1 Introduction

Earlier attempts to develop AFNOR 15CDV6 steel was launched in France. The letters C, D and V denotes carbon, molybdenum and vanadium. As the alloying elements remain less than 5% in proportion by weight, the steel fits into the category of low alloy steel [1, 2].15CDV6 is a low carbon bainitic steel with high strength, toughness and ductility which finds growing popularity in the fields of aerospace, defence and power generation industries and it is specially used in making rocket motor hardware in the Indian Space Program [3, 4]. Despite the other uses, 15CDV6 steel finds its application in making parts of jet engines, nuclear reactor, pressure vessels, and rocket motor casings [5]. The microstructure of 15CDV6 steel in hardened and tempered condition is composed of predominantly lower bainite and a small proportion of lath martensite. [2]. 15CDV6 steel acquires its strength from hardening at 975 ± 5 °C followed by forced air quenching and tempering at 640 ± 5 °C. Generally, hardening and tempering enables in increasing the strength of steel. The fine dispersion of alloy carbides has a major impact in strengthening of the steel. By increasing the tempering temperature and holding time, there is a decrease in the strength and hardness, and at the same time increases the ductility of the material [3]. The properties of steel has been increased through electro slag refining (ESR) process, resulting in sharp increase in ductility and toughness but rather gradual increase in strength [6]. In order to increase the strength of the steel, the proportion of martensite has to be increased to 0.75 in a mixed microstructure of martensite and bainite. This can also be achieved by addition of alloying elements which slows down the bainite reaction. Hence increasing the content of chromium from 1.5 to 4%, increases the strength of the steel, thus helping in the retardation of bainite reaction [4, 7].

The other way to increase the strength is by raising heterogeneous nucleation during solidification by inoculation technique which refines the grain size thereby enhancing the strength [8]. Any manufacturing capability need to be proved through suitable application of any material. In this case, welding capability is demonstrated through the 15CDV6, the most used metal joining process. 15CDV6 has good weldability and ease of fabrication [3, 4]. Chandrasekhar et al. [9] studied electron beam welding and TIG welding, the commonly used welding processes for fabrication using 15CDV6 steel. Ramesh et al. [3] in their work, depicted the parent materials with heat treatment followed by laser beam welding and studied the microstructural evaluation in different regions of the welds. Optimization of the welding process parameters depends upon the ability to measure and control the process variables involved in the welding process. The major contributing parameters of gas tungsten arc welding (GTAW) process are current, voltage, travel speed and gas flow rate. Among the various optimization techniques, grey relational analysis (GRA) and TOPSIS have earned the market due to their multi criteria decision making approaches. This means that GRA and TOPSIS are simple and effective tools to solve the multiple objective problems. GRA and TOPSIS are techniques of multi objective optimization which solves by converting the multi objective function into a single objective function. Deepan Bharathi Kannan et al. [10] in their work successfully used GRA technique in finding the optimized welding parameters in Laser joining of NiTinol shape memory alloy. Seyed Mostafa Mirhedayatian et al. [11] used a combination of data envelopment analysis (DEA) and TOPSIS for the selection of welding process parameters for repairing nodular cast iron engine block. The combination of these two techniques not only enables in optimizing the welding parameters but also extends to varied fields of manufacturing. Muthuramalingam and Mohan [12] successfully used GRA for Multi objective optimization of electrical process parameters in electrical discharge machining. Durairaj et al. [13] successfully used Grey Relational Theory to optimize the cutting parameters in wire EDM for SS304. Lan et al. [14] used TOPSIS in selecting the optimized parameters in CNC turning process.

From literatures, it is understood that welding of 15CDV6 using GTA welding process produces weldments with better properties than the base material which leads to failure at the base material region during tensile testing. In order to homogenize the base metal and weldment region, heat treatment is mandatory. Hence, the workpiece after welding is to be subjected to heat treatment and Post weld heat treated coupon properties should be further used for analysis.

It is also understood from the literatures that only fewer research has been emphasised on welding of 15CDV6 and no such publications related to optimization of the welding parameters using GRA and TOPSIS techniques exist. Hence, this research puts an effort to weld 15CDV6 using GTA welding process and optimize the welding parameters using GRA and TOPSIS techniques.

2 Materials and Methods

The plate with dimensions 300 × 150 × 3.7 mm was used for welding. The chemical composition of the base metal is given in Table 1 and the mechanical properties in annealed conditions are given in Table 2. 8CD12 filler wire was used in GTAW of 15CDV6 steel. In order to minimize the formation of Vanadium Carbide, the usage of filler wire as Vanadium was barred. The Chemical composition in filler wire is given in Table 1. The specifications for TIG welding process are given in Table 3.

Table 1 Chemical composition (wt %) of materials (Nominal)
Table 2 Base Material Mechanical Properties (annealed) [15]
Table 3 Machine specifications of GTAW power source

Taguchi provided an efficient method to find the optimal combination of input parameters. This method used the orthogonal array of experiments to reduce the number of experiments. L9 orthogonal array was used in the present work. The levels for the input parameters are given in Table 4.

Table 4 Welding parameters and their levels

Table 5 Shows the L9 orthogonal array experimental run along with output responses [bead width (BW), reinforcement (R), tensile strength (TS), hardness (Hv) and depth of penetration (DoP)] measured after post weld heat treatment.

Table 5 L9 Orthogonal array with input parameters and output responses

The weld joint configuration is shown Fig. 1.

Fig. 1
figure 1

Weld joint configuration

After welding, the samples were subjected to heat treatment as per heat treatment cycle shown in Table 6. They were sliced to the required size for analyzing. The samples were then etched with Nital (5% nitric acid). Optical microscopy was used to characterize the various regions of weldments. Micro hardness evaluation was carried out at regular intervals (2 mm) across the weldments at a load of 500 g. The test specimens were made by water jet cutting and the mechanical properties were evaluated at room temperature as per ASTM E-8 specification. The heat input was calculated using the following equation

$$Heat\,input\,\left( {HI} \right) = \frac{\eta \times I \times V \times 60}{S}$$
(1)

where η = arc efficiency, I = current in A, V = voltage in V, S = travel speed in mm/min.

Table 6 Heat treatment cycle

3 Results and Discussions

3.1 Grey Relational Approach (GRA)

GRA is a multi-objective optimization technique that converts multi response into single objective problem. GRA has been developed by Deng in 1982, to analyze the uncertainties in systems and relations between systems. The overall performance of experimental trial depends on grey relational grade. The higher grey relational grade attributes to optimal solution.

It can be used to find correlation among sequences with less number of data and also examines several aspects. In this method all the performance characteristics are converted into a single grey relational grade.

Conversion of the various responses into a single grey relational grade is carried out via the following stages.

3.1.1 Stage 1

Grey relational approach has been employed to analyse the obtained results by using signal-to-noise (S/N) ratio. The signal-to-noise (S/N) ratio is a measure of how much useful information is there in a system or process, as a proportion of the entire content. These (S/N) ratios are calculated for all the output responses based on Eqs. (2) and (3). These ratios can be categorized into three types namely: Smaller is Better (SB), Larger is Better (LB) and Nominal is a Better (NB).

In GTAW welding process, in order to achieve increase in the tensile strength, hardness and depth of penetration of the weldments, ‘Larger is Better’ option has been used. Whereas the responses bead width and reinforcement are expected to be of minimum value and hence ‘Smaller is Better’ option has been used for bead width and reinforcement. The values are calculated using the following results.

  1. 1.

    Larger-the-Better

    $$S/N\;ratio = - 10\log \left( {\frac{1}{n}} \right)\sum\limits_{i = 1}^{n} {1/y_{ij}^{2} }$$
    (2)
  2. 2.

    Smaller-the-Better

    $$S/N\;ratio = - 10\log \left( {\frac{1}{n}} \right)\sum\limits_{i = 1}^{n} {y_{ij}^{2} }$$
    (3)

where, n is the number of replications for each experiment, Yij are the response values.

3.1.2 Stage 2

The S/N ratios obtained from the Eqs. (2) and (3) have been normalized using the following relations.

  1. 1.

    Larger-the-Better

    $$N_{i}^{*} (k) = \frac{{y_{i} (k) - min\,y_{i} (k)}}{{max\,y_{i} (k) - min\,y_{i} (k)}}$$
    (4)
  2. 2.

    Smaller-the-Better

    $$N_{i}^{*} (k) = \frac{{max\,y_{i} (k) - y_{i} (k)}}{{max\,y_{i} (k) - min\,y_{i} (k)}}$$
    (5)

where i = 1, …, m, k = 1, 2, 3, …, n, m = no. of trial data, n = no. of factors, yi(k) = original sequence, \({\text{N}}_{\text{i}}^{*} \left( {\text{k}} \right)\) value after GRG, Min yi(k) and max yi(k) are the minimum and maximum value of yi(k) respectively.

The Normalized values for the output responses are given in the Table 7.

Table 7 The normalized values for the output responses

3.1.3 Stage 3

Grey relation coefficient (GRC) has been calculated to identify the relationship between the ideal and actual normalized experimental results. The computation of GRC is done with the help of equation.

$$\epsilon_{i} (k) = \frac{\Delta \hbox{min} + \tau \Delta \max}{{\Delta_{oi} (k) + \tau \Delta \max}}$$
(6)

where \(\epsilon_{i} (k)\) is the GRC, \(\Delta_{oi}\) is deviation among \({\text{N}}_{\text{o}}^{*} ( {\text{k)}}\) and \({\text{N}}_{\text{i}}^{*} ( {\text{k)}}\), \({\text{N}}_{\text{o}}^{*} ( {\text{k)}}\) = ideal (reference) sequence, \(\Delta \hbox{max}\) = highest value of \(\Delta_{oi} (k)\), \(\Delta \hbox{min}\) = least value of \(\Delta_{oi} (k)\), τ is assumed to be 0.5 in this case (distinguishing coefficient).

3.1.4 Stage 4

After averaging the grey relational coefficients, the grey relational grade (GRG) has been calculated using the formula:

$$GRG = \left( {\frac{1}{m}} \right)\sum {\epsilon_{i} (k)}$$
(7)

where m is the number of response variables.

The high value of grey relational grade indicates the stronger relational degree between ideal sequence and present sequence. The ideal sequence is the best response in the machining process. Higher grey relational grade indicates closeness to the optimal response in the process.

3.1.5 Stage 5

The grey relational grade values are then ranked in order. The rank of each trial has been tabulated in Table 8.

Table 8 GRC, GRG and rank for all the output responses for 15CDV6 steel

From the ranking it is seen that experimental trial 8 shows the highest GRG value in Taguchi’s L9 experimentation. But in order to get the best optimal set of parameters, it is necessary to draw the response table. The response table for the various parameters along with their optimal levels is shown in Table 9. From the response table it can be observed that current was having the maximum range (Max–min) indicating that current is the most influential parameter on the overall objective function followed by shielding gas flow rate, travel speed and voltage.

Table 9 Response table for average grey relational grade

From the response table it is seen that the optimized set of parameters fits outside Taguchi’s L9 experimentation. It is observed that level 3 in current, level 1 in voltage, level 2 in travel speed and level 3 in gas flow rate form the optimized set of input parameters.

3.2 Analysis of Variance (ANOVA)

Analysis of variance (ANOVA) is conducted to determine the significance level of each input parameters affecting the multiple responses of GTAW. ANOVA is constructed using the GRG values from GRA and it is shown in Table 10. The influence of each input parameter thus on the responses is graphically shown in Fig. 2.

Table 10 Analysis of variance (ANOVA) using GRG values in GRA
Fig. 2
figure 2

The influence of input parameters on the output responses in GRA

Here the error value has become zero, hence pooled error method has been followed to calculate the parameter influence. The two parameters with least sum of squares have been added and it is used as error value and the calculations are done using MINITAB software.

From ANOVA it can be concluded that current is the most influential parameter followed by gas flow rate, travel speed and voltage taken in that order.

3.3 Technique for Order Preference by Similarity to Ideal Solution Method (TOPSIS)

TOPSIS is a simple and effective multi criteria decision making tool used in many applications corresponding to sustainable concept selection, location of charging stations, computer networks, site selection for solar farms and process parameter selection in manufacturing etc., TOPSIS is one of the multi criteria decision making methods (MCDM) used to solve multi objective problems. It is based on the concept that the optimized solution should have the shortest distance from the ideal solution and the farthest distance from the negative ideal solution.

The following stages have been employed in this approach:

3.3.1 Stage 1

The data have been normalized using the following relation:

$$R_{ij} = \frac{{X_{ij} }}{{\Sigma X_{ij}^{2} }}$$
(8)

For i = 1, …, m; j = 1, …, n

3.3.2 Stage 2

Weights are allocated for each criterion considered in optimization. Equal percentage of weights is considered for all the input parameters.

3.3.3 Stage 3

A weighted normalized matrix is built by multiplying each column of the normalized matrix with the respective weights

$$V_{ij} = W_{j} R_{ij}$$
(9)

Let Wj be the weights for each input parameter where j = 1, …, n (equal to 0.2).

In order to give equal importance to all the parameters, 20% weightage is chosen for all the output parameters.

The normalized (NM) and weighted normalization matrix (WNM) for the output responses are shown in Table 11.

Table 11 Normalized and weighted normalized values

3.3.4 Stage 4

Ideal and negative ideal solution have been found using the relation given

  1. 1.

    Positive ideal solution.

$${\text{A}}^{ + } = \left\{ {{\text{V}}_{1}^{ + } , \ldots ,{\text{V}}_{\text{n}}^{ + } } \right\},$$

where \({\text{V}}_{\text{j}}^{ + } = \{ \hbox{max} \left( {{\text{V}}_{\text{ij}} } \right)\;{\text{if}}\;{\text{j}} \in {\text{J}};\,\hbox{min} \left( {{\text{V}}_{\text{ij}} } \right)\,{\text{if}}\;{\text{j}} \in {\text{J}}^{\prime } \}\).

  1. 2.

    Negative Ideal solution.

$${\text{A}}^{ - } = \left\{ {{\text{ V}}_{1}^{ - } , \ldots ,{\text{V}}_{\text{n}}^{ - } } \right\},$$

where \({\text{V}}_{\text{j}}^{ - } = \{ \hbox{min} \left( {{\text{V}}_{\text{ij}} } \right)\,{\text{if}}\,{\text{j}} \in {\text{J}};\,\hbox{max} \left( {{\text{V}}_{\text{ij}} } \right)\,{\text{if}}\;{\text{j}} \in {\text{J}}^{\prime } \} .\)

Positive and negative ideal solutions for all output responses are given in the Table 12.

Table 12 Positive and negative ideal solution for output responses

3.3.5 Stage 5

The separation measure is found out from the positive and negative ideal solution using the relation given as follows:

The separation from the ideal alternative is:

$$S_{i}^{ + } = \left[ {\sum {\left( {V_{j}^{ + } - V_{ij} } \right)^{2} } } \right]^{1/2} \quad {\text{i}} = 1, \ldots ,{\text{m}}$$
(10)

Similarly, the separation from the negative alternative is:

$$S_{i}^{ + } = \left[ {\sum {\left( {V_{j}^{ - } - V_{ij} } \right)^{2} } } \right]^{1/2} \quad {\text{i}} = 1, \ldots ,{\text{m}}$$
(11)

The values for separation measure are tabulated in Table 13.

Table 13 Separation measure for the various experimental run

3.3.6 Stage 6

Relative closeness values of a particular alternative is found using the relation:

$$P_{i} = \frac{{S_{i}^{ - } }}{{\left( {S_{i}^{ + } + S_{i}^{ - } } \right)}}\quad 0 < {\text{P}}_{\text{i}} < 1$$
(12)

The option with Pi closest to 1 is selected.

3.3.7 Stage 7

Table 14 shows the relative closeness values of each experimental run. From the list of relative closeness values, it is seen that experimental trial 9 displays the maximum relative closeness value among the nine experiments. Higher relative closeness value indicates that the respective experiment is closer to the ideal value. But in order to get the optimized set of parameters from the TOPSIS methodology, a response table has to be constructed as shown in Table 15. The response table has been formulated using the same logic as used in formulating response table for GRA.

Table 14 Relative closeness value
Table 15 Response table for average closeness value

From the response table it is seen that the optimized set of parameters fit outside Taguchi’s L9 experimentation. It is observed that level 1 in current, level 3 in voltage, level 1 in travel speed and level 1 in gas flow rate form the optimized set of input parameters according to TOPSIS.

3.4 Analysis of Variance (ANOVA)

ANOVA has been used to find out the significance of various input parameters with respect to the responses. The ANOVA table is shown in Table 16. From the table it is seen that voltage has the most influence on the characteristics of the output followed by travel speed, current and gas flow rate taken in that order. The influence of Input parameters on Output Responses is shown graphically in Fig. 3. The calculations are done based on pooled error method as followed in ANOVA for GRA using MINITAB software.

Table 16 Analysis of variance (ANOVA) for all the input parameters in TOPSIS
Fig. 3
figure 3

The influence of input parameters on output response in TOPSIS

3.5 Comparison of GRA, TOPSIS Results and Confirmation Test Results

Based on the calculation, it is found that both GRA and TOPSIS yield results outside the Taguchi’s L9 experimentation and also both GRA and TOPSIS yield different set of parameter combinations. In order to compare the results from GRA and TOPSIS and validate the analysis, the predicted closeness value is calculated for both using the following relation.

$$\alpha = \alpha_{m} + \sum {(\alpha_{n} - \alpha_{m} )}$$
(13)

αm = mean of GRG values for the taghuchi’s L9 experiments, αn = mean grey relational at the optimum level.

The predicted value from Eq. 13 for GRA and TOPSIS are 0.90674 and 1 respectively. The predicted closeness value of TOPSIS is found to be higher than that of GRA. Therefore in this study confirmation test is conducted for the optimized set of parameters obtained from TOPSIS. It is seen that the experimental closeness value is 0.98 which is still a better result than that of the taghuchi’s L9 orthogonal array. The results are shown in Table 17.

Table 17 Optimum process parameters

3.6 Mechanical and Metallurgical Characterization of the Optimized Weld

The optimized parameter welding is again carried out and the weld is instantly subjected to heat treatment cycle as done for the L9 experiments and the properties are measured and discussed with the help of microstructure, XRD and fractography.

The macrostructure of the optimized weld is taken with the help of welding expert system (Struers, Austria) with the magnification of 6.25× and is shown in Fig. 4. The bead width, reinforcement, depth of penetration of the optimized weld are 9.10, 1.42 and 4. 83 respectively.

Fig. 4
figure 4

Macrostructure of the weldment obtained with the optimized set of parameters from GRA

The microstructure of the weld, base metal, HAZ of the optimized weld are shown in the Fig. 5. The microstructure of the weld comprise of ferrite, martensite and tempered martensite. The bright portion in the microstructure is the ferrite phase and the needle like dark region represents martensite and the irregular shaped dark region represents tempered martensite. In addition to the above said phases, bainite is also found in very small proportions. Comparatively, the weld has finer grain structure leading to better mechanical properties and the base metal microstructure after post weld heat treatment has almost similar properties as that of base metal. There are no defects in all the three zones of the weld.

Fig. 5
figure 5

Microstructure of HAZ and weldment obtained with the optimized set of parameters from GRA

XRD analysis reveals the presence of some inter metallic phases such as Mo2C and VC which is shown in Fig. 6.

Fig. 6
figure 6

XRD for weldment obtained with the optimized set of parameters from GRA

Microhardness values of the optimised weld are examined along the transverse direction. Microhardness values are measured at five different points and its average value is taken. It is found that the heat affected zone of the optimised weld region has slightly more microhardness than the weld region. The main reason for this lies on the formation of Mo2C and VC precipitates during tempering and its distribution is seen more in the heat affected zone. The base metal region microhardness experiences a drastic improvement after heat treatment process. Tensile strength of the optimised weld is measured and it is found that its value is better than the annealed base metal strength. Tensile specimen break in the heat affected zone of the weld region as it have more microhardness than the base metal region. Heat input to the optimised weld has more impact on the tensile strength and it is observed that higher heat input reduces the formation of martensite in the interface of the weld and heat affected zone.

The fractography of the optimized weld tensile tested specimen is shown in the Fig. 7. The fractography reveals the presence of dimples which signifies the ductile mode of failure and also the presence of some inter metallic phases are seen in the fractograph.

Fig. 7
figure 7

SEM image for the weldment obtained with the optimized set of parameters from GRA

The Properties of the base metal after post weld heat treatment are as follows: Ultimate tensile strength—995 MPa, Microhardness—350 Hv. Thus in this work the properties of both weld and base metal after post heat treatment are made almost same.

4 Conclusion

Butt joint were successfully made between 3.7 mm thick 15CDV6 plates using GTA welding process. The input parameters were successfully optimized using GRA and TOPSIS and the following conclusions were drawn.

  1. 1.

    Full penetration was achieved in all the nine experimental runs.

  2. 2.

    Both in GRA and TOPSIS, the optimized set of parameters were found to be outside the L9 experimental run. Since the predicted GRG value in GRA was lower than predicted closeness value in TOPSIS, confirmation test was done based on the TOPSIS optimized parameter combination and confirmation test results were in good agreement with the actual results.

  3. 3.

    The Optimized parameter combinations obtained using TOPSIS were current = 110 A, voltage = 18 V, travel speed = 25 mm/min, gas flow rate = 7 lpm and the corresponding output values were bead width = 9.10 mm, reinforcement = 1.42 mm, tensile strength = 1014 MPa, hardness = 365 Hv, depth of penetration = 4.83 mm.

  4. 4.

    From GRG value, ANOVA indicated that current was the major influencing factor on the overall objective and in the case of ANOVA done with the TOPSIS relative closeness value, voltage was found to be the most influencing factor.

  5. 5.

    After post weld heat treatment, the base metal attained properties similar to that of weldments.