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Growth, investigation of calcium D-gluconate monohydrate-CDG crystals with shocked impact for electronic usage and the pure crystal for sensor application

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Abstract

The CDG – calcium D-Gluconate monohydrate is the orthorhombic type of crystalline specimen identified from single crystal XRD grown by slow evaporation methodology; the 2 MPa pressure with 2.2 Mach number of shock wave pulses with 864 K temperature of which three versatile categories of 50, 100, and 150 scalings are preceded with the CDG sample and are represented after applied shock wave pulses as CDG-50; CDG-100 and CDG-150. The single crystal XRD of pure CDG is 6.7123, 13.3648, and 19.5447 in Å for bond lengths and bond angles are 90° each with P212121 space group; orthorhombic system for CDG-50, CDG-100, and CDG-150 is 6.7167, 13.3747, and 19.5886, 6.7201, 13.3808, and 19.5898, and 6.7278, 13.3888, and 19.5977, respectively, and angles are same as 90°; and lengths are in Å units. The transparent nature of the materials of the CDG-50 is of 218 nm, the CDG-100 is of 221 nm cut-off wavelength, and finally the CDG-150 is of 220 nm wavelength. The corresponding photonic case of utilization is identified as 5.62 eV, 5.64 eV, and 5.68 eV, respectively, for CDG-50, CDG-100, and CDG-150. The fluorescence analysis of the all CDG shock pulsed samples having bandgap values pertaining to all CDG samples as 2.6956 eV, 2.8440 eV and 2.7312 eV, respectively, for bluish emission for all. The SEM of all samples is free from flaws and rod / bar-like pattern and thorny bar-like structures are observed. The CDG-50, CDG-100, and CDG-150 specimens are of negative photoconductivity type of classification. Dielectric characteristics are measured, and variations may be due to increased defects because of the high applied pressure by shock waves. The red LED with photodetector source for macro-scaled CDG’s sensor analysis is studied and reported.

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The data are fully used and presented here and there is no separate repository for data.

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Acknowledgements

The authors would like to thank St.Joseph’s College for the studies and IITM for crystal data and Phoenix Institute for electronic studies; Prof. Dr. S.A.M. Dhas, Sacred Heart College, for CDG sample’s pressurized provison; Dr Renganathan M of IIT-M for helping with Dr PB for pure sample’s sensor data analyzing.

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Authors and Affiliations

  1. Department of Electronics and Communication Engineering, AAA College of Engineering and Technology, Amathur, Sivakasi, Virudhunagar, Tamilnadu, 626005, India

    B. Padmanaban

  2. Department of EEE, E.G.S Pillay Engineering College (Autonomous), Nagapattinam, Tamilnadu, 611002, India

    V. Yokeswaran

  3. Department of Physics, Saveetha School of Engineering, SIMATS, Saveetha University, Chennai, Tamilnadu, 602105, India

    K. SenthilKannan

  4. Department of Chemistry, St.Joseph’s College of Engineering, OMR, Chennai, Tamilnadu, 600119, India

    V. Swarnalatha

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  1. B. Padmanaban
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Contributions

Padmanabhan.B—Photoconductivity, electronic, photonic work and sensor work. Yokeswaran.V—UV studies, electrical write-up. SenthilKannan.K*- synthesis, shocked impact and over all write-up and submission. Swarnalatha V—fluorescence, SEM work.

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Correspondence to K. SenthilKannan.

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The paper is not submitted priorly or simultaneously to anywhere and no part is presented or published and is the new / novel crystal data.

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Padmanaban, B., Yokeswaran, V., SenthilKannan, K. et al. Growth, investigation of calcium D-gluconate monohydrate-CDG crystals with shocked impact for electronic usage and the pure crystal for sensor application. J Mater Sci: Mater Electron 35, 832 (2024). https://doi.org/10.1007/s10854-024-12579-4

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