Abstract
A series of poly(arylene ether nitrile) containing versatile carboxyl and sulfonic groups (CSPEN) were magnetically functionalized by ferroferric oxide (Fe3O4), and the obtained magnetic adsorbents (Fe3O4/CSPEN) were used to remove methylene blue (MB) dye from aqueous solution. The systematical characterizations that including scanning electron microscope (SEM), X-ray powder diffractometer (XRD), X-ray photoelectron spectroscopy (XPS), vibrating sample magnetometer (VSM), Fourier transform infrared (FTIR) certified that the Fe3O4/CSPEN possessed versatile functional groups and magnetic separation properties. The batch adsorption studies revealed that the Fe3O4/CSPEN not only displayed high selective adsorption ability for cationic MB in the presence of anionic MO, but also exhibited a removal efficiency as high as 98.2%. Besides, the adsorption kinetics and isotherm matched well with pseudo-second-order model and Langmuir model, respectively, and the maximum adsorption capacity of Fe3O4/CSPEN for MB was 92.029 mg/g. The FTIR and Brunauer-Emmett-Teller (BET) analyses confirmed that the outstanding adsorption capacity of Fe3O4/CSPEN was attributed to their own microporous structure and the electrostatic interaction with MB. Therefore, the modified magnetic adsorbent can be used to selectively remove cationic dye from aqueous solution.
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Acknowledgements
The authors gratefully acknowledge the Natural Science Foundation of Henan University of Technology (2020BS038) and Higher youth backbone teachers funded in colleges and universities of Henan province in 2019 (grant number 21220028).
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One-step solvothermal synthesis of poly(arylene ether nitrile) decorated magnetic composite for methylene blue adsorption from aqueous solution
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Zhou, X., Miao, W., Cheng, W. et al. One-step solvothermal synthesis of poly(arylene ether nitrile) decorated magnetic composite for methylene blue adsorption from aqueous solution. Korean J. Chem. Eng. 40, 1486–1496 (2023). https://doi.org/10.1007/s11814-022-1289-7
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DOI: https://doi.org/10.1007/s11814-022-1289-7