Abstract
The Silver nanoparticles with high stability and fine sizes were prepared by wet microwave irradiation with a mixture of silver nitrate, ethanol and a copolymer. The copolymer acts both as a stabilizer and a reducing agent. An observation followed by the effect of concentration on the physical properties of silver nanoparticles. The confirmation of the formation of the silver nanoparticles has been done by several analyzes such as UV - Vis spectra, scanning electron microscopy (SEM), Transmission Electron Microscopy (TEM), Energy Dispersive Spectroscopy (EDS) and X’Ray Diffraction (XRD). The range of 405–425 nm of the UV-Vis spectra of the surface plasmon resonances (SPR) are marked by the characteristic absorption band. When analyzing the SEM and TEM images, the silver nanoparticles were spherical shape and nanosize diameter of about 15 nm. An increase in gap energy was observed during the increase in concentration of silver nitrate.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Similar content being viewed by others
References
Warrier, P., Teja, A.: Effect of particle size on the thermal conductivity of nanofluids containing metallic nanoparticles. 6, 247 (2011)
Sondi, I., Salopek-Sondi, B.: Silver nanoparticles as antimicrobial agent: a case study on E. coli as a model for Gram-negative bacteria. 275, 177–182 (2004)
Schmid, G.: Chem. Rev. 92, 1709 (1992)
Bawendi, M.G., Steigerwald, M.L., Brus, L.E.: Annu. Rev. Phys. Chem. 41, 477 (1990)
Deheer, W.A.: Rev. Mod. Phys. 65, 611 (1993)
Jiang, H.Q., Manolache, S., Wong, A.C., Denes, F.S.: J. Appl. Polym. Sci. 93, 1411 (2004)
Joseph, S., Mathew, B.: J. Rec. Sci. Res. 3, 185 (2014)
Ider, M., Abderrafi, K., Eddahbi, A., Ouaskit, S., Kassiba, A.: Rapid synthesis of silver nanoparticles by microwave-polyol method with the assistance of latex copolymer. https://doi.org/10.1007/s10876-016-1096-6
Ider, M., Abderrafi, K., Eddahbi, A., Ouaskit, S., Kassiba, A.: Silver metallic nanoparticles with surface plasmon resonance: synthesis and characterizations
Tsuji, T., Iryo, K., Watanabe, N., Tsuji, M.: Appl. Surf. Sci. 85, 202 (2002)
Murphy, C., Jana, N.R.: Adv. Mater. 14, 80 (2002)
Wilson, O., Wilson, G.J., Mulvaney, P.: Adv. Mater. 14, 1000 (2002)
Ouaskit, S., Eddahbi, A., Moussetad, M., Adhiri, R., Ider, M., Abderrafi, K.: Procédé d’élaboration de nanoparticules métalliques dans une émulsion acqueuse de latex sous l’effet d’irradiation micro-ondes. Numéro de demande: PCT/MA2013/000036; Numéro de publication: WO 2014/088383 (12 Juin 2014)
Shipway, A.N., Lahav, M., Willner, I.: Adv. Mater. 12, 993 (2000)
El Moutarajji, A., Tbib, B., El-Hami, K.: Effect of Erbium addition on optical and electrical properties of polytetrafluoroethylene. https://doi.org/10.1007/978-3-030-12065-8_10
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2020 Springer Nature Switzerland AG
About this paper
Cite this paper
Moutarajji, A.E., Abdelhafid, A., El-Hami, K. (2020). Synthesis of Silver Nanoparticles by Microwave Irradiation and Their Effect on the Gap Energy of Nano-Composite Based on MWCNT. In: Ezziyyani, M. (eds) Advanced Intelligent Systems for Sustainable Development (AI2SD’2019). AI2SD 2019. Lecture Notes in Electrical Engineering, vol 624. Springer, Cham. https://doi.org/10.1007/978-3-030-36475-5_25
Download citation
DOI: https://doi.org/10.1007/978-3-030-36475-5_25
Published:
Publisher Name: Springer, Cham
Print ISBN: 978-3-030-36474-8
Online ISBN: 978-3-030-36475-5
eBook Packages: Intelligent Technologies and RoboticsIntelligent Technologies and Robotics (R0)