Abstract
The electrodeposited and the rolled 12 to 35 µm thick copper foils are subjected to the bending/unbending strain-controlled flex fatigue over a wide range of strain amplitudes. The fatigue life is associated with an increase in electrical resistance of the specimen beyond a preassigned threshold. For each foil type, in the rolled or as-deposited as well as in the (recrystallization-like) annealed conditions, the inverse Coffin-Manson (C-M) relationship between strain amplitude (Δε/2) and fatigue life (Nf) is established in the high Δε/2 (low Nf) and the low Δε/2 (high Nf) regimes. The Nf, Δε/2, and C-M slopes (c,b) are utilized to calculate the cyclic strain hardening (n′) and fatigue ductility (Df) parameters. It is shown that for a given foil thickness, an universal relationship exists between Df and the strength (σ) normalized fatigue life (Nf/σ). The propagation of fatigue crack through the foil thickness and across the sample width is related to the unique fine grain structure for each foil type: pancaked grains for the rolled foil and equiaxed grains for the electrodeposited foil. The fatal failure corresponds to convergence of the through-thickness and the across-the-width fatigue cracks. The variations in (i) electrical resistance, (ii) mid-thickness microhardness and grain structure and (iii) dislocation configurations with fatigue are monitored. Except for a small but significant fatigue induced softening (or hardening), no convincing evidence of strain localization (and the associated dislocation configurations generally observed for the bulk samples) has been found.
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Merchant, H.D., Minor, M.G. & Liu, Y.L. Mechanical fatigue of thin copper foil. J. Electron. Mater. 28, 998–1007 (1999). https://doi.org/10.1007/s11664-999-0176-x
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DOI: https://doi.org/10.1007/s11664-999-0176-x