Abstract
The residual stress creates deleterious effects on joint properties of dissimilar welding due to differential thermophysical properties and mechanical constraints of dissimilar thickness. Accounting of solid-state phase transformation (SSPT) through the understanding of solidification behavior enhances the prediction accuracy of residual stress. The characterization of microstructural features improves the fundamental understanding of the residual stress evaluation. An attempt is made to comprehend the dependence of heat input on phase transformation and its effect on the generation of compressive residual stress in dissimilar welding. Three distinct heat inputs of 52, 63, and 77 J/mm are considered in micro-plasma arc welding (µ-PAW) of SS316L and SS310 with thicknesses of 800 µm and 600 µm, respectively. The measurement of residual stress is performed using the X-ray diffraction (XRD) method. The variation of δferrite from 11.2 to 7.9% is analogous to the variation of average δferrite lath size from 412 to 1040 nm, where inter-dendritic spacing varies from ~ 10 µm to ~ 20 µm. The solidification mode is identified as ferritic-austenitic (FA), which results in the formation of skeletal and lathy δferrite structures. Electron Backscatter Diffraction (EBSD) results show an increase in heat input leads to an increase in low-angle grain boundaries that results in a rise in the residual stress value. The phase fraction and residual stresses are computed employing a finite element (FE) based thermal-metallurgical-mechanical (TMM) model including the effect of SSPT. The reasonable agreement between the computed and experimental measurements with a maximum error of ~ 8.5% in weld size, ~ 7.5% in peak temperature, ~ 16% in retained δferrite, ~ 17% in residual stress, and ~ 5% in distortion demonstrates the reliability of the developed model. A lower level of heat input (52 J/mm) allows the formation of a high amount of δferrite, which generates comparatively more compressive stress as a disparity in thermal expansion coefficient \({\mathrm{\alpha }}_{{\text{Ni}}}\sim 1.6 {\mathrm{\alpha }}_{{\text{Cr}}}\) aids in the reduction of residual stress.
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1 Introduction
Joining dissimilar grades of austenitic stainless steel (ASS) has found widespread application in the field of automobile, aerospace, medical, and power generation industries and pressurized water reactors [1, 2]. In particular, the SS300 series offers enhanced corrosion resistance and cryogenic properties due to the presence of high chromium and nickel percentages [3]. Dissimilar ASS joints are primarily recognized for their superior corrosion-resistant behavior, better strength at elevated temperatures, and excellent low-temperature fatigue properties. However, with low specific heat and thermal conductivity, high thermal expansion coefficients of ASS often exhibit inferior mechanical properties of welded joints owing to (a) the development of high residual stresses and structural deformation propensity and (b) ignorance of the role of microstructural attribute in residual stress evolution [4]. The accurate prediction of residual stress is always of great interest as it paves the road to eliminate or mitigate it.
The flexibility in power distribution to produce concentrated arc, µ-PAW is a potential candidate for welding dissimilar joints. However, the problem of residual stress arises from the non-uniform heat flux distribution, and it becomes more complex when the welded components have different coefficients of thermal expansion, thermal conductivity, severe variation in composition change, and different microstructures [5, 6]. Several researchers have made an effort to understand the mechanism for the development and mitigation of residual stresses in dissimilar welded joints [7,8,9]. Dawes [10] opined that because the grades of ASS expand 50% more than carbon steels and have poorer heat conductivity, they are more likely to bend and expand unevenly when combined. Usually, high magnitude of residual stress is localized in the heat-affected zone (HAZ) due to phase-change-induced expansion during cooling [11]. Akbari and Sattari-Far [12] showed that heat input mainly controls the level of residual stress in multipass dissimilar welding between stainless steel and carbon steel. The compressive stress in the stainless steel side reduces with a decrease in heat input. However, tensile stress in the stainless steel side reduces with a decrease in heat input. Maurya et al [13] depicted that excessive heat input caused residual stress to rise by 16 and 19%, respectively, in the longitudinal and transverse directions for dissimilar welding of Inconel and stainless steel. In all these cases, the effect of phase transformation was neglected.
The influence of heat input on microstructural evolution and phase transformation effect for similar and dissimilar ASS joints are well studied in the literature. Hsieh et al [14] studied the precipitation and strengthening behavior of dissimilar ASS joints and identified higher hardness values due to Cr-rich massive δferrite at solidified metal. The grain refinement of δferrite is enriched upon increasing the number of weld passes for dissimilar ASS joints [15]. Kianersi et al [16] observed three different morphologies of δferrite (skeletal, acicular, and lathy) in laser-welded ASS structures. The non-equilibrium phases evolved here due to the rapid cooling of welding processes. Relatively higher heat input or lower cooling rate exhibits coarsening of the ferritic-dendritic core and widening of inter-dendritic spacing, which resulted in dampening of tensile strength of welded joints. Harjo et al [17] reported that the compressive strain was generated in the ferrite phase, whereas the tensile strain appeared in the γaustenite matrix. Further, Thibault et al [18] observed compressive residual stress in the weld joint due to lowered martensitic transformation temperature of 13%Cr-4%Ni steel alloy. Hsieh et al [19] examined the propensity of tensile residual stress enhanced with enrichment of δferrite content of SS304. A feathery ferrite and compressive stress pattern are observed by Chen et al [20] in the hybrid laser-welding of ASS. However, the mechanism behind the development of stress was not elucidated adequately.
The chemical composition, cooling rate, and primary solidification mode rendered during welding are the main factors influencing the formation of δferrite. It is realized that the amount and distribution of δferrite in an ASS weldment is crucial since it determines the thermal stability, mechanical performance, and residual stress generation of the weld joint. The primary reason for the generation of residual stresses is linked with the solidification of the weld since the dilution occurs during liquid-to-solid phase transformation, and the solid-state phase transformation (SSPT) occurs after solidification with a differential cooling rate [21]. It is well known that residual stress tops the list in causing severe damage to a welded specimen [22,23,24]. Therefore, predicting, controlling, and finding ways to reduce stress developed in a welded structure remains the utmost priority.
Researchers have tried to predict residual stresses using experimental measurements aided by numerical models [25, 26]. Deng [27] showed the importance of martensitic transformation in the stress generated in medium carbon steel. The variation in the longitudinal stress value was minimized by considering the SSPT effect. Several researchers closely resembled the predicted value with the experimental results by incorporating SSPT [28,29,30]. Zubairuddin et al [28] reported drastic variation in predicting the value of transverse stress with (542 MPa) and without (635 MPa) consideration of the phase transformation effect in the 9Cr-1Mo steel joint. The authors suggested that austenite to martensite transformation accounts for a significant difference in the stress value. Hamelin et al [29] reported that high welding speed resulted in more martensite because of the high cooling rate. Even the prediction of residual stresses resembled the experimental data when phase transformation plasticity was implemented in the numerical model. Yaghi et al [30] reported a stress reversal from tensile to compressive in the fusion zone by including the effect of SSPT and TRIP in the case of P91 steel. Li et al [31] observed that consideration of SSPT accurately predicts the residual stress in dissimilar P22-SS304 joints. Kumar and Bag [32] predicted a low value (810 MPa) of longitudinal stress considering the phase transformation effect and minimum residual stress are observed under the least heat input (45 J/mm) characterized by high δferrite content, finer lath size, and lower inter-dendritic spacing [33]. Taraphdar et al [34] indicated that incorporating the SSPT effect provided significantly better correspondence with the measured value for longitudinal (~ 205 MPa) and transverse (~ 230 MPa) stress fields in the case of carbon steel. A similar observation is reported by Kubiak and Piekarska [35]. Mi et al [36] indicated that physical properties, volume change, and transformation-induced plastic strain are highly influential for reliable estimation of residual stress. Accounting both diffusive and displacive transformations in a TMM improves the welding distortion pattern. In fusion welding of ultra-high strengthened carbon steel, the microstructure consisting of bainite with a lower proportion of martensite also influences the residual stress evolution [37]. Considering the microstructural phenomena details and their kinetics during solidification improves the reliability of residual stress calculation.
The measurement of residual stress is one of the daunting tasks following any destructive and non-destructive techniques. Several researchers have developed contemporary novel techniques to enhance the accuracy of measurement of residual stress components [38,39,40]. Shen et al [38] determined surface residual stress based on spherical indentation. The localization of the largest pile-up around an indentation indicates the maximum residual stress. The particular link between pile-up after unloading and biaxial stress allows us to accurately detect the components of residual stress. Taraphdar et al [39] developed a flexible deep hole contour technique that does not need a complete section of the specimen and has the potential to measure through-thickness residual stress patterns with a relatively lower degree of damage of tested samples. Additionally, Elata et al [40] developed the residual stress measurement method following the electromechanical bifurcation response of a clamped–clamped beam. The presence of weld grooves significantly impacts on residual stress generation [41]. By accommodating the unequal V-groove pattern, the magnitude of residual stress components can be minimized near the root of the weld joint. An alternating weld pass sequence also dampens residual stress generation. However, the application of a single-directional weld pass sequence in an equal double-V groove configuration leads to the agglomeration of higher tensile residual stress [42]. Literature indicates that maintaining an optimum level of heat input governs the quality of weld joints and the presence of tensile residual stress tends to affect the fatigue strength of a weld joint. Thus, the likelihood of generating compressive stresses in the welded structure by considering the influence of microstructural transformation improves the joint quality [43, 44]. The summary of significant advancement in residual stress development in the fusion welding process is presented in Table 1.
It is obvious from the literature that thermal stability, mechanical features, and residual stress of dissimilar ASS welding are controlled by the distribution and quantity of δferrite at the fusion zone. Further, the estimation of residual stress in dissimilar austenitic steels is highly complicated where the solidification behavior and morphology are predominant. There is a significant lack of substantial work on dissimilar joints with the incorporation of SSPT is yet to be explored. Hence, the objective of the present study is to investigate the mitigation of residual stress by controlling microstructural morphologies that can elude the failures of a welded joint. Therefore, an attempt is made to understand the solidification behavior of the weld metal as well as its correlation with microstructural features and residual stress distribution. A sequentially coupled thermal-metallurgical-mechanical model (TMM) is developed and implemented using an in-house developed code through the subroutine of available commercial software. Further, numerically obtained residual stress values are validated with the experimentally measured data. The role of microstructure developed in dissimilar welding on residual stress generation is also established in the present work. An attempt is made to understand the dependence of cooling rate on phase transformation and its effect on the generation of compressive residual stress in dissimilar welding.
2 Experimental methodology
Thin steel sheets (SS316L and SS310) are autogenously joined using the µ-PAW process with 800 µm and 600 µm thicknesses, respectively. This welding process provides excellent joint characteristics at a relatively lower cost than laser and electron beam welding processes [45]. The elemental composition (Table 2) of the base metals SS316L and SS310 primarily comprises Cr and Ni with the inclusion of minor alloying elements (Si, Mn, Mo), and the rest Fe. The complete experimental setup and the feasible range of experimental data are presented elsewhere [46]. Figure 1a–d presents the process window for dissimilar weld joints. The different combinations of current (8–15 A) and speed (2.15–4.65 mm/s) lead to any of the following three weld conditions: (i) insufficient heating leads to no melting/no fusion, (ii) optimum/sufficient heat input corresponds to the formation of uniform weld bead with no visual imperfections, and (iii) overheating leads to burn through of the joints. The feasible het input range is identified as 52–77 J/mm, in which dissimilar joints produced are free from any visual imperfections such as undercut, cracking, underfill, and sagging. The plasma and shielding gas flow rates are 0.7 L/s and 7 L/s, respectively. The nozzle and electrode diameters used are 1.2 mm and 1.0 mm, respectively.
In the current examination, the effect of phase transformation on residual stresses is examined experimentally and numerically. From the feasible range, three parameters, 52 J/mm (L52), 63 J/mm (M63), and 77 J/mm (H77), are selected as the criteria of low, medium, and high heat input context. Further, samples extracted from the dissimilar joints are subjected to microscopic, elemental, electron backscatter diffraction (EBSD), and X-ray diffraction (XRD) analysis. Also, a coordinate measuring machine (CMM) is used to measure the longitudinal and out of the plane distortion for the dissimilar joints. The microscopic analysis is done using a field emission scanning electron microscope (FESEM) to identify the presence of lathy/skeletal ferrite in the austenitic matrix. The relative amount of δferrite in the austenite matrix is calculated. The elemental analysis helps to get an idea regarding the resulting composition of the different regions of the FZ, which aids in determining the concept of solidification mode by calculation of \({{\text{Cr}}}_{{\text{eq}}.}/{{\text{Ni}}}_{{\text{eq}}.}\) ratio using the Schaeffler diagram. Also, \({{\text{Cr}}}_{{\text{eq}}.}\) and \({{\text{Ni}}}_{{\text{eq}}.}\) is marked on the Fe–Ni-Cr ternary diagram (70 wt. % Fe). Further, EBSD analysis provides average grain size and misorientation angle distribution and allows an understanding of grain orientation in the FZ/HAZ. The measurement of residual stress (using XRD technique) at the surface of the weld joints is achieved by Bruker D8-Discover.™ system. Bragg's law is utilized to evaluate the magnitude of residual strain between atomic planes. Further, the value of stress is evaluated by the \({sin}^{2}\psi\) method, which relies on the variation of the peak location of the diffraction for different inclinations (tilt angle) of the sample [47]. The expression used for the calculation of stress by the \({sin}^{2}\psi\) method is given by [48]
where Y⟶ elastic modulus, \(\upsilon\) ⟶ Poisson’s ratio, \(\uppsi\) ⟶ angle between the bisector of the incident and diffracted rays, \({{\text{d}}}^{{\text{o}}}\)⟶ unstrained lattice spacing, and \({{\text{d}}}^{\uppsi }\)⟶ strained lattice spacing. The process condition for the measurement of stress by the XRD technique is represented in Table 3.
3 Theoretical background
A 3D FE-based TMM model is developed to predict the temperature distribution, distortion, and residual stresses in dissimilar joints. The convective and radiative heat transfer from the boundary, the temperature-dependent properties (Fig. 2), and the small deformation theory are considered for distortion evaluation. The influence of shielding gas on the top surface of the melt pool is neglected and presumed to be flat. The initial temperature is considered as 303 K (ambient conditions). The governing heat conduction equation [49] is depicted as
where \(\uprho\) indicates density, \({{\text{k}}}_{{\text{ij}}}\) refers to thermal conductivity, \({\dot{{\text{Q}}}}_{{\text{h}}}\) implies volumetric heat generation, \({{\text{C}}}_{{\text{p}}}\) implies specific heat, \({{\text{v}}}_{{\text{w}}}\) is the welding velocity vector, T stands for temperature, and t indicates time. For the thermal modeling, the heat transfer coefficient and emissivity are selected as available in the literature [49]. The volumetric heat source [49] and thermal boundary conditions [49] are used in the present investigation. The volumetric heat flux is expressed as
where \({p}_{d}\) is the power intensity factor, V is the welding voltage, \({\upeta }_{eff}\) is the efficiency of the µ-PAW process, \({w}_{c}\) is the welding current, \({r}_{eff}\) is the effective radius of the plasma arc, \(d\) is the depth of penetration, and \(h\) is the thickness. The initial temperature is considered as ambient temperature. The heat transfer on the surface during the welding process is expressed as
where \({q}_{sur}\) reflects the surface heat flux and it becomes zero to maintain an energy balance on the surface. It is to be noted that there is no input surface flux in the present case as a volumetric heat source term is included through the energy conservation equation. However, heat loss by convection and radiation is incorporated here. Tsur and Tin stand for surface and initial temperature, respectively. \(\upsigma\) and \(\upvarepsilon\) illustrate the Stefan-Boltzmann constant and emissivity of the base materials. The values of the heat transfer coefficient are 30 (SS316L) and 15 (SS310) on the top surface, and 1000 on the bottom surface (due to the highly conductive fixture, made of copper). The emissivity values are used as 0.7 for SS316L) and 0.75 for SS310.
The Schaeffler and pseudo-binary illustration of the Fe–Cr-Ni ternary system accurately depicts the phase transformation behavior of FZ evolved in the dissimilar joint under various process conditions. The material under investigation undergoes a eutectic reaction that produces liquid, γaustenite, and δferrite phases at temperatures between solidus (Tsolidus ~ 1648 K) and liquidus (Tliquidus ~ 1728 K). The present work does not consider the phase change dynamics from liquid to solid. The isopleth of the ternary Fe–Ni-Cr system (with 70 wt.% Fe) states that on the verge of SSPT, the austenitic steel comprises γaustenite and δferrite at Tsolidus. µ-PAW is categorized as a rapid cooling-assisted welding technique due to its highly collimated and coherent plasma arc. γaustenite (Ni) has a comparatively high solubility at elevated temperatures, while δferrite is extremely stable at high temperatures. The initial phase fractions of γaustenite and δferrite at solidus temperature are arbitrarily considered in the current work to be 4–5% and 94–95%, respectively [50]. It is assumed that the SSPT between δferrite → γaustenite adheres to the John-Mehl-Avrami-Kolmogorov (JMAK) equation [51], which is written as
where \({{\text{k}}}_{\updelta \to\upgamma }\) specifies the nucleation and growth rate, which primarily depends on temperature, and \({{{\text{f}}}^{\mathrm{^{\prime}}}}_{\upgamma }({{\text{T}}}_{({\text{t}})})\) represents the phase proportion of the austenitic phase at a temperature (T) and time (t). \({{\text{n}}}_{\updelta \to\upgamma }\) is the Avrami coefficient to account for the nucleation, followed by growth, and \({{{\text{f}}}_{\upgamma }}^{{\text{eq}}.}\) indicates the maximum value of the phase proportion of the γ-phase at the equilibrium stage. Further, \({{\text{T}}}_{\mathrm{\gamma s}}\) and \({{\text{T}}}_{\mathrm{\gamma f}}\) signify δferrite dissolution starts (1673 K) and finish temperature (1273 K), respectively. Based on the Temperature–Time-Transformation (TTT) diagram, the highest value of transformation is assumed to be 98%, and as a result, \({{\text{n}}}_{\updelta \to\upgamma }\) and \({{\text{k}}}_{\updelta \to\upgamma }\) are estimated as 2.65 and 0.01, respectively [52].
The aforementioned empirical relation is applicable only for calculating phase proportion growth about transformation under isothermal conditions. However, to account for non-isothermal characteristics, Scheil's additivity rule is used [52]. It signifies that the total amount of time needed to attain a specified fraction of a particular phase during continuous cooling is calculated by adding several incremental isothermal steps corresponding to instantaneous temperature changes. For the incorporation of the non-isothermal behavior of phase transformation, the term fictitious time (\({\tau }_{f}^{*}\)) is introduced. \({\tau }_{f}^{*}\) is the time required for the transformation to arbitrary volume fraction, i.e., \({{\text{f}}}_{\updelta \to {\text{s}}}\) at temperature \({{\text{T}}}_{{\text{o}}}\), considering an isothermal transformation at temperature \({{\text{T}}}_{{\text{o}}}+\Delta {\text{T}}\). Thus, \({\tau }_{f}^{*}\) [33, 53] is evaluated as
Using the Avrami model, the phase proportion at equilibrium for the transformation is displayed against temperature [51, 54] to determine the γ-phase proportion at equilibrium at a specific temperature \({T}_{t}\) and \({T}_{t+\Delta t}\). Thus, by using fictitious time, Eq. (5) is changed to
For mechanical analysis, the static equilibrium and thermo-elastic–plastic models are considered. The governing equation for static equilibrium condition [33, 53] is written as
where \({{\text{f}}}_{{\text{i}}}^{{\text{b}}}\) represents the body force vector and \({{\text{S}}}_{{\text{ij}}}\) is the Cauchy stress tensor. The stress tensor is symmetric by nature. The incremental nature of the elastic–plastic analysis is evident from the fact that total strain increment (\({\upvarepsilon }_{{\text{ij}}}^{{\text{total}}}\)) [55] is denoted as the sum of the strain components represented by
where the components of the elastic strain (\({\Delta \varepsilon }_{{\text{ij}}}^{{\text{e}}}\)), the thermal strain (\({\Delta \varepsilon }_{{\text{ij}}}^{{\text{thm}}}\)), the plastic strain (\({\Delta \varepsilon }_{{\text{ij}}}^{{\text{p}}}\)), and the phase transformation-induced strain (\({\Delta \varepsilon }_{{\text{ij}}}^{{\text{pt}}}\)) are all listed. However, strain accompanied by other factors, including TRIP, is ignored because it shows an insignificant effect on residual stress, particularly for stainless steel [56]. The present study incorporated yield stress and associated plastic strain as a function of temperature. The plasticity model adheres to the isotropic hardening, related rate-independent flow rule, and von Mises yield criterion. The thermal and mechanical boundary conditions are represented in Fig. 3 to simulate the clamping state used in welding. The thermal strain components are algebraically added to the volumetric expansion that takes place during instantaneous phase fraction evolution corresponding to SSPT. Overall strain is composed of a thermal and a phase-transition component [33, 53] and is represented as
where \({\varepsilon }^{\Delta {\text{vt}}}\) is the change in volumetric strain brought on by SSPT during the cooling stage, and \({\Delta \mathrm{f{\prime}}}_{\upgamma }\) is the instantaneous change in the phase fraction of the austenite phase. The expansion coefficient corresponding to SSPT is denoted by the symbol \({\mathrm{\alpha }}_{{\text{pt}}}\). The interaction of ferrite and austenite lattice characteristics is used to estimate the volumetric strain [33, 53], which is denoted as
where \({{\text{A}}}_{\mathrm{\delta {\prime}}}\) and \({{\text{A}}}_{\mathrm{\gamma {\prime}}}\) represent the lattice constant of \(\updelta\)- and \(\upgamma\)-phases, respectively. The \({{\text{A}}}_{\mathrm{\delta {\prime}}}\) and \({{\text{A}}}_{\mathrm{\gamma {\prime}}}\) [33, 53] are evaluated as
Equation (12) is implemented to approximate the temperature-related austenite’s lattice parameter, which is dependent on the percentage of carbon [57]. Carbon is a strong austenitic stabilizer and the lattice constant is highly influenced by its concentration. Overall, the volumetric strain component is used to alter the thermal strain component in structural analysis to account for the SSPT effect.
The development of a numerical model is accomplished using two separate phases. Phase I comprises of heat transfer model to extract temperature variation concerning time using the DFLUX subroutine in ABAQUS [32, 33]. Further, different temperature ranges are defined as \({\text{T}}\; < \;{\text{T}}_{{\text{solidus}}} ,\) \({\text{T}}_{{\text{solidus}}} \; \le \;{\text{T}}_{{\text{melting}}} ,\) \({\text{T}}\;{ > }\;{\text{T}}_{{\updelta } \to {\text{f}}} ,\) and \({\text{T}}_{\delta {\text{,f}}} \; \le \;{\text{T}}_{{\text{solidus}}} ,\) where \({\text{T}}\)⟶ desired temperature, \({\text{T}}_{{\text{solidus}}} \to\) solidus temperature, \({\text{T}}_{{\text{melting}}} \to\) melting temperature, \({\text{T}}_{\delta \to {\text{f}}}\) ⟶ ferrite finish temperature. The mentioned temperature ranges are stated under subroutine USDFLD as state-dependent [32, 33]. The \({\text{dT}}/{\text{dt}}\) is evaluated for the cooling phase for each node, and the node that complies with \({\text{dT}}/{\text{dt}}\) criteria and its peak temperature corresponds to the SSPT temperature scale. This satisfying criterion displays volumetric dilation and goes through phase transformation phenomena. The output of Phase I of the numerical simulation is used as input to Phase II, in which the UEXPAN subroutine is implemented to predict the time and temperature-dependent percentage growth of γaustenite/δferrite. After predicting the fraction of γaustenite/δferrite, \({\varepsilon }^{{\text{pt}}}\) is added to \({\varepsilon }^{{\text{thm}}}\). Further, the \({\varepsilon }^{{\text{t}}}\) is used to evaluate residual stresses in the dissimilar joints.
The validation of the finite element (FE) model is performed using experimental measurement of temperature history, weld macrograph, residual stress, distortion, and phase fraction. These are explained in the results and discussion section. However, the calibration of the FE model requires a lot of trials including the selection of elements, extent of solution geometry, and unknown properties like convective heat transfer coefficient and mesh size. Out of these, mesh size is more sensitive to the final results. Initially, all variables are fixed except mesh size and we set the calibrated model for thermal analysis. The calibration of the model is performed with experience and data from existing literature. Here, a trade-off between mesh size and computational time is maintained to reach the optimum mesh size, which is decided to reach a constant value of peak temperature at the center of the heat source for a particular mesh size. In the present case, a mesh size of 0.2 mm is used. The elements used for the thermal and metallurgical-mechanical analysis are DC3D8 (eight-noded diffusive heat transfer linear brick element) and C3D8R (brick element accompanied by reduced integration), respectively. The number of elements and nodes selected for the present analysis are 126,000 and 141,703, respectively.
4 Results and discussion
Figure 4a–d presents a comparison between experimentally obtained micrographs and numerically simulated thermographs for L52 and H77 process conditions. The temperature contour distinguishes the fusion, mushy, and HAZ. The FZ (orange contour) is identified by Tliquidus (1728 K), the mushy zone (red band) exists between Tliquidus and Tsolidus, and the HAZ is depicted by temperature below Tsolidus. The weld geometry shows neither crater defect at the weld top nor root sagging at the bottom/root of the weld. The reliability of the developed numerical model is verified by comparing the dimensions of the top (Wtop) and root (Wroot) portion of the FZ. Additionally, the peak temperature obtained during the simulation is validated with the measured values by a K-type thermocouple where the limits of the inaccuracy of the thermocouple are as per ASTM E230 standard [60]. The error for the Wtop and Wroot is evaluated as ~ 1.77% and ~ 8.51% for the L52 specimen, whereas ~ 2.46% and ~ 7.21%, respectively, for case H77.
Figure 4e,f compares the peak temperature for L52 and M63 conditions on either side of the dissimilar joints at a distance of 1.6 mm from the weld centerline. The error (absolute value) for the temperature data yields ~ 5.17%, ~ 5.28% (L52 condition), and ~ 7.43%, ~ 5.31% (M63 condition) on the SS316L and SS310 sides of the FZ. Figure 4g allows us to understand the variation of temperature at the top, middle, and root regions at the weld centerline for L52, M63, and H77 conditions. The peak temperature values extracted from the numerical model turn out as ~ 2032 K, ~ 2243 K, and ~ 2537 K for the cases L52, M63, and H77, respectively. It shows a rise in the value from L52 ⟶ M63 ⟶ H77, which is quite understandable due to the increasing amount of heat input. As the heat source moves away from a particular space, the value of peak temperature decreases. The maximum and minimum temperatures are seen at the Wtop and Wroot, respectively. As the heat source is in close contact at the top surface, the maximum temperature is seen at the Wtop, whereas the minimum temperature is observed at the Wroot, which is in contact with a highly conductive copper fixture. The time–temperature curve consists of two phases: heating and cooling. Once peak temperature is achieved, the heating phase is over, and the cooling phase begins. The cooling rate is evaluated by using the parameters \(G\) (temperature gradient) and \(R\) (growth rate). The value of \(G\) (K/mm) is extracted from the numerical model, and the value of \(R\) (mm/s) is substituted as the welding speed [61]. The value of the cooling rate \(\left(G \times R\right)\) is evaluated as 1063 K/s for L52, 832 K/s for M63, and 583 K/s for H77.
The microscopic images of FZ for the dissimilar joints at L52 conditions are depicted in Fig. 5a-f. Figure 5a,b depicts the fusion boundary and FZ at the two different interfaces near the SS310 and SS316L sides. Further, in the FZ due to variations in the local cooling rate, different microstructural morphology is observed. From the fusion boundary to the center of the FZ, the cooling rate decreases; accordingly, cellular, columnar, and equiaxed structures are observed in the different regions of the FZ. In Fig. 5c–f, different areas of the FZ are shown in magnified view for clear visibility of the microstructural evolution. An equiaxed structure is evident at the weld center, followed by a columnar, and cellular structure at the fusion boundary. The FZ comprises δferrite within the γaustenite region, and the presence of both δferrite and γaustenite (both phases) is related to the incomplete diffusional phase transformation of δferrite ⟶ γaustenite within the FZ. The specimen associated with the high heat input condition (H77) results in skeletal ferrite, whereas lathy δferrite is observed for the lowest heat input condition (L52). Different morphologies of the ferrite phase evolved due to the localized cooling rate variation in the solidified molten pool. Solidification of the melt pool governs the resulting metallurgical evolution in the dissimilar joints. To identify the mode of solidification and ferrite number in the joints, it becomes inherently necessary to calculate equivalent chromium \(\left({{\text{Cr}}}_{{\text{eq}}.}\right)\) and nickel equivalent \(\left({{\text{Ni}}}_{{\text{eq}}.}\right)\) content. An elemental analysis is carried out in the FZ, and the corresponding results are shown in Fig. 6a–c. The values of \({{\text{Cr}}}_{{\text{eq}}.}\) and \({{\text{Ni}}}_{{\text{eq}}.}\) are evaluated from the elemental analysis for L52, M63, and H77 conditions. The \({{\text{Cr}}}_{{\text{eq}}.}/{{\text{Ni}}}_{{\text{eq}}.}\) ratio corresponds to the mode of solidification as austenitic (A) < 1.37, austenitic–ferritic (AF) 1.37–1.5, ferritic–austenitic (FA) 1.5–2, and ferritic (F) > 2 [62]. The estimated \({{\text{Cr}}}_{{\text{eq}}.}/{{\text{Ni}}}_{{\text{eq}}.}\) ratio is evaluated as 1.77 for L52, 1.65 for M63, and 1.54 for H77, which is marked in the Schaeffler diagram to identify the ferrite no. and also highlighted in the pseudo phase diagram of ASS (Fig. 6d,e). Thus, from the obtained \({{\text{Cr}}}_{{\text{eq}}.}/{{\text{Ni}}}_{{\text{eq}}.}\) ratio, it is confirmed that the FZ of the dissimilar joints undergoes FA solidification mode for all three cases, leading to a dual-phase structure of ferrite (lathy) and austenite. Once the liquid melt pool starts to solidify, after 1728 K, the molten pool comprises liquid metal (L) and δferrite (δ). On reaching 1648 K, along with L and δ, it also shows γ-phase. On complete solidification, L completely transforms into δ and γ phases. After solidification, the retained δferrite ranges from 7 to 12% for the conditions L52, M63, and H77.
Figure 7a–c illustrates point, line, and area mapping analysis for selected regions in the FZ for sample L52. In Fig. 7a, point elemental analysis is carried out for two spectrums: the first point (spectrum 1) is selected inside the austenitic region, and the second (spectrum 5) is selected in the dendritic ferrite region. Ni is an austenitic stabilizer, and Cr is a ferritic stabilizer; therefore, the elemental analysis indicates the predominant variation of Cr and Ni in the austenitic and dendritic regions. The austenitic region shows higher Ni content, whereas the dendritic region shows higher Cr content. It is observed that phase transformation from δferrite ⟶ γaustenite relies on diffusion, with pct. of Cr increasing from ~ 19% (austenitic region) to ~ 25% (dendritic region), and pct. of Ni decreasing from ~ 14% (austenitic region) to ~ 9% (dendritic region). Figure 7b illustrates the line elemental analysis for a selected length of 100 µm, in which the variation of all the elements can be observed, especially Cr and Ni. A peak in the Cr line (pink color) can be observed as it crosses the dendritic region, whereas a peak in the Ni line (cyan color) can be seen as it passes through the austenitic matrix. Iron (Fe) is present in maximum pct.; thus, red (color) remains at the top. Figure 8a-b, e–f illustrates the base metals (BM) (SS310, SS316L), HAZ, FB, and FZ; Fig. 8c-d, g-h presents the line spectrum at the interface of the weld joints for a better understanding of the elemental diffusion across the FZ, HAZ, and BMs. The line spectrum shows consistency in the elemental analysis with no significant rise/sudden drop in the major elements like Fe, Cr, and Ni.
The elements Cr and Ni act as ferritic and austenitic stabilizers, respectively. An increase in Cr and a decrease in Ni content is related to the rejection of Cr and absorption of Ni in the austenitic region. Thus, complete transformation fails to occur during the solidification process at a high cooling rate. This incomplete transformation forces δferrite to be partially transformed into γaustenite. The complete physics of the process is explained in Fig. 9. The process starts with the equiaxed grain structure of the base metal (Fig. 9a). The process follows the heating, solidification, and cooling stages. Figure 9b illustrates solidification stages for L52 and H77 conditions, wherein FA solidification prevails. The solidification stages for L52 and H77 conditions can be stated as: \(L \to L+\delta \to L+\delta + \gamma \to \delta +\gamma\). During \(the L+\delta\) stage, a high cooling rate (1063 K/s) results in the formation of more amount of δferrite in the L52 condition compared to a low cooling rate (583 K/s) in the H77 condition. Just before Tsolidus, \(L+ \delta + \gamma\) a mixture exists together for a short-lived period. The formation of γaustenite results from the complete transformation of δ ⟶ γ. As shown in Fig. 9b, the transformation of δ ⟶ γ is caused by the combination of Cr in the dendritic region and the dissociation of Ni from the austenitic matrix. In the final stage, the temperature reaches from Tsolidus to Troom, which results in a microstructure comprising both phases (δ \(+\) γ). Here, the lathy and skeletal shape pattern δferrite is identified. Figure 9c shows the completely transformed austenitic matrix with enriched dendritic core ferrite boundary. Figure 9d illustrates the complete transformation (δ ⟶ γ) and the existing variation in the elemental composition of the dendritic core and austenitic region. Due to the presence of δferrite in the dendritic core region, the percentage of Cr is high, whereas in the austenitic region, Ni content is high.
The influence of heat input on microstructural morphology is observed in Fig. 10a–d. Irrespective of the heat input, lathy and skeletal shape pattern δferrite are identified. However, the relative amount of lathy δferrite is directly proportional to the cooling rate. In Fig. 10a,b, the lath size for the dendritic arms is shown in blue color, the δferrite is represented in maroon color arrows, and the γaustenite matrix is shown in yellow color arrows for L52 and H77. The figure also depicts inter-dendritic or primary dendritic arm spacing (PDAS) and secondary dendritic arm spacing (SDAS). Figure 10c depicts the FZ, fusion boundary, and the heat-affected region for the L52 condition; Fig. 10d shows the enlarged view in the FZ, wherein the presence of lathy δferrite can be observed. The measurement (average value) of δferrite lath size reveals 412 nm (L52), 723 nm (M63), and 1040 nm (H77). It is to be noted that the low heat input (high cooling rate) condition allows limited time for the overall growth of lath size, whereas high heat input allows sufficient time for the growth of dendrites; a similar trend has been reported earlier [63]. The inter-dendritic spacing (average) measures ~ 10 µm (L52), ~ 15 µm (M63), and ~ 20 µm (H77). It is to be noted that the value of inter-dendritic spacing also shows an increasing trend with an increase in heat input [64].
During the cooling phase, the initial phase fractions of γaustenite and δferrite at Tsolidus are arbitrarily considered as 4–5% and 94–95%, respectively [35]. During solidification, once the temperature falls below Tsolidus, unstable δferrite goes into the γaustenite matrix due to elemental diffusion, wherein the crystal structure changes from BCC (δferrite) to FCC (γaustenite). The BCC ⟶ FCC transformation corresponds to volumetric enlargement; thus, the proportion of ferrite decreases, and the amount of austenite increases. The complete phase transformation (δferrite ⟶ γaustenite) fails to occur below 1273 K (γ finish temperature), and some ferrite content is retained in the FZ, which remains as retained ferrite. Figure 11a-c illustrates the transformation of δferrite ⟶ γaustenite and retained ferrite concerning temperature and time. The slope of the phase diagram for the experimental and numerical conditions shows a considerable variation due to the high cooling rate achieved in the FZ. The percentage of retained ferrite using the numerical model is predicted as ~ 13.1% for L52, ~ 11.2% for M63, ~ 8.8% for H77, and the remaining fraction comprises an austenite matrix in the FZ. Figure 11d shows a quite satisfactory comparison between numerical results and the data determined from the Seferian relation [50].
Figure 12 depicts the FESEM spectrum of the solidified weld zone along with calculated δferrite volume fraction at three different heat inputs. A Gaussian blur is applied before applying a manual threshold to determine the volume pct. of the δferrite phase. This comprises converting an unprocessed image (RGB) to a greyscale (8-bit) image, which is then thresholded to generate a binary (black and white) image. Accordingly, the δferrite is identified as white-branched skeletons in the black region (matrix), as depicted in Fig. 12b. The fraction measurements are performed using the standard manual point count method [65], in which a grid of points is superimposed on the microstructural images illustrated after thresholding using ImageJ software. The ratio of the total number of points occurring in the phase that is of interest to the total available number of grid points is obtained, and this ratio yields the estimated statistical value of the phase in volume fraction. The dual-phase microstructure clarifies the incomplete phase transformation from δferrite to γaustenite. Figure 12c, d displays dampening of skeletal-structured δferrite phase fraction from 11.2% → 7.9% upon increasing heat input from 52 → 77 J/mm. Higher heat input provides the platform for the dissolution of δferrite into the γaustenite matrix, which leads to the diffusional transformation of δferrite → γaustenite. The error in the numerically predicted values of δferrite concerning experimental values is evaluated as ~ 16% for L52, ~ 15% for M63, and ~ 11% for H77 process conditions.
Figure 13a illustrates the XRD pattern of the FZ, and the intensity counts are depicted in Fig. 13b. The planes (111), (200), (220), and (222) represent γaustenite peaks, and the plane (110) corresponds to δferrite peak. Intensity counts (intensity peak) directly relate to the quantity of phases available in the inspected region [66]. The intensity counts of the γ (111), γ (200), γ (220), γ (222), and δ (110) show a decreasing trend as the heat input increases. The decreasing intensity of the γ-phase is related to incomplete transformation (δferrite ⟶ γaustenite), which is elaborated under the mode of solidification section in Fig. 9. The case of δ (110) also shows a decreasing trend with increasing heat input. The highest count is observed for the case L52 (~ 1063 K/s). The time availability for conversion of δferrite ⟶ γaustenite is less for a high cooling rate and hence, the amount of δferrite enhances with an increase in the cooling rate [33].
EBSD analysis for the base metals and the FZ at different process conditions is conducted, and the variation of grain size with inverse pole figure (IPF) maps is depicted in Fig. 14. The IPF maps of the base metals are depicted in Fig. 14a. It provides the grain size variation throughout the area fraction, from 1.39 µm to 37.06 µm for SS316L and from 1.39 µm to 45.89 µm for SS310. The average grain size for the base metals is 7.42 µm for SS316L and 9.63 µm for SS310. Figure 14b depicts the fluctuation in grain size with heat input, where a rise in heat input results in increased grain size. An increase in heat input leads to a slower cooling rate, which provides more time for the grains to grow. The increase in grain size can be observed from the IPF maps, where the grain diameter varies from 3.55 µm to 211.71 µm for L52, 2.87 µm to 247.22 µm for M63, 5.65 µm to 426.27 µm for H77. The average grain size is evaluated as 28.68 µm for L52, 42.57 µm for M63, and 58.53 µm for H77. Figure 14b also illustrates the IPF maps for all three cases, L52, M63, and H77. Further, the enlarged view of IPF maps for L52, M63, and H77 conditions is shown in Fig. 14c–e. Figure 14f,g denotes the misorientation angle and the frequency with which it occurs. It enables us to understand the presence of low-angle grain boundaries (LAGBs, \({2}^{^\circ }<\uptheta < {15}^{^\circ }\)), and high-angle grain boundaries (HAGBs, \({15}^{^\circ }<\uptheta < {65}^{^\circ }\)) [67]. The LAGB and HAGB are relatively similar for the base materials, whereas LAGB and HAGB vary with heat input. The pct. of LAGBs increased (23.64 ⟶ 38.16 ⟶ 48.99%), and HAGBs decreased (76.36 ⟶ 61.48 ⟶ 51.01%) with an increase in the heat input value. Thus, it can be concluded that an increase in heat input value leads to a decrease in HAGBs. The relative decrease in HAGBs or increase in LAGBs results from a high cooling rate. As the solidification rate decreases, the FZ is in a state of extreme non-equilibrium, corresponding to the formation of high-density LAGBs [68, 69]. Also, fatigue resistance positively correlates with residual stress value; in other words, low-density LAGBs lead to a lower value of stresses developed [70, 71].
The estimated residual stress obtained from the numerical results is validated with the experimental values, and a comparison is made in Fig. 15a,b at three heat input conditions. The longitudinal component (S11) of residual stresses against the distance across the weld cross-section is presented in Fig. 15a. The numerically calculated S11 stress values are 212, 239 and 280 MPa, where the pct. error in predicting the S11 stress value is evaluated as ~ 17% for L52, ~ 11% for M63, and ~ 15% for H77 process conditions. As the heat input increases from L52 to H77, a high rise of 147.3 MPa is observed because high heat input (H77) leads to more melting of the base materials, leading to larger contraction, and higher values of residual stresses. In contrast, low heat input corresponds to lower melting of the base materials, which confines the FZ to a narrower region, thus leading to a lower value of residual stress. The S11 stress changes from positive (tensile) at the weld center line and nearby location to negative (compressive) at a faraway location i.e., at a distance of ~ 5 mm from the weld center line for the L52 condition. As the heat source moves away, the heated region starts to cool down and regain its length, wherein positive (tensile) stresses are developed [72]. The maximum magnitude of the longitudinal stress field (S11) is measured as ~ 181 \(\pm\) 38 MPa at the fusion line, whereas it is obtained as ~ 266 \(\pm\) 34 MPa and ~ 328 \(\pm\) 20 MPa for specimens M63 and H77, respectively. The localization in the distribution of tensile residual stress is also seen by a highly collimated micro-plasma beam, which resulted in a relatively low cooling rate and less temperature gradient at distant locations across the weld region for the lowest heat input condition (L52). The maximum compressive residual stress (S11) of 88 \(\pm\) 30 MPa (SS310 side) and 94 \(\pm\) 33 MPa (SS316L side) at location ~ 11 mm is seen for case L52; however, it is measured as 144 \(\pm\) 35 MPa (SS316L side) and 122 \(\pm\) 34 MPa (SS310 side) for M63 sample and 165 \(\pm\) 34 MPa (SS310 side) and 183 \(\pm\) 28 MPa (SS316L side) for case H77. The tensile stress at the nearby location of the weld region is compromised by successive compressive stress at a distant location to maintain the neutrality of the structural stress field or to accommodate structural equilibrium. Figure 15b illustrates the comparison in the residual stress values along the transverse direction (perpendicular to the weld direction, S22). The S22 stress (transverse) value is relatively smaller than the S11 component. The S22 stress values also show a similar trend as S11 stress, wherein, residual stresses also increase with the increase in the heat input value. The value of S22 stress is experimentally determined as \(-\) 19.5 \(\pm\) 10 MPa, 67.3 \(\pm\) 23 MPa, and 124.6 \(\pm\) 32 MPa for L52, M63, and H77 conditions, respectively. The S22 stress value primarily relies on the size of the FZ, i.e., a smaller width of the FZ achieved under low heat input conditions lowers the stress value alongside changing the nature of stress [73]. The S22 value for L52 changes its value from negative (compressive) at the weld center line to zero at the outer edges. The highest value of S11 (328.6 \(\pm\) 20 MPa) and S22 (124.6 \(\pm\) 32 MPa) stress components correspond to the maximum heat input condition (H77), whereas the minimum heat input condition (L52) results in relatively low stress (S11 and S22) value.
The FZ for the L52 condition comprises 11.2% δferrite and 88.8% γ-austenite, and for the H77 condition comprises 7.9% δferrite and 92.1% γaustenite. Figure 15c presents the stress generation in the γaustenite region and δferrite core regions in a tabular format. The presence of higher δferrite involves more amount of Cr and less Ni content. Also, it is to be noted that the austenitic matrix comprises higher Cr and less Ni content, whereas δferrite contains higher Ni and less Cr content, and the coefficient of thermal expansion \((\alpha\)), for Ni is ~ 1.6 times that of Cr [33, 74]. Due to the difference in the value of \(\alpha\), the γ-region (containing more amount of Ni) contracts more as compared to the δ-region (containing more amount of Cr), which corresponds to compressive stresses in the dendritic core region and tensile stresses in the γ-region. Figure 15d illustrates the tensile and compressive stress behavior associated with the γ-region and δferrite core region, respectively. The reduction of tensile stresses in the FZ for L52 and M63 conditions is observed. Under the high heat input condition (H77), lower δferrite content restricts compressive stresses in the FZ. Also, the deformation of δferrite is restricted by the surrounding hard phase austenite, which restricts the development of back stress due to δferrite, thus resulting in a lower stress level for L52 than the H77 condition. It suggests that residual stress distribution is changing mostly due to volumetric changes during phase transition, which might greatly reduce the cumulative longitudinal stress. Hence, an increase in lath size (412 nm for L52 to 1040 nm for H77) and an increase in inter-dendritic spacing (10 µm for L52 to 20 µm for H77) also aid in the overall enhancement of the value of locked-in stress. Figure 15e shows the inter-relationship between δferrite lath size and retained δferrite on the resulting S11 stress value. It is observed that a lower value of lath size (412 nm) and higher retained δferrite pct. (11.2%) leads to a minimum S11 value (181.3 \(\pm\) 38 MPa). Overall, a low heat input value, higher retained δferrite, fine lath size, and reduced inter-dendritic spacing lead to minimum residual stress value [6, 10].
Figure 16 represents the longitudinal (S11) stress for L52, M63, and H77 conditions. The presence of tensile stress near the weld region for all the cases is obvious. Further, to maintain structural equilibrium, the tensile (positive) nature of the stress changes to compressive (negative) for the region away from the FZ. The maximum value of residual stress for L52 and M63 cases is identified as 235.7 and 269.7 MPa, respectively, which falls within the yield strength value of the base metals (277 MPa for SS310 [75] and 376 MPa for SS316L [76]). In contrast, the value of residual stress is estimated as 315.7 MPa for the H77 condition, which is on the higher side with reference to the base material SS310. It indicates a severe chance of structural failure on the SS310 side.
The effect of phase transformation is also observed in the resulting distortion value of the steel joints. To evaluate the influence of phase transformation, the distortion value is analyzed for dissimilar joints fabricated at maximum heat input conditions (H77). Figure 17a-b illustrates distortion along the weld direction and out-of-the-plane distortion for the H77 condition. An outward convex-type shape along the weld (longitudinal, Ux) direction indicates that the maximum deflection occurs near the center, and the minimum deflection occurs at the edges. The maximum deflection (Ux) with and without consideration of phase transformation is measured as 1.17 and 1.54 mm, respectively. The experimental value determined from the CMM is 1.23 mm. Thus, the error in predicting Ux for the H77 process condition is evaluated as ~ 5% and ~ 25% with and without consideration of phase transformation, respectively. The significant error of Ux implies that the incorporation of phase transformation immensely aids in accurately predicting the value of distortion. Notably, the value of Ux is found to be highest for the H77 process condition. The probable reason for such a scenario is the involvement of a high amount of plastic strain induced in the joints. Figure 17b illustrates the out-of-the-plane distortion (Uz) for specimen H77, wherein the maximum deflection occurs near the edges of the sheets, and the minimum deflection at the weld center. The maximum value of the deflection with and without phase transformation is identified as 0.008 and 0.00654 mm, respectively. The experimental data is measured as 0.0068 mm, and the corresponding error in predicting the value of Uz is evaluated as ~ 4% and ~ 17% with and without phase transformation, respectively. Similar to Ux, it is observed that the value of Uz is found to be highest for the high heat input process condition (H77). Figure 17c-f represents the comparison between the transverse deflection (Uy) and out-of-plane distortion (Uz) distortion contour of the H77 sample. It is observed that the magnitude of Uy is maximum without consideration of the phase transformation effect, and the value of Uy is lowered with consideration of the phase transformation effect. The out-of-the-plane distortion is shown in Fig. 17d,f, where the deflection is the highest at the edges, and reduces with consideration of the phase transformation effect. The incorporation of phase transformation prevents overestimation of stress value due to consideration of compressive stresses created by δferrite enriched core. Similarly, a reduction in deflection value is observed due to partial cancelation of deflection in Ux and Uz directions. A similar trend is reported in the martensitic transformation of medium carbon steel, resulting in a considerable reduction in distortion with the incorporation of the phase transformation effect [27].
The microstructural features, residual stress, distortion, and temperature variation in dissimilar welding of steels using µ-PAW are discussed in this section. The summary of the comparative results between experiments and numerical calculation is presented in Table 4. The complete details of the quantitative results of the input parameter (heat input) and the corresponding output results (cooling rate, peak temperature, \({{\text{Cr}}}_{{\text{eq}}.}/{\mathrm{ Ni}}_{{\text{eq}}.}\) ratio, lath size, PDAS, weld dimensions, retained δferrite percentage, grain misorientation, longitudinal residual stress, and distortion) are presented here.
5 Conclusions
The current investigation is carried out to identify the influence of SSPT on residual stress developed for dissimilar joints formed by the µ-PAW welding process. Experimental and numerical analysis is carried out to predict mainly the retained δferrite and residual stress generated in the dissimilar joints. The conclusive statements derived from the present work are as follows.
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The evaluated \({{\text{Cr}}}_{{\text{eq}}.}/{{\text{Ni}}}_{{\text{eq}}.}\) ratio ranges from 1.54 to 1.77, which suggests FA mode of solidification exists, where the FZ consists of δferrite (skeletal and lathy) within the austenitic matrix.
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The retained δferrite decreases (11.2 ⟶ 9.7 ⟶ 7.9%) with an increase in heat input (52 ⟶ 63 ⟶ 77 J/mm). The predicted values of δferrite show a maximum error of ~ 16%. Further, a reduction in the peak intensity obtained from the XRD pattern confirms a decrease in δferrite amount, when the heat input enhances.
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An increase in heat input is analogous to the reduction in cooling rate (1063 ⟶ 832 ⟶ 583 K/s) that allows the growth of δferrite lath (412 ⟶ 723 ⟶ 1040 nm) and enhances the inter-dendritic gap (10 ⟶ 15 ⟶ 20 µm).
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The difference in the magnitude of the thermal expansion coefficient (\({\mathrm{\alpha }}_{{\text{Ni}}}\sim 1.6 {\mathrm{\alpha }}_{{\text{Cr}}}\)) corresponds to tensile residual stress in the γ-region (where Ni % is high) and compressive stress in the dendritic core (where Cr % is high). A low heat input condition (52 J/mm, highest retained δferrite) generates comparatively more compressive stress than high heat input conditions (63 and 77 J/mm).
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The deflection in the resulting dissimilar joints shows significant error (Ux ~ 25% and Uz ~ 17%) without consideration of the phase transformation effect and it is only Ux ~ 5% and Uz ~ 4% including the effect of the SSPT effect.
It is summarized that a successful joining of dissimilar materials can be achieved by using a minimum amount of heat input analogous to high δferrite content, relatively finer lath size, and minimum gap between dendritic arms. The combination of such characteristics of δferrite aids in reducing the residual stress generated.
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Acknowledgements
The authors gratefully acknowledge the NECBH and DBT (IIT Guwahati), Govt. of India, for the project no. BT/COE/34/SP28408/2018 for the FESEM instrumentation facility.
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Dwibedi, S., Kumar, B. & Bag, S. Phase transformation effect on residual stress development in fusion welding of dissimilar stainless steels with different thickness. Arch. Civ. Mech. Eng. 24, 148 (2024). https://doi.org/10.1007/s43452-024-00958-x
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DOI: https://doi.org/10.1007/s43452-024-00958-x