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Sulfur Amide Hydroxide Derivatives, N,N-Substituted Amino-organyloxy-sulfanes

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S Sulfur-Nitrogen Compounds

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Abstract

The compounds compiled in Table 64, p. 282, were prepared by the following methods: Method I: Reaction of CISNR2R3 with R1OM (M = H, Na, and Sn(C4H9-n)3)

a. For C2H5OSN(CH2)5:

A solution of CISN(CH2)5 and pyridine (mole ratio 1: 1) in petroleum ether is added dropwise to a solution of equimolar amounts of C2H2OH in petroleum ether cooled to 0 °C and stirred vigorously. The mixture is stored for 24 h at room temperature. Then, pyridine hydrochloride is filtered off, and the filtrate is washed with water and dried over CaCl2. The solvent is removed at 25 Torr, and the residue distilled [1].

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  1. Frankfurt am Main, Germany

    Alfons Kubny

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  1. Norbert Baumann
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  2. Hans-Jürgen Fachmann
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  3. Reimund Jotter
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Baumann, N., Fachmann, HJ., Jotter, R., Kubny, A. (1994). Sulfur Amide Hydroxide Derivatives, N,N-Substituted Amino-organyloxy-sulfanes. In: Baumann, N., Fachmann, HJ., Jotter, R., Kubny, A. (eds) S Sulfur-Nitrogen Compounds. Gmelin Handbook of Inorganic and Organometallic Chemistry / Gmelin Handbuch der Anorganischen Chemie, vol S / S-N / 10 / a. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-06351-4_13

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  • DOI: https://doi.org/10.1007/978-3-662-06351-4_13

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