Abstract
CdO thin films on glass substrate were prepared by home built spray pyrolysis unit from aqueous solution of Cd(CH3COO)2·2H2O at different substrate temperatures. X-ray diffraction (XRD) studies indicate the formation of polycrystalline cubic CdO phase with preferential orientation along (111) plane. X-ray line broadening technique is adopted to study the effect of substrate temperature on microstructural parameters such as grain size and microstrain. Scanning electron microscopy (SEM) shows that the film prepared at 250°C consists of spherical shape grains with size in nanometer range and is comparable with the XRD studies.
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References
Chamberlin R R and Skarman J S 1966 J. Electrochem. Soc. 113 86
Chen C H, Kelder E M, Vander Put P J J M and Schoonman J 1996 J. Mat. Chem. 6 765
Chopra K L, Kainthla R C, Pandya D K and Thakoor A P 1982 Physics of thin films (New York and London: Academic Press) Vol. 12 167
Ghosh P K, Maity R and Chattopadhyay K K 2004 Sol. Energy Mat. Sol. Cells 81 279
Gurumurugan K, Mangalaraj and Narayandass S K 1994 Thin Solid Films 251 7
Hadouda H, Pouzet J, Bernede J C and Barreau A 1995 Mat. Chem. Phys. 42 291
JCPDS (Joint Committee on Powder Diffraction Standards — Data file: 05-0640)
Patil P S 1999 Mater. Chem. Phys. 59 185
Perednis D and Gauckler L J 2005 J. Electroceramics 14 103
Phatak G and Lal R 1994 Thin Solid Films 245 17
Sanatana G, Acevedo A M, Vigil O, Cruze F, Contreraspuente G and Vaillan L 1999 Phys. Rev. B60 9191
Sciti D, Celotti G, Pezzotti G and Guicciardi S 2007 Appl. Phys. A86 243
Su L M, Grote N and Schmitt F 1984 Electron. Lett. 20 716
Ueda N, Meada H, Hosono H and Kawazoe H 1998 J. Appl. Phys. 84 6174
Verkey A and Fort A F 1994 Thin Solid Films 239 211
Williamson G K and Hall W H 1953 Acta Metall. 1 22
Yan M, Lane M, Kannewurf C R and Chang R P H 2001 Appl. Phys. Lett. 78 2342
Zhao Z, Morel D L and Ferekides C S 2002 Thin Solid Films 413 203
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Jeyaprakash, B.G., Kesavan, K., Ashok Kumar, R. et al. Temperature dependent grain-size and microstrain of CdO thin films prepared by spray pyrolysis method. Bull Mater Sci 34, 601 (2011). https://doi.org/10.1007/s12034-011-0169-2
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DOI: https://doi.org/10.1007/s12034-011-0169-2