Abstract
The principal focus of this review will be to document and discuss the recent developments in the synthesis, properties and applications of polyorganosiloxane containing block, segmented and graft copolymers and network structures. Special emphasis will be given to the synthesis and characterization of reactive, organofunctionally-terminated siloxane oligomers, which are the key starting materials or intermediates in the preparation of these well-defined copolymers. Use of these functionally terminated oligomers in the modification of network structures will be discussed. Detailed descriptions of the copolymer formation reactions and the effect of reaction variables, such as temperature and solvent, on the properties of the resultant materials will be given. Discussions of the bulk and surface morphology of siloxane containing copolymers and their blends with other polymeric systems will be provided. Potential applications of these novel materials and possible future directions in the chemistry and technology of polyorganosiloxane containing polymeric systems will also be discussed.
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Abbreviations
- PDMS:
-
Polydimethylsiloxane
- PDPS:
-
Polydiphenylsiloxane
- D:
-
Dimethylsiloxane
- D3 :
-
Hexamethylcyclotrisiloxane
- D4 :
-
Octamethylcyclotetrasiloxane
- D″:
-
Diphenylsiloxane
- D″4 :
-
Octaphenylcyclotetrasiloxane
- M:
-
Trimethylsilicon
- F:
-
(1,1,1-trifluoropropyl,methyl)siloxane
- TMPS:
-
Tetramethyl-p-silphenylenesiloxane
- PSX:
-
Polysiloxane oligomer
- Mn:
-
Number average molecular weight
- Mw:
-
Weight average molecular weight
- MWD:
-
Molecular weight distribution
- Tg:
-
Glass transition temperature
- Tm:
-
Melting temperature
- Tc:
-
Crystallization temperature
- THF:
-
Tetrahydrofuran
- DMF:
-
N,N-Dimethylformamide
- DMAC:
-
N,N-Dimethylacetamide
- NMP:
-
1-Methyl-2-pyrrolidinone
- EEE:
-
2-Ethoxyethyl ether
- MEK:
-
Methyl ethyl ketone
- MMA:
-
Methyl methacrylate
- St:
-
Styrene
- MDI:
-
4,4′-Diphenylmethane diisocyanate
- TDI:
-
Tolylene diisocyanate
- HMDI:
-
Bis(4-isocyanatocyclohexyl)methane
- PMDA:
-
Pyromellitic dianhydride
- BTDA:
-
Benzophenonetetracarboxylicacid dianhydride
- ODA:
-
4-Aminophenyl ether
- DDS:
-
p-Aminophenyl sulfone
- Bis-A:
-
Bisphenol-A
- BPF:
-
Bisphenol fluorenone
- MDEA:
-
N-Methyldiethanolamine
- HEMA:
-
Hydroxyethyl methacrylate
- PACM:
-
Bis(4-aminocyclohexyl)methane
- AIBN:
-
Azobisisobutyronitrile
- PEO:
-
Poly(ethylene oxide)glycol
- PVC:
-
Poly(vinyl chloride)
- PMMA:
-
Poly(methyl methacrylate)
- PSF:
-
Polysulfone
- PS:
-
Polystyrene
- PC:
-
Bisphenol-A Polycarbonate
- PET:
-
Poly(ethylene terephthalate)
- RTV:
-
Room Temperature Vulcanization
- SIS:
-
Styrene-Isoprene-Styrene Triblock Copolymer
- SBS:
-
Styrene-Butadiene-Styrene Triblock Copolymer
- DP:
-
Degree of polymerization
- IPN:
-
Interpenetrating Network
- DSC:
-
Differential Scanning Calorimetry
- TMA:
-
Thermomechanical Analysis
- TGA:
-
Thermogravimetric Analysis
- DMA:
-
Dynamic Mechanical Analysis
- UV:
-
Ultraviolet Spectroscopy
- IR:
-
Infrared Spectroscopy
- 'H-NMR:
-
Proton Nuclear Magnetic Resonance Spectroscopy
- FT-IR:
-
Fourier Transform Infrared Spectroscopy
- DR:
-
Diffuse Reflectance
- ATR:
-
Attenuated Total Reflectance
- GPC:
-
Gel Permeation Chromatography
- VPO:
-
Vapor Pressure Osmometry
- ESCA:
-
Electron Spectroscopy for Chemical Analysis (also called XPS)
- XPS:
-
X-Ray Photoelectron Spectroscopy
- SEM:
-
Scanning Electron Microscopy
- TEM:
-
Transmission Electron Microscopy
- SAXS:
-
Small Angle X-Ray Scattering
- WAXS:
-
Wide Angle X-Ray Scattering
- SANS:
-
Small Angle Neutron Scattering
- E′:
-
Storage Modulus
- MPa:
-
Mega Pascal
- [η]:
-
Intrinsic Viscosity
- LEO:
-
Low Earth Orbit
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© 1988 Springer-Verlag
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Yilgör, İ., McGrath, J.E. (1988). Polysiloxane containing copolymers: A survey of recent developments. In: Polysiloxane Copolymers/Anionic Polymerization. Advances in Polymer Science, vol 86. Springer, Berlin, Heidelberg. https://doi.org/10.1007/BFb0025274
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DOI: https://doi.org/10.1007/BFb0025274
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Publisher Name: Springer, Berlin, Heidelberg
Print ISBN: 978-3-540-18506-2
Online ISBN: 978-3-540-47994-9
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