Abstract
As an asymmetric organic molecular crystal, p-N,N-dimethylaminobenzaldehyde (DAB) exhibits peculiar optical property. It was first grown by solution technique adopting slow evaporation method at room temperature using CCl4 as growth medium. The solubility of DAB increases with temperature. Good quality transparent crystals of p-N,N-dimethylaminobenzaldehyde were carefully collected and subjected various characterization studies such as UV, FTIR, 1H and 13CNMR spectral studies and thermal (TG-DTG) studies to determine the purity and application oriented properties of the grown crystals.
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References
J. Williams (Ed), Nonlinear Optical Properties of Organic and Polymeric Materials, American Chemical Society Symposium Series 233, American Chemical Society, Washington, DC, 1983.
D. S. Chemla and J. Zyss (Eds), Nonlinear Optical Properties of Organic Molecules and Crystals, Vols 1 and 2, Academic Press. New York 1987.
P. Gunter, Ch. Bosshard, K. Sutter, H. Arend, G. Chapuis, R. J. Twieg and D. Dobrowolski, Appl. Phys. Lett., 50 (1987) 486.
K. Kagawa, M. Sagawa, A. Kakuta, M. Kaji, H. Nakayama and K. Ishii, J. Cryst. Growth, 139 (1994) 309.
D. Yuan, Z. Zhong, M. Liu. D. Xu, Q. Fang, Y. Bing, S. Sun and M. Jiang, J. Crystal Growth, 186 (1998) 240.
P. N. Prasad and D. J. Williams, Introduction to Nonlinear Optical Effects in Molecules and Polymers. Wiley, New York 1991.
J. P. Farges, Organic Conductors, Marcel Dekker, New York, 1994.
T. Ishiguro and K. Yamaji, Organic Superconductors, Springer, Berlin 1990.
Ch. Bosshard, K. Sutter, Ph. Pretre, J. Hulliger, M. Florshimer, P. Kaatz and P. Gunter, Organic Non Linear Optical Materials, Gordan and Breach, London, 1995.
L. Zhengdong, W. Baichange, S. Genbo and G. Huwnag, Appl. Phys. Lett., 70 (1997) 562.
M. M. Waldrop, Science, 250 (1993) 456.
G. Madhurambal and P. Anbusrinivasan, Cryst. Res. Technol., 41 (2006) 231.
P. Anbusrinivasan and S. Kavitha, Asian J. Chem., 20 (2008) 979.
G. Madhurambal, P. Ramasamy, P. Anbusrinivasan and S. C. Mojumdar, J. Therm. Anal. Cal., 86 (2006) 601.
P. Anbusrinivasan and M. Suganthi, Asian J. Chem., 20 (2008) 1775.
G. Madhurambal, P. Anbusrinivasan and S. C. Mojumdar, J. Therm. Anal. Cal., 90 (2007) 673.
G. Li, L. Xue, G. Su, Z. Li, X. Zhuang and Y. Ha, Cryst. Res. Technol., 40 (2005) 867.
S. C. Mojumdar, M. Melník and E. Jóna, J. Anal. Appl. Pyrolysis, 53 (2000) 149.
D. Czakis-Sulikowska, A. Czylkowska and A. Malinowska, J. Therm. Anal. Cal., 67 (2002) 667.
A. More, V. M. S. Verenkar and S. C. Mojumdar, J. Therm. Anal. Cal., 94 (2008) 63.
S. C. Mojumdar and L. Raki, J. Therm. Anal. Cal., 85 (2006) 99.
S. Y. Sawant, V. M. S. Verenkar and S. C. Mojumdar, J. Therm. Anal. Cal., 90 (2007) 669.
R. A. Porob, S. Z. Khan, S. C. Mojumdar and V. M. S. Verenkar, J. Therm. Anal. Cal., 86 (2006) 605.
S. C. Mojumdar, K. G. Varshney and A. Agrawal, Res. J. Chem. Environ., 10 (2006) 89.
M. Dovál’, M. Palou and S. C. Mojumdar, J. Therm. Anal. Cal., 86 (2006) 595.
K. G. Varshney, A. Agrawal and S. C. Mojumdar, J. Therm. Anal. Cal., 90 (2007) 721.
G. Madhurambal, P. Ramasamy, P. A. Srinivasan and S. C. Mojumdar, J. Therm. Anal. Cal., 90 (2007) 673.
K. G. Varshney, A. Agrawal and S. C. Mojumdar, J. Therm. Anal. Cal., 90 (2007) 731.
B. Borah and J. L. Wood, Can. J. Chem., 50 (1976) 2470.
S. C. Mojumdar, M. Sain, R. Prasad, L. Sun and J. E. S. Venart, J. Therm. Anal. Cal., 90 (2007) 653.
A. Ramadevi and K. Srinivasan, Res. J. Chem. Environ., 9 (2005) 54.
S. Meenakshisundaram, S. Parthiban, G. Madhurambal and S. C. Mojumdar, J. Therm. Anal. Cal., 94 (2008) 21.
J. S. Skoršepa, K. Györyová and M. Melník, J. Thermal Anal., 44 (1995) 169.
D. Ondrušová, E. Jóna and P. Šimon, J. Therm. Anal. Cal., 67 (2002) 147.
E. Jona, E. Rudinska, M. Sapietova, M. Pajtasova and D. Ondrušova, Res. J. Chem. Environ., 10 (2006) 31.
M. Kubranová, E. Jóna, E. Rudinská, K. Nemšeková, D. Ondrušová and M. Pajtášová, J. Therm. Anal. Cal., 74 (2003) 251.
E. Jóna, M. Hvastijová and J. Kohout, J. Thermal Anal., 41 (1994) 161.
D. Czakis-Sulikowska and A. Czylkowska, J. Therm. Anal. Cal., 71 (2003) 395.
R. K. Verma, L. Verma, M. Ranjan, B. P. Verma and S. C. Mojumdar, J. Therm. Anal. Cal., 94 (2008) 27.
G. Madhurambal, P. Ramasamy, P. Anbusrinivasan, G. Vasudevan, S. Kavitha and S. C. Mojumdar, J. Therm. Anal. Cal., 94 (2008) 59.
E. A. Ukraintseva, V. A. Logvinenko, D. V. Soldatov and T. A. Chingina, J. Therm. Anal. Cal., 75 (2004) 337.
S. C. Mojumdar, M. Melník and E. Jóna, J. Therm. Anal. Cal., 56 (1999) 541.
H. S. Rathore, G. Varshney, S. C. Mojumdar and M. T. Saleh, J. Therm. Anal. Cal., 90 (2007) 681.
S. C. Mojumdar, G. Madhurambal and M. T. Saleh, J. Therm. Anal. Cal., 81 (2005) 205.
K. G. Varshney, A. Agrawal and S. C. Mojumdar, J. Therm. Anal. Cal., 81 (2005) 183.
E. Jóna, E. Rudinská, M. Sapietová, M. Pajtášová, D. Ondrušová, V. Jorík and S. C. Mojumdar, Res. J. Chem. Environ., 9 (2005) 41.
S. C. Mojumdar, J. Mikloviš, A. Krutošíková, D. Valigura and J. M. Stewart, J. Therm. Anal. Cal., 81 (2005) 211.
S. C. Mojumdar, Res. J. Chem. Environ., 9 (2005) 23.
G. Madhurambal, S. C. Mojumdar, S. Hariharan and P. Ramasamy, J. Therm. Anal. Cal., 78 (2004) 125.
S. C. Mojumdar, J. Therm. Anal. Cal., 64 (2001) 629.
C. N. R. Rao, Ultraviolet and visible spectroscopy of organic compounds, Prentice Hall, New Delhi 1984.
P. Kalsi, Spectroscopy of Organic Compounds, Wiley, Eastern, New Delhi 1985.
W. Kemp, Organic Spectroscopy, 3rd Ed., W. H. Freeman, New York 1991.
R. M. Silverstein and Fx. Webster, Spectrometric identification of organic compound, 6th Ed., John Wiley and Sons, Inc., Canada 1998.
J. R. Dyer, Applications of absorption spectroscopy of organic compounds, Prentice, Hall of India (p), New Delhi 1987.
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Anbusrinivasan, P., Madhurambal, G. & Mojumdar, S.C. p-N,N-dimethylaminobenzaldehyde (DAB) grown by solution technique using CCl4 as growth medium. J Therm Anal Calorim 96, 111–115 (2009). https://doi.org/10.1007/s10973-008-9882-5
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DOI: https://doi.org/10.1007/s10973-008-9882-5