigma }_{yy} \) and shear stress \(\tilde{\sigma }_{xy} \) along the imaginary crack line are shown in Fig. 2. Notice that both the plastic zone d and the median crack depth c changed with the normal force P, and therefore the horizontal axis in Fig. 2 has been replaced by a normalized position \({\left( {x_i -d} \right) }/{\left( {c-d} \right) }\) for comparison. In addition, the material and geometric parameters adapted in calculation are given in Table 1 [48, 53, 56].
It can be seen that if there is a lateral force (Fig. 2c, d) or not (Fig. 2a, b), the normal stress component is always positive which means the median crack is always open while the shear stress component is always negative. As a result, both climb dislocations and glide dislocations need distributing along the crack line. Besides, larger surface normal load corresponds to smaller normal stress and the tangential force can increase both the normal and shear stresses.
In the presence of median crack, the normal N(x) and shear S(x) tractions arising on the crack faces (\(y = 0\)) can be expressed as [59]:
The corrective solutions \(\bar{{\sigma }}_{xy} \left( {x,0} \right) \) and \(\bar{{\sigma }}_{yy} \left( {x,0} \right) \) due to the crack can be obtained as distributions of edge dislocations.
where \(K\left( {x,\xi } \right) =-\frac{1}{x+\xi }-\frac{2\xi }{\left( {x+\xi } \right) ^{2}}+\frac{4\xi ^{2}}{\left( {x+\xi } \right) ^{3}}\), \(B_x \left( \xi \right) \) and \(B_y \left( \xi \right) \) are the density of glide and climb dislocations at point \(\left( {\xi , 0} \right) \), respectively. The integration limits in Eqs. (14) and (15) are controlled by the plastic zone and the median crack depth depending on normal force P as expressed in Eqs. (1) and (2).
According to the definition of stress intensity factor, the Mode I and Mode II SIFs at crack tips D and C are
Substituting Eqs. (14), (15) into Eqs. (12), (13) yields
When the crack is open at all points, the requirement that the crack faces holds traction-free is
Then Eqs. (20), (21) can be rewritten as:
Notice that these two equations give rise to two uncoupled integral equations as for a crack normal to the surface of a half-plane.
In addition, due to the uniqueness of displacements, two further equations are needed to render the problem determinate.
3 Numerical solutions
As the presence of the Cauchy integral in Eqs. (23) and (24), firstly, the interval of integration \(\left( {d,c} \right) \) is normalized by the change of variables
where
Substituting Eqs. (27), (28) into Eqs. (23), (24) yields
where
and Eqs. (25), (26) can be rewritten as:
For handling singular integral equations with Cauchy kernels, we follow the widely used Gauss–Chebyshev numerical quadrature developed by Erdogan and Gupta [60]. Since both \(B_x \) and \(B_y \) are bounded functions, we set
where the unknown \(\varphi _x \left( r \right) \) and \(\varphi _y \left( r \right) \) in the expressions of dislocation density are some smooth regular functions.
In current case, both the crack tips are singular. The corresponding fundamental function \(w\left( r \right) \) has been given by Dundurs and Comninou [61].
Finally, the discrete forms of Eqs. (29) and (30) become
where
And the stress intensity factors at crack tips are directly related to the regular functions \(\varphi \left( r \right) \) at end points \(r=\pm 1\) which can be determined as:
The expressions of \(\varphi \left( {\pm 1} \right) \) are given as [59]:
where
Note that in the above equations, the negative sign refers to the shallower crack tip D, while the positive sign + refers to the deeper one C. Additionally, although the indexes for \(\varphi \left( {\pm 1} \right) \) on the right side of Eqs. (41) and (42) are impossible, these two vitally important values can be obtained by the discrete set of points \(r_i \) from Krenk’s interpolation formulae [62].
4 Results and discussion
The stress intensity factor can be used for determining whether the mode of material removal is plastic deformation or crack propagation along certain slip systems [2]. On the other hand, each machining method has its corresponding input parameters. For scratch test, the main input parameters are normal force P, lateral force Q and penetration depth h applied on indenter. Notice that there is no lateral force in indentation experiment. Therefore, the stress intensity factors at both the shallower and deeper median crack tip under scratch or indentation test can be directly obtained from Eqs. (40) and (41) based on the MATLAB procedure.
Figure 3 shows the variation of stress intensity factors at point C with different positions of edge dislocation located at plastic deformation boundary in the presence of lateral force. Results show that the main fracture mode is opening rather than shear as the mode I SIF is always positive, while the mode II SIF is always negative. By comparing the data in Fig. 3a, c, we also find that the mode I SIF is larger than the fracture toughness \(K_\mathrm{c}\) when \(P=100\,\hbox {mN}\) which means that a large surface normal load can promote the growth of type I cracking. However, it makes the occurrence of mode II crack difficult as depicted in Fig. 3b, d. Besides, each curve has a maximum value when the edge dislocation coincides with the start point of median crack \((\alpha _d =90^{\circ })\). In the following analyses, we take \(\alpha _d =36^{\circ }\) when the effect of edge dislocation is under consideration.
The influence of normal force on stress intensity factors at both the two crack tips are illustrated in Fig. 4. It is seen that, when the median crack is well developed, the mode I SIF at the shallower tip is always larger than the deeper one with a positive value whether there is a lateral force or not. It is worth mentioning that this result does not mean the propagation of shallower crack is easier. The reason is that the plastic zone expands with the increased surface normal load and finally engulfs the shallower crack tip as demonstrated in Eq. (1). In addition, the mode II SIFs are positive only when the lateral force is absent and two intersections occur when the normal force is close to 37.5 and 500 mN, respectively.
As the shallower crack tip will become engulfed with the increased normal force, we are more interested in the crack propagation behavior of the deeper one. By comparing the critical normal force when the fracture occurs with and without consideration of existence of tangential force Q (see Fig. 4b, a respectively), we find that the threshold in the absence of lateral force is much larger (350 mN) than that in the presence of lateral force (1.33 mN). It means that the residual stress caused by plastic zone plays an important role in fracture behavior. This is most probably because the residual stress induced by plastic deformation in the subsurface is tensile as mentioned in Chen et al. [63]. Moreover, the Mode II fracture toughness can be easily obtained according to Chang et al. [64], i.e., \(K_{\mathrm{IIC}} =\frac{\sqrt{3}}{2}K_{\mathrm{IC}} =0.52\). Therefore, we can conclude that the Mode II crack propagation never happens whether the tangential force exists or not from the stress intensity factor shown in Fig. 4c, d. In particular, the tangential force has a obvious shielding effect on Mode II crack growth.
It is generally known that dislocation pile-up or coalescence is one of the mechanisms leading to the crack nucleation. According to the typical crack systems in brittle materials machining mentioned by Chen et al. [6], the median crack is the main type of subsurface damages. However, the lateral crack also initiates at or close to the boundary of the plastic zone and spreads out laterally on a plane closely parallel to the machined surface. Therefore, in this paper, an edge dislocation with specified location as discussed by Fang et al. [48] has been introduced before the lateral crack formation to investigate the interaction between median crack and dislocation. Figure 5a shows the proportion of stress intensity factors caused by dislocation in the absence of lateral force. Result indicates that the normal force P has no effect on mode II SIF. As illustrated in Fig. 5b, the percentage of mode II SIF caused by tangential force is above 100 % after considering the present of lateral force. That is to say, the dislocation generates a positive mode II SIF, while the lateral force induces a negative one. The total mode II SIF is caused by the combination of dislocation and residual stress. The proportion of mode I SIF caused by residual stress is nearly 83 % as depicted in Fig. 5b which reconfirms again the dominant role of plastic zone in growth of subsurface crack. In addition, a single edge dislocation can bring about 3 % of mode I SIF when normal force is close to 10 mN (see Fig. 5a). According to Yan et al. [65], the dislocation density depends on the machining conditions such as cutting depth and tool rake angle. A high dislocation density may exhibit around the potential crack. Therefore, the effect of dislocations on fracture behavior cannot be ignored in machining of brittle crystal materials. In the future work, the interaction between lateral crack and median crack can be further studied by utilizing the distributed dislocation technique as well.
When a component is processed by grinding, the main input parameters become wheel speed \(V_s \), workpiece speed \(V_w \) and penetration depth h. As mentioned by Zhu et al. [66], median cracks could be effectively inhibited by moderate wheel speed. In order to quickly obtain the effect of various grinding parameters on subsurface crack propagation, we introduce the following equation established by Gu and Yao [67].
where \(\lambda _c =0.206{\left( {\mu H} \right) ^{1/3}}/{\left( {K_c \beta _c } \right) ^{2/3}}\left( {\cot \alpha _i } \right) ^{4/9}\left( {\tan \alpha _i } \right) ^{4/3}\), H is the hardness, \(K_c \) is the fracture toughness, and \(\beta _c \) is material parameter depended on elastic recovery.
The maximum penetration depth \(h_m \) was deduced by Shaw [68].
where \(r_c \) is the chip width-to-thickness ratio, A is the grain surface density (usually a large grain surface density corresponds to a small grit), \(a_p \) is the grinding depth, and \(d_e \) is the equivalent diameter of grinding wheel.
Then the median crack \(c_m \) can be expressed as a function of material properties, geometry of the abrasive grain and other grinding parameters by substituting Eqs. (45) into (44)
In the current situation, the normal grinding force P, the strength parameter of residual stress field \(F_{r}\) and the plastic zone size d can be rewritten as
Finally, the effects of grinding parameters and abrasive grain geometry on crack propagation can be obtained by substituting Eqs. (47), (48) and (49) into Eqs. (40), (41). For convenience, we introduce two dimensionless parameters, i.e., the speed ratio \(r_s \) and the dimension ratio \(r_d \).
As shown in Figs. 6 and 7, the mode I SIF at crack tip C is always positive, while the mode II SIF is always negative. The large speed ratio and dimension ratio correspond to a large magnitude of SIF, while the blunt and small grit corresponds to a small magnitude. Results indicate that a small grinding speed, a sharp large tool, a large table speed and grinding depth will lead to strong anti-shielding effect on mode I crack propagation and strong shielding effect on mode II crack propagation. As a main fracture mode in brittle crystal materials grinding, the starting point of opening fracture is also affected by grinding parameters and tool geometry.
It is worth mentioning that the branch fracture will occur under the mixed-mode I/II loading conditions. Li et al. [69] stated that the angle between branches of brittle fracture was between \(45^{\circ }\) and \(90^{\circ }\) in most papers. Kozhushko et al. [70] observed the fracture behavior of silicon with mixed-mode loading, an angle of \(\sim 70^{\circ }\) providing an example of crack bifurcation after nucleation. In the following analysis, the bifurcation angle \(\theta _\mathrm{b} \) is calculated as Eq. (51) according to Erdogan’s criterion mentioned by Chang et al. [64].
The effects of grinding speed, grinding depth and the apex of indenter on bifurcation angle are shown in Fig. 8. Results indicate that the large grinding depth and the large apex angel of indenter will increase the bifurcation angle, while the grinding depth has little effect on it. In particular, the calculated bifurcation angle is approximately between \(62.5^{\circ }\) and \(66.5^{\circ }\). Therefore, the result is within the acceptable range of values.
5 Conclusions
As one of the most significant properties of brittle materials, the estimation of subsurface crack propagation resistance in finish machining has been drawn much attention. However, controlling the crack stability is still a challenge. In this paper, the grinding of brittle materials with pre-existing subsurface crack is analyzed utilizing a numerical investigation of stress intensity factor (SIF) from the perspective of process parameters. Both the plastic deformation below the tool and the intrinsic line defect (dislocation) located at the plastic zone boundary in silicon substrate are taken into consideration. This analysis aims at understanding the influence of various grinding parameters and tool geometries on the growth of subsurface crack. The results can be used to provide guidance for the development of controlled spalling technology which enables the reuse of cracking substrate. The conclusions drawn from this study are:
-
1.
The main fracture mode for median crack induced in brittle material is opening rather than shear. A large compressive force perpendicular to surface will promote the growth of type I cracking and make the occurrence of mode II crack difficult. Comparing with the situation in the presence of lateral force, the threshold normal force of fracture occurrence is much larger when the lateral force is zero. It indicates that the residual stress caused by plastic zone plays an important role in fracture behavior.
-
2.
A single edge dislocation at plastic zone boundary can bring about 3 % of mode I SIF when normal force is close to 10 mN. Since a high dislocation density may exhibit around the potential crack, the effect of dislocations on fracture behavior cannot be ignored in machining of brittle crystal materials. In addition, the edge dislocation generates a positive mode II SIF, while the lateral force induces a negative one. The mode II SIF is totally caused by the combination of dislocation and residual stress.
-
3.
As a main fracture mode in brittle crystal materials grinding, the starting point of opening fracture is also affected by grinding parameters and tool geometry. A small grinding speed, a sharp large tool, a large table speed and grinding depth will lead to strong anti-shielding effect on mode I crack propagation and strong shielding effect on mode II crack propagation.
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Acknowledgments
The authors would like to deeply appreciate the support from the NNSFC (51601100, 11672141, 11572118 and 11402128), the Hunan Provincial Science Fund for Distinguished Young Scholars (2015JJ1006), the Fok Ying-Tong Education Foundation, China (141005), and K. C. Wong Magna Fund administered by Ningbo University.
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Chen, J., Fang, Q., Du, J. et al. Impact of process parameters on subsurface crack growth in brittle materials grinding. Arch Appl Mech 87, 201–217 (2017). https://doi.org/10.1007/s00419-016-1187-8
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DOI: https://doi.org/10.1007/s00419-016-1187-8