Abstract
Fe-based matrix segments were prepared by hot-pressing sintering with Fe powder and Sn powder. The microstructures of the sintered matrixes were analyzed by SEM, EDS and XRD. The effects of the composition ratio of Fe powder and Sn powder and sintering temperature on the microstructure were studied. The results show that the microstructure of FeSn matrix sintered at 620 ℃ is mainly composed of α-Fe and FeSn phase. There is no metallurgical bonding between the Fe powders, and the FeSn compounds in the matrix are mainly distributed along the interface between α-Fe. The microstructure of FeSn matrix sintered at 760 ℃ mainly contains α-Fe, (Fe, Sn) solid solution and Fe3Sn2 compound. Metallurgical bonding occurs between α-Fe phase. The increase of Sn content boosts metallurgical bonding between (Fe, Sn) solid solution. Fe3Sn2 compounds mainly distribute along the pores between Fe powders.
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References
Tyrala, D., Romanski, A., Konstanty, J.: The effects of powder composition on microstructure and properties of hot-pressed matrix materials for sintered diamond tools. J. Mater. Eng. Perform. 29(3), 1467–1472 (2019)
Mechnik, V.A., Bondarenko, N.A., Kolodnitskyi, V.M., Zakiev, V.I., Zakiev, I.M., Ignatovich, S.R., et al.: Formation of Fe-Cu-Ni-Sn-VN nanocrystalline matrix by vacuum hot pressing for diamond-containing composite. mechanical and tribological properties. J. Superh. Mater. 41(6), 388–401 (2019)
Bulut, B., Tazegul, O., Baydogan, M., Kayali, E.S.: Investigation and application of Fe–Co−Cu based diamond cutting tools with different bronze content used in marble production. In: Silva, Lucas F M. (ed.) Materials Design and Applications. ASM, vol. 65, pp. 307–314. Springer, Cham (2017). https://doi.org/10.1007/978-3-319-50784-2_23
Barbosa, A.P., Bobrovnitchii, G.S., Skyry, A.L., Guimars, R.S., Filgueira, M.: Structure, microstructure and mechanical properties of PM Fe-Cu-Co alloys. Mater. Des. 31(1), 522 (2010)
Wang, L., Pouchly, V., Maca, K., Shen, Z., Xiong, Y.: Intensive particle rearrangement in the early stage of spark plasma sintering process. J. Asian Ceramic Soc. 3(2), 183–187 (2015)
Azevedo, J., Serrenho, A.C., Allwood, J.M.: The deformation of metal powder particles: hardness and microstructure. Procedia Eng. 207, 1200–1205 (2017)
Schubert, W.D., Fugger, M., Wittmann, B., Useldinger, R.: Aspects of sintering of cemented carbides with fe-based binders. Int. J. Refract Metal Hard Mater. 49, 110–123 (2015)
Martin, W., David, L., John, Å., et al.: Diffusion modeling in cemented carbides: solubility assessment for Co, Fe and Ni binder systems. Int. J. Refrac. Metals Hard Mater. 68 (2017)
Li, B., Zheng, Z., Yu, H., Zeng, D.: Improved permeability of fe based amorphous magnetic powder cores by adding permalloy. J. Magnet. Magnet. Mater. 438, 138–143 (2017)
Acknowledgment
The authors gratefully acknowledge the financial support received from the Doctoral Foundation for Henan University of Engineering (No. DKJ2019024).
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Gao, Y., Zhang, J., Zhao, Q., Meng, Y., Li, L. (2022). Microstructure Analysis of Sintered Metal with Iron Powder and Tin Powder. In: Wang, Y., Martinsen, K., Yu, T., Wang, K. (eds) Advanced Manufacturing and Automation XI. IWAMA 2021. Lecture Notes in Electrical Engineering, vol 880. Springer, Singapore. https://doi.org/10.1007/978-981-19-0572-8_53
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DOI: https://doi.org/10.1007/978-981-19-0572-8_53
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