Abstract
Currently, the strength of hot-press-forming steel has been increased to produce lightweight vehicles, and in this study, the first arc welding investigation on a 2.0 GPa-strength hot-press-forming steel was conducted. Hot-press-forming steel sheets with thicknesses of 1.1 mm were butt-welded by gas tungsten arc welding without a filler metal, with the heat input controlled in the range of 140-260 J/mm. The weld metal, coarse-grained heat-affected zone (HAZ), and fine-grained HAZ had martensitic microstructures. The softened zone was composed of an intercritical HAZ (with polygonal ferrite and martensite/bainite) and a subcritical HAZ (with tempered martensite). The intercritical HAZ was softened the most during welding and fractured during tensile testing. The strengths of the arc welds were in the range of 1141-1264 MPa, which were 57-63% strength of the base metal. The equiaxed austenite on martensite or ferrite matrix was developed at the intercritical HAZ of gas tungsten arc welds, therefore transforming into the coarse martensite during quenching. However, the intercritical HAZ of laser welds indicated acicular austenite transforming into the fine martensite due to its high cooling rate. The intercritical HAZ softening was revealed to originate from carbon diffusion during the martensite to austenite transformation, which is unavoidable in arc welding and should be considered in the design of a welded structure.
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1 Introduction
Hot-press-forming (HPF) steel, also known as hot-forming steel or press-hardened steel, is a boron-alloyed high-strength steel with a full martensitic microstructure. Considering martensitic steels has limited formability, HPF steel sheets are supplied as low-strength pearlite structures and formed above the austenitization temperature. During forming, they are simultaneously quenched in a water-cooled die, causing an austenite-to-martensite transformation. HPF steels with a tensile strength of 1.5 GPa, represented by 22MnB5 steel, have been successfully applied to automotive body components, such as pillars, bumper beams, and impact beams. Moreover, recently steel mill companies have introduced higher-grade HPF steels in the market (Ref 1,2,3).
As welding is the main assembly process for HPF steel sheets, the weldability of 1.5 GPa-grade HPF steels has been evaluated for various welding processes. These include resistance spot welding of overlap joints (Ref 4,5,6,7,8); laser welding of overlap (Ref 9,10,11,12), butt (Ref 13, 14), and lap–fillet joints (Ref 15), and tailor-welded blanks (Ref 16,17,18,19); arc welding of butt (Ref 20,21,22) and lap–fillet joints (Ref 23); and friction stir welding of butt (Ref 24) and overlap joints (Ref 25).
However, the literature on welding higher-grade HPF steel sheets is limited compared with that on 1.5 GPa-grade HPF steels. Fahlstrom et al. (Ref 26) evaluated the laser weldability of 1.8 GPa and 1.9 GPa-tensile-strength steels. Kang and Kim (Ref 27) presented the effects of surface oxides during laser welding of 1.8 GPa HPF steel, and Shi et al. (Ref 28) demonstrated laser-welded patchwork blanks of 1.8 GPa HPF steel. Lu et al. (Ref 29) conducted the first study on the laser weldability of 2.0 GPa HPF steel, and the authors (Ref 30, 31) investigated in detail the heat-affected zone (HAZ) softening and joint strength of laser welds. More recently, laser welds of 1.5/2.0 GPa dissimilar-strength HPF steels were analyzed (Ref 32). However, within the authors’ knowledge, thus far, only laser welding has been investigated for HPF steels above 1.8 GPa.
The HAZ of an HPF-steel-weldment is softened during welding, whereas that of a mild-steel-weldment is hardened owing to the high cooling rate during welding. For partial or full martensitic steels, the degree of HAZ softening increases with increasing the tensile strength of the base metal (Ref 13, 24, 33). In a previous study on 1.5 GPa-grade HPF steel (Ref 13), the tensile strength of a laser-welded specimen was reduced by 15% owing to HAZ softening, even by low-heat-input laser welding. As a relatively high input is applied to HPF steel during arc welding, a more severe loss in tensile strength is expected compared with laser welding.
Along with resistance spot welding, arc welding is an important welding process in automotive body assembly. In this study, autogenous gas tungsten arc welding was conducted on a 2.0 GPa-grade HPF steel. The mechanical and metallurgical characteristics of the welds were investigated with various heat inputs per unit length. The measured properties were compared with those by laser welding with smaller heat input, and kinetics of HAZ softening was discussed based on the measured properties.
2 Experimental Setup
The base metal (BM) used was Docol® PHS CR 2000 supplied by SAAB AB (Ref 34), and its chemical composition is summarized in Table 1. After the HPF process, the BM had the tensile strength, hardness, and elongation of 2.08 GPa, 609 HV, and 3.36%, respectively, and had a full martensite microstructure. The details of the HPF processing and BM properties are available in the previous study (Ref 20).
Welding specimens were machined to a width of 150 mm, length of 150 mm, and thickness of 1.1 mm. Fig. 1 shows that the specimen configuration is a gapless butt joint, along which gas tungsten arc welding is conducted. A 2% thoriated tungsten rod with a diameter of 2.4 mm was used as the electrode according to the AWS A5.12 M/A5.12:2009 standard (specification for tungsten and tungsten–alloy electrodes for arc welding and cutting). The distance between the gas nozzle and the specimen was 5 mm, and the arc length was 3 mm. The work angle was 90° in the cross-sectional direction, and the travel angle was 10° inclined against the forward direction. Argon shielding gas (99.9%) was supplied at a flow rate of 15 L/min.
The welding power source was operated in the direct current electrode negative mode. Table 2 lists the detailed welding conditions adopted to change the heat input. The heat input was varied from 140 to 260 J/mm, and the welding speed was set at 5 and 10 mm/s.
The mechanical and metallurgical properties of welded specimens were measured. The specimens were polished and etched with 3% nital solution (3 mL HNO3 and 100 mL ethanol). The etched transverse cross sections were imaged using stereo microscopy, light optical microscopy (LOM), and field-emission scanning electron microscopy (FESEM) to study their microstructures. In the metallurgical analysis, the laser welding specimens used in the authors’ previous study (Ref 30) were compared with the arc welded specimens. In the comparative study, the laser power and welding speed were 2 kW and 7 m/min, respectively, and the heat input was 17.1 J/mm, much lower than that of gas tungsten arc welding in this study. Details of the laser welding conditions are provided in the previous study (Ref 30). To investigate the retained austenite in intercritical HAZ (ICHAZ), electron backscattered diffraction (EBSD) was performed at an acceleration voltage of 15 kV, a working distance of 15 mm, and a step size of 0.05 μm.
Three tensile specimens per condition were extracted from the welded specimens by using electrical discharge machining. The gage width and length were 12.5 mm and 50 mm, respectively, and the detailed shape is specified in the ASTM E8 standard. Static tensile tests were conducted at a head speed of 1 mm/min. The micro-Vickers hardness distribution was measured along the specimen centerline of the cross section of each specimen. Hardness measurements were conducted for 81 measuring points at an indent interspacing of 0.22 mm, and the load and hold time were 1.96 N and 10 s, respectively.
3 Results and Discussion
3.1 Macrosections and Hardness Profiles for Various Heat Inputs
Table 3 reports the macrosectional dimensions of the gas tungsten (GTA) welds produced for various heat inputs. Each fusion zone is indicated by a yellow dotted line. Noticeably, the bead width increased with increasing heat input. As the heat input was increased from 140 to 260 J/mm, the bead width in the centerline increased from 3.0 to 4.4 mm. White bands are observed on the cross sections outside the weld metal (WM), indicating the location of the ICHAZ (Ref 9, 13, 30). Fig. 2 shows that the hardness of the WM decreases with the increase in the heat input, and the Pearson’s r value was − 0.949. In contrast, the hardness of the supercritical HAZ adjacent to the WM was approximately 600 HV regardless of heat input and comparable to the BM hardness of 609 HV. The hardness of the ICHAZ with respect to the heat input shows a weak negative correlation with Pearson’s r value (− 0.374). In addition, the distance between the ICHAZs increased from 6.2 to 9.2 mm on increasing the heat input from 140 to 260 J/mm.
3.2 Mechanical Behavior for Various Locations
Fig. 3 shows the cross-sectional LOM images of typical welds, and the WM and the HAZ are noticeable. The detailed morphology of the welds was analyzed using FESEM, and the results are shown in Fig. 4. The BM had a full martensitic microstructure with a needle-like lath morphology (Fig. 3(b) and 4(a)). The ICHAZ exhibited a dual-phase structure of ferrite and martensite (Fig. 3(e), 4(d) and (e)), whereas other locations, such as the coarse-grained HAZ, fine-grained HAZ, subcritical HAZ, and BM, were composed of martensitic lath and/or tempered martensite.
No phase transformation is observed in the subcritical HAZ because the peak temperature is lower than the AC1 temperature; the tempered martensite (TM), including carbides, precipitates primarily along the prior austenite grain (PAG) and lath boundaries. Owing to the tempering of martensite, the sharpness of the martensite lath was reduced, whereas the packet shape remained (Fig. 3(c) and (d)). Within the SCHAZ, the locations closer to the BM (subcritical HAZ1 in Fig. 3(c) and 4(b)) showed sharper martensitic laths and fewer tempered carbides than the locations closer to the ICHAZ (subcritical HAZ2 in Fig. 3(d) and 4(c)).
The ICHAZ presented polygonal grains in the LOM image (Fig. 3(e)); more specifically, it was comprised of polygonal ferrite (PF) and martensite (M) (Fig. 4(d) and 4(e)). The full martensite of the BM is transformed into polygonal ferrite and austenite at the peak temperature between the AC1 and AC3 temperatures. Subsequently, the austenite is transformed into the nonequilibrium phase of martensite during cooling. Only the ICHAZ presents an equilibrium phase (polygonal ferrite), accompanied by martensite and bainite as nonequilibrium phases. Therefore, the ICHAZ has a lower surface energy than the other zones (Ref 35) and has a relatively lower reaction with the etchant, resulting in the white bands at the cross sections, as seen in Table 3.
As shown in Fig. 3(f)-(h) and 4(f)-(h), the fine-grained HAZ, coarse-grained HAZ, and WM regions became fully austenitic during heating and transform into full martensite during cooling owing to their peak temperatures higher than the AC3 temperature and the extremely high hardenability of the HPF steel, confirmed by the hardness profile shown in Fig. 2. In contrast, the ICHAZ and subcritical HAZ regions cannot reach the full austenization temperature (AC3) during heating, but transform into partial and tempered martensite, respectively, after welding. Consequently, the hardness values of the ICHAZ and the subcritical HAZ were relatively lower than that of the BM. The lowest hardness was observed in the ICHAZ, comprising a dual-phase structure of polygonal ferrite and martensite.
3.3 Tensile Strengths for Various Welds
The tensile strengths of the welds, as shown in Fig. 5, decreased linearly with increasing heat input. Fig. 6 shows the fracture locations in the tensile testing, indicating that a tensile fracture occurs near the ICHAZ in all cases. This test was associated with the ICHAZ having the lowest hardness, as shown in the hardness profiles in Fig. 2.
The tensile strength presents better linearity (Fig. 5) with the heat input than the hardness (Fig. 2(f)) with respect to the heat input. Pearson’s r value is − 0.9568, much better than that between the heat input and the hardness (− 0.374). The relatively low linearity between the heat input and the hardness is caused by the spatial resolution of the hardness measurement in the ICHAZ. As shown in Fig. 2, because the ICHAZ is narrow, the hardness is measured at only one or two points within it.
A tensile fracture is initiated in the middle of the specimen, as shown in Fig. 6(a), and propagates toward the edges. Simultaneous crack initiation at multiple locations was confirmed by craters, marked as red arrows in the middle (Fig. 6(b)). Moreover, shear lips and slight necking were observed at the edges with mid-to-edge crack propagation (marked as white arrows in Fig. 6(b)). Therefore, the fracture surface with a cup-and-cone shape had a ductile mode fracture (Fig. 6(b)). A dimple fracture was confirmed in the more detailed surfaces of the fracture (Fig. 7).
3.4 Microstructural Features of Weld Metal and HAZ According to Heat Input
In this section, the microstructures of the WM and ICHAZ of GTA welds with higher heat inputs and laser welding with a much lower heat input of 17.1 J/mm are discussed. The WM, coarse-grained HAZ, and fine-grained HAZ showed fully martensitic microstructures because the peak temperature exceeded the AC3 temperature, whereas the peak temperature of the ICHAZ lay between the AC1 and AC3 temperatures. In particular, HAZ softening occurred in the ICHAZ and subcritical HAZ, and the softening kinetics are discussed in detail.
3.4.1 Weld Metal Morphology for Various Heat Inputs and Laser Welds
Figure 8 presents the microstructures of the WMs of laser welding with a heat input of 17.1 J/mm and GTA welding with varying heat inputs between 160 and 260 J/mm, which increment was approximately 50 J/mm. As the heat input increased in GTA welding, the WM was primarily martensitic and had a small amount of bainite-containing carbide precipitation (Fig. 8(d)). The decrease in the heat input increases the cooling rate, which decreases the time for carbon diffusion during the austenite-to-martensite transformation. At a magnification of × 10,000, the lath width of the martensite decreased as the heat input decreased. The weakening of the martensite morphology was consistent with the decrease in the hardness with increasing the heat input. (Fig. 2). Finally, the WM morphologies of the laser and arc welds with the minimum heat input (specimen No. 2) were similar despite a significant difference in the heat input.
From the analytical solution for the temperature distribution of a thin sheet by a moving heat source (Ref 36), the cooling time from 800 °C to 500 °C can be calculated by the following equation (Ref 37):
where q is the actual power of the heat source, v is the welding speed, λ is the thermal conductivity, ρ is the density, c is the specific heat, d is the thickness of the sheet, and T0 is the room temperature in degree Celsius. The actual power of the heat source can be calculated by multiplying the welding power and the welding efficiency, η.
The cooling rate for each case is calculated using the material properties and parameters listed in Table 4, and the calculated values are listed in Table 5. The mill maker recommends a cooling rate of at least 60 K/s for the hot-press-forming process to achieve full design hardness (Fig. 9) (Ref 34). The cooling rates for Fig. 8(a) and (b) are higher than 60 K/s, explaining the identical WM morphology for both cases despite the large difference in the cooling rate. In the highest heat input case (260 J/mm), the cooling rate is reduced to 10.3 K/s. Therefore, bainite formation in Fig. 8(d) can be explained by the cooling rate and the continuous cooling transformation (CCT) diagram (Fig. 9).
3.4.2 ICHAZ Morphology for Various Heat Inputs Arc Welds and Laser Welds
In the welds of partial or full martensitic steel with a strength over 780 MPa, softening is unavoidable in the ICHAZ (Ref 39). Consequently, the width of the ICHAZ (Ref 40) and the amount of softening determine the strength of the welded joint and the fracture location during tensile testing (Ref 33).
The ICHAZ width was measured at five points along the depth direction for the laser welds and arc welding specimen no. 2, and it was indicated with the boxplot shown in Fig. 10. The ICHAZ width with GTA welding was 380 μm, approximately 13 times larger than that in laser welding (29 μm). In both cases, the tensile specimens were fractured in the ICHAZ. In the laser welding of 800 MPa-grade dual-phase steel (Ref 40), HAZ softening did not affect the fracture location and tensile strength when the heat input was below 42 J/mm, despite the ICHAZ width in the reference being much larger than the ICHAZ width in this study. Furthermore, in the case of 1180 MPa-grade transformation-induced plasticity (TRIP) steel, the heat input criterion for determining the ICHAZ fracture was 80 J/mm (Ref 41). The ICHAZ hardness of 2.0 GPa-grade HPF steel was similar to that of 800 MPa-grade dual-phase steel and 1180 MPa-grade TRIP steel. However, BM fracture rarely occurred in this study despite the narrow ICHAZ because the strength difference between the ICHAZ and the BM was significantly larger than that of lower-grade steels.
Fig. 11 shows the ICHAZ microstructures for various heat inputs. Although the laser welds with a heat input of 17.1 J/mm and GTA welding specimen No. 2 with a heat input of 160 J/mm indicated similar WM microstructures of full martensite (Fig. 8), the ICHAZ microstructures were clearly different from each other (Fig. 11). The ICHAZs of the GTA welds consisted of polygonal ferrite and martensite, whereas those of the laser welds included martensite and lath ferrite. It was also coincided with the previous study (Ref 30). The WM microstructure according to the heat input is determined solely by the cooling rate along the CCT curve (Fig. 9) since the WM is rapidly cooled through the austenite single-phase area from a liquid state. In comparison, the ICHAZ is rapidly cooled from the austenite and ferrite area between A1-A3 temperatures, and the ICHAZ microstructure depends on the cooling rate and time to stay in the A1-A3 region according to the heat input. In the HPF steel welds with significantly high hardenability, most austenite in the A1-A3 region is transformed to martensite during quenching. A small amount of carbide is observed in the ICHAZ of the GTA welds when the cooling rate is 40 K/s or less (Fig. 9).
The ICHAZ microstructure changes with the heat input significantly depending on the phase transformation process from martensite to ferrite and austenite. The microstructure of the ferrite–martensite transformation in the ICHAZ is completely different from that of martensite in the BM, suggesting that sufficient carbon is diffused and the grains are restructured during the martensite to austenite transformation in the ICHAZ. The kinetics of this process will be discussed in the coming Section 3.4.3.
HAZ softening is related to the welding process and specifically heat input and the cooling rate determines the extent of softening (Ref 42). The ICHAZs under various heat inputs are compared in Fig. 12, and the heat input for the samples is listed in Table 6. When heat input was between 17.1-45 J/mm, the boundary of the initial martensite morphology appeared to be maintained (Fig. 12(a)-(c)). As the heat input increased to 60-5.7 J/mm, the size of ferrite grain increased and the shape changed from lath into polygonal (Fig. 12(d) and (e)). By increasing the heat input more than 160 J/mm, the ferrite grain had the equiaxed morphology and the ferrite fraction increased (Fig. 12(f)).
3.4.3 Kinetics of HAZ Softening for Gas Tungsten Arc and Laser Welds
Apple and Krauss suggested two mechanisms in the martensite to austenite transformation of high carbon steel (Ref 43). At higher heating rate, plate-like or acicular austenite was alternated with martensite in the ICHAZ. At lower heating rate, austenite had equiaxed morphology, curved boundaries, and lack of sharp surface due to the thermally activated mechanism.
The kinetics for ICHAZ softening is depicted in Fig. 13. At the earliest stage of GTA welding, carbon in martensite is precipitated along the packet, block, and lath boundaries and their triple junctions in Fig. 13(a). As the temperature increased just below the AC1 temperature, carbide increased. Furthermore, the lath boundary got disappeared and the packet boundary became slightly curved, as shown in the Subcritical HAZ2 (Fig. 4(c)). At the ICHAZ, the temperature was between AC1 and AC3, and carbon was diffused into austenite across the boundaries. Due to the volume change during austenization (Ref 44), boundaries became round, and equiaxed austenite on martensite or ferrite matrix was developed at the ICHAZ. During cooling, the equiaxed austenite was transformed into coarse martensite (Fig. 13(a)). Therefore, the ICHAZ was composed of martensite, bainite, and ferrite as shown in Fig. 11(a).
In laser welding, phase transformation is relatively simple. The martensite boundaries of the packet, block, and lath were maintained during welding due to its high cooling rate. Carbon was diffused along the boundaries as in the GTA welding, and carbon-rich lath was transformed into austenite with sluggish diffusion of carbon across the boundaries. And a ferrite lath was formed in the area with relatively low carbon. During cooling, acicular austenite was transformed into fine martensite (Fig. 13(b)).
The phase distribution and retained austenite locations were confirmed by EBSD of GTA and laser welds (Fig. 14). In the phase map (Fig. 14(c) and (f)), the red grains represent the retained austenite with FCC structure (white arrows in Fig. 14), and the green color indicates either ferrite with the BCC structure or martensite with the BCT structure. The retained austenite was observed in the triple junction due to the high surface energy in both ICHAZs of GTA and lase welds. In image quality maps (Fig. 14(a) and (d)), the dark area represents martensite with high deformation density inside the grain. The martensite packets with various crystal orientations are represented as various colors in inverse-pole figure maps (Fig. 14(b) and (e)). The feature morphology of the ferrite and martensite packet corresponded well with Fig. 11.
4 Conclusions
This study conducted the first investigation on an arc-welded HPF steel with a strength of 2.0 GPa. A detailed analysis of the mechanical and microstructural properties of the autogenous GTA welds produced by various heat inputs (140-260 J/mm) was performed and the following conclusions were drawn:
-
1.
In the GTA welds, the WM, coarse-grained HAZ, and fine-grained HAZ had fully martensite microstructures, while the ICHAZ and subcritical HAZ contained dual-phase (ferrite and martensite) and tempered martensite, respectively. The ICHAZ had the lowest hardness among the weldments, ranging between 287 HV and 322 HV under the heat inputs applied in this study.
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2.
The tensile strength of the GTA welds decreased from 1264 to 1141 MPa as the heat input increased from 140 to 260 J/mm. Fracture occurred in the ICHAZ, the most softened zone, and it was initiated in the ductile mode at the mid-thickness of the specimen and propagated toward the edge.
-
3.
The hardness of the coarse-grained HAZ and fine-grained HAZ was similar to that of the BM, while the WM had a slightly lower hardness than the BM. The WM primarily had a martensite structure, and a small amount of bainite formation was observed as the heat input was more than 200 J/mm, as confirmed by the CCT diagram.
-
4.
The ICHAZ of GTA welds showed a dual-phase structure of polygonal ferrite and martensite/bainite, unlike those of the laser welds composed of martensite and lath ferrite. The width of the arc ICHAZ (380 μm) was significantly larger than that of the laser ICHAZ (29 μm).
-
5.
The packet boundaries of ICHAZ of GTA welds became round and equiaxed austenite on martensite or ferrite matrix was developed at the ICHAZ, therefore transforming into the coarse martensite during quenching. However, the ICHAZ of laser welds indicated acicular austenite transforming into the fine martensite due to its high cooling rate.
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Acknowledgments
This study was supported by the Technology Innovation Program-Materials and Components Development Program (Grant No. 20011427) and Industrial Strategic Technology Development Program (Grant No. 20014820), funded by the Korean Ministry of Trade, Industry, and Energy (MOTIE).
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Kim, K., Park, H., Kang, N. et al. Mechanical and Microstructural Properties of Autogenous Arc Welds of 2 GPa Strength Hot-Press-Forming Steel. J. of Materi Eng and Perform 33, 5988–5999 (2024). https://doi.org/10.1007/s11665-023-08378-3
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DOI: https://doi.org/10.1007/s11665-023-08378-3