Abstract
The properties of a Diasorb-130-IDK sorbent based on silica gel with a grain size of about 6 µm were studied in order to choose conditions for the separation of the rare-earth elements from the samples of natural wine and their subsequent determination by inductively coupled plasma mass spectrometry. The possibility of the quantitative separation of the elements with the use of an ultrasonic flow suspension column was demonstrated. The results were compared with data obtained with the use of other sample preparation methods. A procedure was proposed for the determination of the rare-earth elements and yttrium in the samples of wines.
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Original Russian Text © R.Kh. Dzhenloda, V.M. Shkinev, T.V. Danilova, Z.A. Temerdashev, V.K. Karandashev, B.Ya. Spivakov, 2015, published in Zhurnal Analiticheskoi Khimii, 2015, Vol. 70, No. 12, pp. 1264–1270.
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Dzhenloda, R.K., Shkinev, V.M., Danilova, T.V. et al. Suspension columns with grain sorbents retained in an ultrasonic field for separation and determination of rare-earth elements in wines. J Anal Chem 70, 1456–1462 (2015). https://doi.org/10.1134/S1061934815120059
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DOI: https://doi.org/10.1134/S1061934815120059