Summary
A new method is proposed for preparation of ap-tert-butyl-calix[4]arene-bonded silica stationary phase. The chemically modifiedp-tert-butyl-calix[4]arene is attached to silica gel via the silane coupling reagent γ-(ethylenediamino)-propyl-triethoxyl-silane. The bonded phase has been characterized by29Si and13C cross polarization/magic angle spinning solid-state nuclear magnetic spectrometry. The retention behavior of polycyclic aromatic hydrocarbons (PAHs), nucleosides and bases has been investigated on the bonded phase in the reversed-phase mode.
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Xiao, XZ., Feng, YQ., Da, SL. et al. Preparation and evaluation ofp-tert-butyl-calix[4]arene-bonded silica stationary phases for high performance liquid chromatography. Chromatographia 49, 643–648 (1999). https://doi.org/10.1007/BF02466906
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DOI: https://doi.org/10.1007/BF02466906