1 Introduction

Considering the importance of mechanical properties in the design of timber structures, such as bridges, sheds and timber residences (Dadzie and Amoah 2015), it is of great relevance to evaluate equations that aim to estimate the characteristic strengths of species for structural use. In Brazil, the timber structures have an elevated applicability potential due to a vast number of wood species existing in the Amazonian rainforest, estimated at more than 10,000 species according to Steege et al. (2016). This number induces the development of new research focused on unknown species, which may replace those that are already commonly used in civil construction. Works by Ravenshorst et al. (2004), Ruelle et al. (2011), Mascia and Nicolas (2013), Segundinho et al. (2015), dos Reis et al. (2018), and Silva et al. (2018) can be mentioned as researches that sought to investigate different wood species for structural use.

The use of timber for structural purpose is regulated in Brazil by standard ABNT NBR (1997), which establishes the requirements for project development, construction and control of wood structures, based on semiprobabilistic methods, which assess fracture strength, instability, excessive deformation, and durability of the structure.

Thus, it is important to examine the equations that estimate the mechanical strengths of the species used in construction. Such equations are established in the Brazilian standard, which allows obtaining the characteristic values used for structural design for distinct properties (compressive, tensile and shear strengths) of the well-known woods. However, Logsdon et al. (2010) emphasize that these equations should not be the only rule for determination of characteristic wood properties. They sought to benchmark a model for characteristic compression strength (\(f_{c0,k}\)) estimation for Dinizia excelsa species and concluded that NBR equation is more conservative as it provides slightly lower \(f_{c0,k}\) values.

Similarly, Matos and Molina (2016) investigated a correlation between compression and shear strength (\(f_{c0,k}\) and \(f_{v0,k}\)) of Pinus elliotti and Corymbia citriodora species, comparing an experimental relation with the standardized relations of ABNT NBR (1997) and ISO 13910 (2005), and concluded that the values obtained from relations of the Brazilian standard were superior to those of the European standard for both species.

Longui et al. (2017) also researched the shear strength parallel to the grain with tests on four Brazilian wood species. The research evaluated the shear with distinct ray orientation and concluded that specimens with parallel ray orientation to the shear plane did not differ statistically from shear values when compared to specimens having perpendicular and diagonal orientation to shear plane. Already Aicher et al. (2018) studied the shear strength and wood failure of European and tropical hardwoods.

Recently, Christoforo et al. (2019a) evaluated relations based on the probability models to check which model was more adherent and accurate in estimating the characteristic values, \(f_{t0,k}\), \(f_{v0,k}\) and \(f_{c0,k}\), comparing five wood species with the estimates from ABNT NBR (1997). Among the evaluated relationships, the obtained results were significantly higher (up to \(92\%\)) when compared to those estimated by the Brazilian standard.

These studies demonstrate the importance of assessing the mechanical properties of wood in order to obtain reliable and safe estimates for structural design. Several authors can be cited for investigating the species studied herein, focusing on physical and mechanical properties for distinct sites: Mezilaurus itauba (da Silva et al. 2014), Parinari excelsa (Almeida et al. 2015), Hymenaea sp. (Icimoto et al. 2015), Dinizia excelsa (Ravenshorst 2015), Cedrela sp. (Soriano et al. 2015; Tenorio and Moya 2018), Copaifera sp. (Aquino et al. 2018), Goupia sp. (Almeida et al. 2018), and Peltophorum sp. (Christoforo et al. 2019b).

Observing the studies presented here, it may be possible to estimate mechanical properties of distinct wood species for structural purpose using probability models. So, this paper aimed to evaluate, using 30 wood species, the chance to use possibility models to estimate the mechanical properties (compressive, tensile and shear strength) with a set of experimental results. A need for such estimates motivated the present study, thus reinforcing the reliability of the statistical analyses carried out here for tropical hardwoods, enabling their use for structural purpose.

2 Materials and methods

In this work, homogeneous batches, of 30 wood species (Table  1) were used in the experimental tests, as required by ABNT NBR (1997) with a batch volume limited to \(12~m^3\) and the specimens randomly extracted, limited to one sample per bar for each test, according to the scheme in Fig. 1. In order to carry out the tests, all specimens were stored at \(12\%\) moisture level, which corresponds to equilibrium moisture content as defined by this standard. These tests were performed at the LaMEM (Laboratório de Madeiras e Estruturas de Madeiras) of the University of São Paulo, following the procedures of ABNT NBR (1997, Appendix B).

Fig. 1
figure 1

Extraction scheme and dimensions (in mm) of specimens for compressive, tensile and shear tests

It should be noted that 12 specimens were used for each mechanical property of 30 hardwood species as shown in Table 1, following the Brazilian Standard, resulting in a total of 1080 experimentally obtained values. Two trees per wood species were used to produce the specimens. According to the Brazilian standard, the specimens must be free of defects and extracted far from the end of the bar, randomly chosen along the wood batch.

Table 1 Scientific name and identification (ID) of 30 tropical hardwoods

It can also be highlighted that the statistical equivalence of strength properties between small and defect-free specimens and structurally sized elements has been proven for native forest wood trees, used in this research, and for planted forest wood trees (Lanini 2018).

2.1 Characteristic strength values from Brazilian standard

The characteristic value of the evaluated properties (\(f_{c0}\), \(f_{t0}\) and \(f_{v0}\)) were calculated from 12 specimens for each species using the equations recommended by ABNT NBR (1997). The characteristic strength value (\(f_{w,k}\)) is given as the highest value among the values of \(f_1\), the value equivalent to \(70\%\) of the value of \(f_{m}\), and the value equivalent to \(1.10\cdot z_{b}\), that is:

$$\begin{aligned} f_{w,k} = \left\{ f_{1}; ~0.70\cdot f_{m}; ~1.10\cdot z_{b} \right\} , \end{aligned}$$
(1)

where \(f_{m}\) is the average strength value obtained from the tested samples, and the estimator \(z_{b}\) is given as:

$$\begin{aligned} z_{b} = \left( 2~\frac{f_{1} + f_{2} + f_{3} + \ldots + f_{\left( \frac{n}{2}-1\right) }}{\left( \frac{n}{2}-1\right) } - f_{\left( \frac{n}{2}\right) } \right) , \end{aligned}$$
(2)

where \(f_{n}\) is n determined strength values, arranged in ascending order (\(f_{1}\), \(f_{2}\), \(f_{3}\)\(\ldots\)\(f_{n}\)).

Pinto et al. (2004) emphasize which adoption of Eq. 1 can result in significantly different values (or not) from the characteristic value associated with a given probability density model, considering the diversity of probability functions. This fact contributes to the objectives of this study, with the possibility of adopting new probabilistic models, such as those mentioned in the sequence.

2.2 Probability density functions (PDFs)

The relations proposed by the Brazilian standard (Eq. 1) can be evaluated from the probability distribution function (PDF) obtained for each mechanical property evaluated in this research. The probability function (f) of an aleatory variable (x) is expressed as Normal (N), LogNormal (L), Weibull (W) and Exponential (E) functions, respectively, as follows:

$$\begin{aligned} f(x)=\frac{1}{\sigma \sqrt{2 \pi }} \cdot e^{-\frac{1}{2}\cdot (\frac{x- \mu }{\sigma })^{2}}, ~x ~\epsilon ~(-\infty , \infty ) ~, \end{aligned}$$
(3)

where \(\sigma\) is the standard deviation and \(\mu\) the population mean of normal function;

$$\begin{aligned} f(x)= \left\{ \begin{array}{ll} \frac{1}{x\cdot \sigma \cdot \sqrt{2\pi }} \cdot e^{-\frac{1}{2}\cdot (\frac{ln(x)-\mu }{\sigma })^{2}}, &{} \hbox { if x }> 0; \\ ~~~~~~~~~~~~~~~~~ 0 ~~~~~~~~~~~~~~~~, &{} \hbox { if x }\le 0. \end{array} \right. \end{aligned}$$
(4)

where \(\sigma\) is the standard deviation and \(\mu\) is the log population mean;

$$\begin{aligned} f(x)=\frac{\beta }{\alpha ^\beta } \cdot x^{\beta -1} \cdot e^{-(\frac{x}{\alpha })^\beta }, ~ x~>~0 ~, \end{aligned}$$
(5)

where \(\beta\) and \(\alpha\) are the shape and scale parameters, respectively;

$$\begin{aligned} f(x) = \frac{1}{\theta } \cdot e^{-\frac{x}{\theta }}, ~ x~>~0 ~, \end{aligned}$$
(6)

where \(\theta\) is the scale parameter.

The adherence tests, at the level of \(95\%\) of reliability used to verify the best PDF, were obtained via least squares estimation (LSE) and Minitab Software support (Minitab 2018).

The characteristic values (\(f_{c0,k}\), \(f_{t0,k}\) and \(f_{v0,k}\)) obtained using the four PDFs (Eqs. 36) were related to the mean value of the variable (\({\bar{x}}\)), the coefficient of variation (\(CV\%\)), and the lowest (LO) and the highest (HI) strength value using a multiple linear regression model based on the analysis of variance (ANOVA); to evaluate the quality of adjustment, the coefficient of determination (\(R^{2}\)) was used:

$$\begin{aligned} f_{w,k}^{Prob} = \beta _{0} + \beta _{1} \cdot {\bar{x}} + \beta _{2} \cdot CV + \beta _{3} \cdot LO + \beta _{4} \cdot HI + \varepsilon ~, \end{aligned}$$
(7)

where \(\beta _{i}\) consists of the coefficients adjusted by the LSE and \(\varepsilon\) is the random error.

Therefore, the ANOVA is adopted to verify the accuracy of probabilistic equations (Eq. 7), when compared to the proposition of the Brazilian standard (Eq. 1). The distribution normality of ANOVA was validated with the normality test by Anderson-Darling (Weerahandi 1995), with significance level of 0.05. Given the hypotheses accepted, P-value (probability P) equal to or greater than \(5\%\) implies accepting the null hypothesis (\(H_0\)—the model is not representative or variations of the factors do not explain the variations in the dependent variable), and rejecting the null hypothesis, if P-value \(<0.05\) (alternative hypothesis, \(H_1\)).

Firstly, the statistical equivalent, between Eqs. 1 and 7, is confirmed by Tukey pairwise comparisons. In this test, A and B denote, respectively, the first and second group with the highest mean value and the same letters indicate statistically equivalent means. Finally, the coefficient of determination (\(R^{2}\)) was used as a criterion to validate the PDF of better adherence.

3 Results and discussion

Firstly, Fig. 2 shows the mean values, confidence intervals (CI for \(95\%\) confidence level) of the strength properties (Fig. 2a (\(f_{c0}\)), b (\(f_{t0}\)), and c (\(f_{v0}\))) of the 30 hardwoods investigated. The individual standard deviations were used to calculate the CIs, being compared with those found in ABNT NBR (1997, Appendix  E). Species highlighted in gray exceeded the CI values stipulated by this standard.

Fig. 2
figure 2

Results for compressive (a), tensile (b), and shear (c) strengths from the mean values and confidence intervals (95% CI) for the 30 hardwood species

The coefficients of variation of \(f_{c0}\) (Fig. 2a) reached those referenced by the Brazilian standard with ranges of variance equal to the \(CV(\%)=(04\) to 26). However, for some species this limit was exceeded: Silva et al. (2018) Erisma uncinatum (\(26\%\)), Icimoto et al. (2015) Cedrelinga cateniformis (\(23\%\)), Kollmann and Côté (2015) Goupia paraensis (\(20\%\)), Segundinho et al. (2015) Tapirira sp. (\(22\%\)), Steege et al. (2016) Vochysia haenkeana (\(20\%\)), and Christoforo et al. (2019a) Cassia ferruginea (\(19\%\)) (highlighted in light grey).

Already for the \(f_{t0}\) (Fig. 2b), most species reached coefficients of variation above the values recommended by the Brazilian standard. The ranges of variance were equal to the \(CV(\%)=\) (13–36). The high values of this coefficient can be explained, according to Kollmann and Côté (2015), by the rupture mode of the material during loading and the intrinsic wood anatomical structure of each species. These aspects include the type of applied stress, grain direction, density, as well as orthotropy, and it demonstrates the importance of more detailed studies on such behaviors. So, only the species Ocotea neesiana (\(18\%\); Mascia and Nicolas 2013), Manilkara inundata (\(18\%\); Minitab 2018), Parkia pendula (\(16\%\); Almeida et al. 2015), Calycophyllum multiflorum (\(15\%\); Dadzie and Amoah 2015), Clarisia racemosa (\(15\%\); Ravenshorst 2015), and Sextonia rubra (\(13\%\); Matos and Molina 2016) reached values of the coefficient as expected, while for other species the values of the coefficients differed from the standard (highlighted in light grey).

For the strength \(f_{v0}\) (Fig. 2c), all the species reached coefficients of variation in accordance with those referred to by the standard. The ranges of variance were equal the \(CV(\%)=\) (07–28).

To compare the values presented in Fig. 2, the \(CV=18\%\) was used for normal stresses and \(28\%\) for tangential stresses, according to the Brazilian standard. It is important to emphasize, however, that this standard does not require the difference in the CV, i.e., Eq. 1 is formulated for a \(CV=18\%\), regardless of the mechanical strength to be calculated.

Table 2 shows the characteristic values for compressive, tensile, and shear strengths calculated, following Eq. 1, from 1080 experimental values obtained for the 30 species.

Table 2 Characteristic values for compressive, tensile, and shear strengths, according to (ABNT NBR 1997) (Eq. 1)

The characteristic values calculated by Eq. 1, the PDF of better adherence is defined by the highest P-value for each of the 30 tropical hardwoods.

Sequentially, the mean values (\({\bar{x}}\) in MPa), the coefficient of variation (\(CV\%\)) and the lowest (LO in MPa) and highest (HI in MPa) strength values (\(f_{c0}\), \(f_{t0}\), and \(f_{v0}\)) are adopted in the construction of the equation to estimate the probabilistic characteristic value, according to the multivariate linear regression model based on ANOVA (Eq.  7).

3.1 PDFs for compressive strength

Table 3 shows the characteristic values of compressive (\(f_{c0,k}^{Prob}\)) strength obtained using the PDF of better adherence, among the four distribution functions, following Eqs. 36. Note that \(57\%\) (17/30) obtained better adjustments by the LogNormal (L), \(27\%\) (8/30) by the Normal (N), and \(16\%\) (5/30) by the Weibull (W) functions.

Table 3 Characteristic values of \(f_{c0,k}^{Prob}\) strength, according to PDF of better adherence

From ANOVA of the regression function (Eq. 7), the model is significant given a coefficient \(R^{2}\approx 99\%\), which results in an error close to \(<1\%\). Therefore, the estimate of \(f_{c0,k}^{Prob}\) can be expressed by Eq. 8, as follows:

$$\begin{aligned} f_{c0,k}^{Prob} = 7.91 + 0.48 {\bar{x}} - 0.56 CV + 0.39 LO ~[R^{2}=99.5\%] \end{aligned}$$
(8)

It is observed that three terms are significant (\({\bar{x}}\), CV, LO), and the term HI is not significant, according to Table  4.

Table 4 Results of ANOVA on the sample sets: \(f_{c0,k}^{Prob}\) (probability compressive values)

It should be noted that it was possible to exclude the non-significant coefficients without influencing the \(R^{2}\) value.

3.2 PDFs for tensile strength

Table 5 shows the characteristic values for tensile (\(f_{t0,k}^{Prob}\)) strength obtained using the PDF of better adherence, among the four distribution functions (Eqs. 36). It is noteworthy that \(53\%\) (16/30) obtained better adjustments by the LogNormal (L), \(37\%\) (11/30) by the Normal (N), and \(10\%\) (3/30) adjusted by the Weibull (W) functions.

Table 5 Characteristic values of \(f_{t0,k}^{Prob}\), according to the best PDF

From ANOVA of the regression function (Eq. 7), the strength \(f_{t0,k}^{Prob}\) can be estimated by Eq. 9:

$$\begin{aligned} f_{t0,k}^{Prob} = 24.26 + 0.42 {\bar{x}} - 1.01 CV + 0.33 LO ~[R^{2}=96.3\%] \end{aligned}$$
(9)

It is observed that three terms are significant (\({\bar{x}}\), CV, LO), and the term HI is not significant (Table 6), whose model was considered significant given the coefficient \(R^{2}\approx 96\%\), which results in an error close to \(<4\%\).

Table 6 Results of ANOVA on the sample sets: \(f_{t0,k}^{Prob}\) (probability tensile values)

3.3 PDFs for shear strength

Table 7 shows the characteristic values for tensile (\(f_{v0,k}^{Prob}\)) strength obtained using the PDF of better adherence, among the four distribution functions (Eqs. 36). It is emphasized that \(43\%\) (13/30) obtained better adjustments by the Normal (N), \(43\%\) (13/30) by the LogNormal (L), and \(14\%\) (4/30) adjusted by the Weibull (W) functions.

Table 7 Characteristic values of \(f_{v0,k}^{Prob}\), according to the best PDF

It is observed from Table 8 that only two terms are significant (\({\bar{x}}\), CV), whereas the terms LO and HI are not significant, whose model was considered significant given the coefficient \(R^{2}\approx 97\%\), which results in an error close to \(<3\%\). Therefore, the \(f_{v0,k}^{Prob}\) can be expressed by Eq. 10, as follows:

$$\begin{aligned} f_{v0,k}^{Prob} = 4.27 + 0.74 {\bar{x}} - 0.25 CV ~~~~~[R^{2}=97.7\%] \end{aligned}$$
(10)
Table 8 Results of ANOVA on the sample sets: \(f_{v0,k}^{Prob}\) (probability shear values)

Again, the exclusion of non-significant terms (LO and HI) did not have an effect on a high value of \(R^{2}\) coefficient.

3.4 Synthesis of the results

Table 9 shows the characteristic values estimated from probabilistic functions for compressive (\(f_{c0,k}^{Prob}\)—Eq.  8), tensile (\(f_{t0,k}^{Prob}\)—Eq. 9), and shear (\(f_{v0,k}^{Prob}\)—Eq. 10) strengths.

Table 9 Characteristic values of the mechanical properties estimated by probabilistic functions (PDFs)

Finally, the statistical equivalence between Eq. 1 (Brazilian standard approach) and, respectively, Eqs. 8, 9, and 10 was confirmed by Tukey pairwise comparisons, at \(95\%\) confidence level. Table 10 presents the grouping information for compressive, tensile and shear strengths.

Table 10 Tukey pairwise comparisons for compressive, tensile and shear strengths

It is important to highlight the non-statistical equivalence for tensile strength, according to Table 10. This fact reinforces the importance of the revision of the equations proposed in the Brazilian standard, highlighting the probabilistic functions proposed in this study, which can be included in this normative document.

From the results for each of the 30 tropical hardwoods, the mean characteristic values can be calculated by the Brazilian standard equations (Eq. 1) and by regression models proposed in this research (Eqs. 8, 9 and 10). Figure 3 shows the comparison of these values, respectively, for compressive, tensile, and shear strengths.

Fig. 3
figure 3

Characteristic values of compressive, tensile, and shear strength from the mean value of 30 hardwoods—Brazilian standard (left) and probabilistic (right) values

Finally, it should be pointed out that the probabilistic models herein proposed have mean values below those suggested by the Brazilian standard and, therefore, being in favor of safety in the design of timber structures.

4 Conclusion

The mechanical properties of 30 species were experimentally determined and the obtained values were in accordance with those found in ABNT NBR (1997, Appendix E), with results for a great variety of tropical Brazilian species with structural potential in the civil engineering and possibilities of application in the manufacturing industry of hardwoods.

The probabilistic functions (Eqs. 8, 9 and 10) proposed in this research are an alternative to the equations of the Brazilian standard, with great potential of application to tropical species worldwide, considering the wide set of species herein studied.

The high coefficients of determination (\(R^2\)) achieved in this research demonstrate that these probabilistic models are appropriate for estimating the characteristic values of compressive, tensile and shear strengths. This fact reinforces the importance of the revision of ABNT NBR (1997) with the inclusion of the probabilistic models here proposed for tropical hardwood species.